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78651328209
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note
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10] (262 mg, 0.64 mmol) in acetone (2 ml) was stirred overnight in inert atmosphere. The solvent was removed in vacuo. The residue was extracted with petroleum ether. After evaporation of the solvent, complex 1 was obtained as a yellow crystalline solid. Yield 243 mg (96%). For spectral data see Ref. 6.
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35
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78651295573
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note
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2NRh (%): C, 14.97; H, 3.59; N, 2.49; B, 15.40.
-
-
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36
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78651267834
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note
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2 (%): C, 15.53; H, 3.72; N, 2.59; B, 16.97.
-
-
-
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37
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78651332880
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note
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17NRh (%): C, 24.56; H, 7.10; N, 3.18; B, 41.77.
-
-
-
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38
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78651332016
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note
-
eq(C) are the equivalent thermal parameters of the atoms to which the corresponding H atoms are bound. All calculations were performed using the SHELXTL software: G. M. Sheldrick, SHELXTL, Version 5.10, Bruker AXS Inc., Madison, WI, USA, 1998.
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Štíbr, B.6
Kudinov, A.R.7
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