Tetrameric entity resulting from two distinct dinuclear uranyl-centered motifs bridged through μ2-OH and pyridazine-3,6-dicarboxylate

Inorganic Chemistry Communications

Volumn 14, Issue 2, 2011, Pages 429-432

  Henry, Natacha ^a   Lagrenée, Michel ^a   Loiseau, Thierry ^a   Clavier, Nicolas ^b   Dacheux, Nicolas ^b   Abraham, Francis ^a  

^a UNITÉ DE CATALYSE ET DE CHIMIE DU SOLIDE   (France)

^b DIF   (France)

Author keywords

Infrared; Luminescence; Pyridazine 3,6 dicarboxylate; Raman; Single crystal; Uranyl; X ray diffraction

Indexed keywords

EID: 79551469643     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.12.019     Document Type: Article

References (48)

1. P.C. Burns Can. Mineral. 43 2005 1839
2. G. Férey Chem. Soc. Rev. 37 2008 191
3. O.M. Yaghi, M. O'Keeffe, N.W. Ockwig, H.K. Chae, M. Eddaoudi, and J. Kim Nature 423 2003 705
4. S. Kitagawa, R. Kitaura, and S.-I. Noro Angew. Chem. Int. Ed. 43 2004 2334
5. A.K. Cheetham, C.N.R. Rao, and R.K. Feller Chem. Commun. 2006 4780
6. A. Immirzi, G. Bombieri, S. Degetto, and G. Marangoni Acta Cryst. B. 31 1975 1023
7. B. Masci, and P. Thuéry Polyhedron 24 2005 229
8. J.M. Harrowfield, N. Lugan, G.H. Shahverdizadeh, A.A. Soudi, and P. Thuéry Eur. J. Inorg. Chem. 2006 389
9. B. Masci, and P. Thuéry CrystEngComm 10 2008 1082
10. P. Thuéry Acta Cryst. C. 64 2008 m50
11. B. Masci, and P. Thuéry Cryst. Growth Des. 8 2008 1689
12. M. Frisch, and C.L. Cahill Dalton Trans. 2006 4679
13. N.E. Dean, R.D. Hancock, C.L. Cahill, and M. Frisch Inorg. Chem. 47 2008 2000
14. Y.-Z. Zheng, M.-L. Tong, and X.-M. Chen Eur. J. Inorg. Chem. 2005 4109
15. Y.-S. Jiang, G.-H. Li, Y. Tian, Z.-L. Liao, and J.-S. Chen Inorg. Chem. Commun. 9 2006 595
16. J.-Y. Kim, A.J. Norquist, and D. O'Hare Chem. Mater. 15 2003 1970
17. Y.-S. Jiang, Z.-T. Yu, Z.-L. Liao, G.-H. Li, and J.-S. Chen Polyhedron 25 2006 1359
18. C.L. Cahill, D.T. de Lill, and M. Frisch CrystEngComm 9 2007 15
19. S. Sueur, M. Lagrenée, F. Abraham, and C. Bremard J. Heterocycl. Chem. 24 1987 1285
20. A. Escuer, R. Vicente, B. Mernari, A. El Gueddi, and M. Pierrot Inorg. Chem. 36 1997 2511
21. S. Sobanska, M. Lagrenée, J.-P. Wignacourt, and E.M. Holt Acta Cryst. C. 55 1999 553
22. S. Sobanska, J.-P. Wignacourt, P. Conflant, M. Drache, M. Lagrenée, and E.M. Holt New J. Chem. 23 1999 393
23. M. Gryz, W. Starosta, and J. Leciejewicz Acta Cryst. E. 62 2006 m3470
24. W.-W. Sun, A.-L. Cheng, Q.-X. Jia, and E.-Q. Gao Inorg. Chem. 46 2007 5471
25. W.-W. Sun, Q. Yue, A.-L. Cheng, and E.-Q. Gao CrystEngComm 10 2008 1384
26. N. Henry, S. Costenoble, M. Lagrenée, T. Loiseau, and F. Abraham CrystEngComm 10 2011 251
27. J. Leciejewicz, and W. Starosta Acta Cryst. E. 65 2009 m94
28. 2O (0.6 mmol) was dissolved in 25 ml deionized hot water with 0.1 g sodium pyridazine-3,6-dicarboxylate (0.6 mmol) and then left at room temperature. After one week, well formed pale yellow single crystals appeared in the mother liquid and dried in air.
