Inter-laboratory comparison of an analytical method for the determination of the feed additive semduramicin in poultry feed at authorised level by liquid chromatography single quadrupole mass spectrometry

Food Additives and Contaminants - Part A

Volumn 28, Issue 1, 2011, Pages 35-43

  de la Huebra, M J González ^a   Vincent, U ^a   von Holst, C ^a  

^a JOINT RESEARCH CENTRE   (Italy)

Author keywords

Additives general; Animal feedingstuffs; Feeding; Inter laboratory validation; Liquid chromatography; Mass spectrometry

Indexed keywords

ADDITIVES; FEEDING; LABORATORIES; MASS SPECTROMETRY;

ADDITIVES GENERALS; ADMINISTRATIVE PROCEDURES; ANIMAL FEEDINGSTUFFS; INTER-LABORATORY VALIDATIONS; INTERLABORATORY COMPARISON; PERFORMANCE CHARACTERISTICS; RELATIVE STANDARD DEVIATIONS; SINGLE QUADRUPOLE MASS SPECTROMETRY;

LIQUID CHROMATOGRAPHY;

FOOD ADDITIVE; SEMDURAMICIN; UNCLASSIFIED DRUG;

ANIMAL FOOD; ARTICLE; INTER LABORATORY VALIDATION; LIQUID CHROMATOGRAPHY SINGLE QUADRUPOLE MASS SPECTROMETRY; MASS SPECTROMETRY; POULTRY FEED; PRIORITY JOURNAL; VALIDATION STUDY;

ANIMALIA;

EID: 78751555140     PISSN: 19440049     EISSN: 14645122     Source Type: Journal    
DOI: 10.1080/19440049.2010.538727     Document Type: Article

References (12)

1. AOAC Official Methods of Analysis. 2002. Guidelines for collaborative study procedures to validate characteristics of a method of analysis [Internet]. AOAC Official Methods of Analysis (2002) Appendix D 1-12. Available from: http://www.aoac.org/Official_Methods/Collaborative_Study_Validation_Guidelines.pdf/.
2. Comité Européen de Normalisation (CEN). 2010. CEN prEN 16158. Animal feeding stuffs - determination of semduramicin content - liquid chromatographic method using a tree analytical approach. Brussels (Belgium): CEN; ICS 65.120.
3. European Commission. 2002. Commission Decision 2002/ 657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Comm. L 221:8-36.
4. European Commission. 2009. Commission Directive 2009/8/ EC. Off J Eur Union L 40:19-25.
5. European Communities. 2004. Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 on official controls performed to ensure the verificationof compliance with feed and food law, animal health and animal welfare rules. Off J Eur Union L 165:1-141.
6. European Union. 2006. Commission Regulation (EC) No. 1443/2006 of 29 September 2006 concerning the permanent authorisations of certain additives in feedingstuffs and an authorisation for 10 years for a coccidiostat. Off J Eur Union L 271:12-18.
7. González de la Huebra MJ, Vincent U, von Holst C. 2010. Determination of semduramicin in poultry feed at authorized level by liquid chromatography single quadrupole mass spectrometry. J Pharm Biomed Anal. 53:860-886.
8. Horwitz W. 1995. Protocol for the design, conduct and interpretation of method-performance studies. Pure Appl Chem. 67:331-343.
9. Horwitz W, Albert R. 2006. The Horwitz ratio (HORRAT): a useful index of method performance with respect to precision. J AOAC Int. 89:1095-1109.
10. Horwitz W, Kamps LR, Boyer KW. 1980. Quality assurance in the analysis of foods and trace constituents. J Assoc Off Anal Chem. 63:1344-1354.
11. International Organization for Standardization (ISO). 1994. ISO 5725. Accuracy (trueness and precision) of measurement methods and results. Geneva (Switzerland): ISO; Standards, ICS 03.120.30.
12. Thompson M, Wood R. 1993. The International Harmonised Protocol for the proficiency testing of (chemical) analytical laboratories. Pure Appl Chem. 65:2123-2144.