Validation of the Charm 3 SL3 β-lactam test for screening raw milk in compliance with the U.S. pasteurized milk ordinance

Journal of AOAC International

Volumn 94, Issue 1, 2011, Pages 348-357

  Salter, Robert S ^a   Douglas, David ^a   McRobbie, Lindsey ^a   Quintana, Julio ^a   Legg, David ^a   Schwartz, Janine ^a   Conaway, David ^a   McPhee, Carla ^a   Saul, Steven ^a   Markovsky, Robert ^a   Boison, Joe ^b   Kijak, Phil ^c   Agin, Jim ^d  

^a Charm Sciences Inc   (United States)

^b CANADIAN FOOD INSPECTION AGENCY   (Canada)

^c CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

^d Q Laboratories Inc   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ACTIVE METABOLITES; AMOXICILLIN; ANALYTES; BACTERIAL CELLS; CENTER FOR VETERINARY MEDICINES; DAIRY CATTLES; DETECTION LEVELS; FOOD AND DRUG ADMINISTRATION; FROZEN SAMPLE; LATERAL FLOWS; PASTEURIZED MILK; PENICILLIN G; RAW MILK; RESEARCH INSTITUTES; SOMATIC CELLS; TEST PROCEDURES; TESTING PROGRAMS;

DAIRIES; DRUG PRODUCTS; METABOLISM; METABOLITES; VETERINARY MEDICINE;

TESTING;

ANTIINFECTIVE AGENT; BETA LACTAM;

ANIMAL; ARTICLE; CATTLE; CHEMISTRY; FOOD ANALYSIS; FOOD CONTAMINATION; LEGAL ASPECT; METHODOLOGY; MILK; QUALITY CONTROL; STANDARD; UNITED STATES; VALIDATION STUDY;

ANIMALS; ANTI-BACTERIAL AGENTS; BETA-LACTAMS; CATTLE; FOOD ANALYSIS; FOOD CONTAMINATION; MILK; QUALITY CONTROL; UNITED STATES;

BACTERIA (MICROORGANISMS); BOS;

EID: 79551565614     PISSN: 10603271     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (19)

1. Salter, R.S., Conaway, D., & Markovsky, R. (2008) J. AOAC Int. 91, 675-683
2. Maturin, L. (2008) Milk Residues: What, When, Where and How to Do Drug Residue Tests, National Mastitis Council Proceedings, New Orleans, LA, pp 28-33
3. U.S. Department of Health and Human Services (2007) Pasteurized Milk Ordinance, Appendix N, U.S. Food and Drug Administration, Public Health Service, Publication 229, Washington, DC
4. U.S. Food and Drug Administration, Center for Veterinary Medicine (2009) Data Requirements for Milk Screening Tests Labeled for Testing Milk at the Bulk Tank/Tanker Truck for Drug Residues-Tests with Instrument Readers/Printers Only-Antibiotic Class: β-Lactams, Laurel, MD
5. U.S. Food and Drug Administration (Jan. 2010) Coded Memorandum to NCIMS M-a-85 Revision 13-Approved β-Lactam Tests and Their Detection Levels, IMS List HFS 626, Vol. 07-4, Washington, DC
6. U.S. Pharmacopeia (2009) 32nd Ed., U.S. Pharmacopeial Convention Inc., Rockville MD, pp 86-90
7. U.S. Food and Drug Administration (July 31, 1996) Coded Memorandum to NCIMS M-a-85 Rev. 5, Charm II β-Lactam Quantitative Assay Screening and Detection Levels, IMS List, HFS 626, Vol. 97-2, Washington, DC
8. Code of Federal Regulations (1994) Title 21, Part 58, U.S. Government Printing Office, Washington, DC
9. XLStat Software, http://www.xlstat.com/en/ho-Hlt191261487-Hlt191261487- Hlt191261488me (accessed February 2008)
10. ISO 5725-2 (1994) Accuracy (Trueness and Precision) of Measurement Methods and Results, International Organization for Standardization, Geneva, Switzerland, pp 6-9
11. Youden, W.J., & Steiner, E.H. (1975) Statistical Manual of the AOAC, AOAC INTERNATIONAL, Gaithersburg, MD, pp 33-36
12. Chu, P., Von Bredow, J., & Carson, M. (2000) Multiresidue Detection of 5 β-Lactam Residues in Milk by HPLC, U.S. Food and Drug Administration, Center for Veterinary Medicine, Laurel, MD
13. Jaglan, P., Yein, F., Hornish, R., Cox, B., Arnold, T., Roof, R., & Gilbertson, T. (1992) J. Dairy Sci. 75, 1870-1876
14. Moats, W., & Raida, H. (1995) J. AOAC Int. 79, 49-54
15. Schermerhorn, P., Ngoh, M.A., Chu, P., & Von Bredow, J. (Nov. 22, 2000) Procedure for Determination of Cephapirin and Ceftiofur Residues in Bovine Milk Using Liquid Chromatography and Ultraviolet Light Detection, U.S. Food and Drug Administration, Center for Veterinary Medicine, Laurel, MD
16. Zomer, E., Quintana, J., Saul, S., & Charm, S. (1995) J. AOAC Int. 78, 1165-1172
17. Salter, R.S., Legg, D., Ossana, N., Boyer, C., Skeemaker, J., Markovsky, R., & Saul, S. (1999) J. AOAC Int. 84, 29-36
18. Aki, H., Sawawai, N., Yamamoto, K., & Yamamoto, M. (1991) Pharm. Res. 8, 119-122
19. Van Der Bijl, P., Seifart, H.I., Parkin, D.P., & Mattheyse, F.J. (1988) S. Afr. Medical J. 73, 453-455