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78651277143
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note
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-1) 3631(br), 3419(w), 3334(w), 3087(w), 1622(vs), 1359(vs), 1076(w), 823(w), 726(m), 557(w), 444(w).
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32
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78651332361
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note
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-1, GOF = 1.047, R1 = 0.0246, wR2 = 0.0663 [I > 2σ(I)]. Absorption correction: SADABS (Tmin / Tmax = 0.7468 / 0.6791). X-ray data collection was carried out using a Bruker APEX II diffractometer with a CCD area detector. The structure was solved by direct methods and refined with the full-matrix least-squares technique using the SHELXS-97 and SHELXL-97 programs. All non-hydrogen atoms were treated anisotropically. C-bound H atoms of the ligands were placed geometrically refined as riding atoms.
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