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79551489575
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- 1): 3078(w), 1599(m), 1515(s), 1456(w), 1433(w), 1403(w), 1361(m), 1269(m), 1241(w), 1166(w), 1127(m), 1100(w), 1059(s), 1031(s), 994(w), 953(w), 929(m), 878(w), 801(m), 774(s), 720(s).
-
- 1): 3078(w), 1599(m), 1515(s), 1456(w), 1433(w), 1403(w), 1361(m), 1269(m), 1241(w), 1166(w), 1127(m), 1100(w), 1059(s), 1031(s), 994(w), 953(w), 929(m), 878(w), 801(m), 774(s), 720(s).
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29
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79551493213
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- 1): 3079(w), 1615(w), 1601(w), 1531(s), 1439(m), 1402(m), 1360(s), 1314(w), 1272(s), 1245(s), 1224(w), 1118(s), 1094(w), 1057(s), 1013(w), 1022(w), 978(w), 921(s), 888(m), 804(s), 782(s), 720(s).
-
- 1): 3079(w), 1615(w), 1601(w), 1531(s), 1439(m), 1402(m), 1360(s), 1314(w), 1272(s), 1245(s), 1224(w), 1118(s), 1094(w), 1057(s), 1013(w), 1022(w), 978(w), 921(s), 888(m), 804(s), 782(s), 720(s).
-
-
-
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30
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79551499220
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-
note
-
- 1, R(wR) = 0.0384 (0.0699) and GOF = 0.969 for 3858 reflections with I > 2σ(I). The crystal structure of 1 and 2 were solved by direct method and refined by full-matrix least-squares using the SHELXTL-97 program. All non-hydrogen atoms of 1-2 were refined anistropically, and all the hydrogen atoms attached to carbon were fixed at their ideal positions.
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31
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36248990704
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Ye, J.W.2
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Zhang, D.J.4
Ma, K.R.5
Ha, J.6
Xu, J.N.7
Zhang, P.8
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