29. 3. The crystal structure measurement was performed on an X8 Bruker diffractometer (Apex 2 area detector) using a graphite monochromated MoKα radiation. The Intensities were integrated from the collected frames and corrected for background, Lorentz and polarization effects, using SAINT [Bruker Analytical X-ray system, "SAINT+, Version 7.12", Madison USA (2004)] and for crystal/detector area absorption from the SADABS software [Scheldrick G.M., SADABS, Bruker-Siemens Area Detector Absorption and Other Correction, Version 2006/1, Göttingen Germany (2006).]. The lattice parameters were refined from the complete data set. The structure was solved primarily by direct method and second by Fourier difference techniques [G. M. Sheldrick, SHELXS 97, Program for the Solution of Crystal Structures, University of Göttingen, Germany, 1997]. The structure refinement was performed with the SHELXL-97 software [G. M. Sheldrick, SHELXL 97, Program for the Refinement of Crystal Structures, University of Göttingen, Germany, 1997] by the full-matrix least-squares method. All non-hydrogen atoms positions were anisotropically refined. Hydrogen atoms of the benzene ring were included in calculated positions and allowed to ride on their parent atoms.
30. P.C. Burns, R.C. Ewing, and F.C. Hawthorne Can. Mineral. 35 1997 1551
31. M.Y. Artem'eva, Y.N. Mikhailov, Y.E. Gorbunova, L.B. Serezhkina, and V.N. Serezhkin Russ. J. Inorg. Chem. 48 2003 1337
32. L. Duvieubourg, G. Nowogrocki, F. Abraham, and S. Grandjean J. Solid State Chem. 178 2005 3437
33. J.C. Berthet, M. Nierlich, and M. Ephritikhine Chem. Commun. 2003 1660
34. J.C. Berthet, M. Nierlich, and M. Ephritikhine Dalton Trans. 2004 2814
35. N.W. Alcock, D.J. Flanders, and D. Brown J. Chem. Soc. Dalton Trans. 1985 1001
36. E. Rabinowitch, and R.L. Belford Spectroscopy and Photophysics of Uranyl Compounds 1964 Pergamon Press Oxford
37. J.T. Bell, and R.E. Biggers J. Mol. Spectrosc. 25 1965 312
38. A. Brachmann, G. Geipel, G. Bernhard, and H. Nitsche Radiochim. Acta 90 2002 147
39. L.A. Borkowski, and C.L. Cahill Cryst. Growth Des. 6 2006 2241
40. L.A. Borkowski, and C.L. Cahill Cryst. Growth Des. 6 2006 2248
41. S.S. Bukalov, V.M. Vdovenko, I.N. Ladygin, and D.N. Suglobov J. Appl. Spectros. 12 1970 263
42. J.R. Bartlett, and R.P. Cooney J. Mol. Struct. 193 1989 295
43. L.H. Jones Spectrochim. Acta 15 1959 409
44. Y. Ozono, Y. Nibu, H. Shimada, and R. Shimada Bull. Chem. Soc. Jpn 59 1986 2997
45. F. Billes, H. Mikosch, and S. Holly THEOCHEM 423 1998 225
46. A.D. Boese, and J.M.L. Martin J. Phys. Chem. A 108 2004 3085
47. S. Breda, I.D. Reva, L. Lapinski, M.J. Nowak, and R. Fausto J. Mol. Struct. 786 2006 193
48. K. Nakammoto Infrared and Raman Spectra of Inorganic and Coordination Compounds 2009 John Wiley & Sons Eds Hoboken, New Jersey