Evaluation of QuEChERS, cartridge SPE cleanup, and gas chromatography time-of-flight mass spectrometry for the analysis of pesticides in dietary supplements

LCGC North America

Volumn 28, Issue 11, 2010, Pages 972-977

  Kowalski, Julie ^a   Misselwitz, Michelle ^a   Thomas, Jason ^a   Cochran, Jack ^a  

^a RESTEK CORPORATION   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 78651311335     PISSN: 15275949     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (8)

1. US Food and Drug Administration, Current Good Manufacturing Practice in Manufacturing, Packaging, Labeling, or Holding Operations for Dietary Supplements, Docket No. 1996N-0417 (formerly No. 96N-0417), CFSAN 200441(2007) 34752.
2. US Food and Drug Administration, Pesticide Analytical Manual, Volume I: Multiresidue Methods, 3rd ed. 1994.
3. M. Anastassiades, S. J. Lehotay, D. Stajnbaher, and F. J. Schenck, J. AOAC Int. 86, 412(2003).
4. J. W. Wong, M. S. Wirtz, M. K. Hennessy, F. J. Schenck, A. J. Krynitsky, and S. G. Capar, Acta Hort. (ISHS) 720, 113-128 (2006).
5. J. W. Wong, M. K. Hennessy, D. G. Hayward, A. J. Krynitsky, I. Cassias, and F. J. Schenck, J. Agric. Food Chem. 55, 1117-1128 (2007).
6. D. G. Hayward and J. W. Wong Anal. Chem. 81, 5716-5723 (2009).
7. Foods of Plant Origin - Determination of Pesticide Residues Using GC-MS and/or LC-MS/MS Following Acetonitrile Extraction/Partitioning and Cleanup by Dispersive SPE (QuEChERS-method). (EN 15662 Version 2008.)
8. M. Okihashi, Y. Kitagawa, K. Akutsu, H. Obana, and Y. Tanaka, J. Pestic. Sci. 30, 368-377 (2005).