Essential oils and volatiles: Sample preparation and analysis. A review

Flavour and Fragrance Journal

Volumn 25, Issue 5, 2010, Pages 282-290

  Rubiolo, P ^a   Sgorbini, B ^a   Liberto, E ^a   Cordero, C ^a   Bicchi, C ^a  

^a UNIVERSITY OF TURIN   (Italy)

Author keywords

Essential oils; Qualitative analysis; Quantitative analysis; Sample preparation; Volatile fraction

Indexed keywords

ENANTIOSELECTIVE; FAST GC; HEADSPACE SAMPLING; HYDRODISTILLATIONS; ISOTOPIC RATIOS; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; SAMPLE PREPARATION; STATE OF THE ART; STEAM DISTILLATION; VEGETABLE MATRICES; VOLATILE FRACTIONS;

DISTILLATION; ESSENTIAL OILS; MASS SPECTROMETRY; SAMPLING;

QUALITY CONTROL;

ESSENTIAL OIL; VOLATILE AGENT;

ANALYTIC METHOD; DISTILLATION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; REVIEW;

EID: 78650674359     PISSN: 08825734     EISSN: 10991026     Source Type: Journal    
DOI: 10.1002/ffj.1984     Document Type: Review

References (79)

1. Association francaise de normalisation AFNOR NF T 75006 Feb 1998 www.afnor.org.
2. European Pharmacopoeia, 6th edn. EDQM (Council of Europe), Strasbourg, France, 2008.
3. B. Kolb, L. Ettre. Static Headspace Gas Chromatography: Theory and Practice. Wiley-VCH: New York, 1997.
4. J. F. Clevenger. J. Am Pharm Assoc. 1928, 17, 346.
5. J. F. Clevenger. Assoc. Off. Agricult. Chem. J. 1928, 17, 346.
6. C. Bicchi, C. Cordero, P. Rubiolo. J. Chromatogr. Sci. 2004, 42, 402.
7. C. Bicchi, C. Cordero, E. Liberto, B. Sgorbini, P. Rubiolo. Headspace sampling of the volatile fraction of vegetable matrices. J. Chromatogr. A. 2008, 1184, 220.
8. Z. Zhang, J. Pawliszyn. Anal. Chem. 1993, 65, 1843.
9. M. E. McComb, R. D. Oleschuk, E. Giller, H. D. Gesser. Talanta 1997, 44, 2137.
10. F. Musshoff, D.W. Lachenmeier, L. Kroener, B.Madea. J. Chromatogr. A. 2002, 958, 231.
11. C. Bicchi, C. Cordero, E. Liberto, P. Rubiolo, B. Sgorbini. J. Chromatogr. A. 2004, 1024, 217.
12. C. Bicchi, C. Cordero, C. Iori, P. Rubiolo, P. Sandra. J. High Resolut. Chromatogr. 2000, 23, 539.
13. B. Tienpont, F. David, C. Bicchi, P. Sandra. J. Microcol. Sep. 2000, 12, 577.
14. M. Ishikawa, O. Ito, S. Ishizaki, Y. Kurobayashi, A. Fujita. Flavour Fragr. J. 2004, 19, 183.
15. A. L. Theis, A. J. Waldack, S. M. Hansen, M. A. Jeannot. Anal. Chem. 2001, 73, 5651.
16. A. Tankeviciute, R. Kazlauskas, V. Vickackaite. Analyst 2001, 126, 1674.
17. A. Segal, T. Gorecki, P. Mussche, J. Lips, J. Pawliszyn. J. Chromatogr. A. 2000, 873, 13.
18. I. Bruheim, X. Liu, J. Pawliszyn. Anal. Chem. 2003, 75, 1002.
19. C. Bicchi, C. Cordero, E. Liberto, P. Rubiolo, B. Sgorbini, P. Sandra. J. Chromatogr. A. 2007, 1148, 137.
20. C. Bicchi, F. Belliardo, C. Cordero, E. Liberto, P. Rubiolo, B. Sgorbini. J. Chromatogr. Sci. 2006, 44, 416.
21. D. Joulain. In Bioactive Volatile Compounds from Plants. American Chemical Society: Washington, DC, 1993, 187.
22. M. Ishikawa, T. Honda, A. Fujita, Y. Kurobayashi, T. Kitahara. Biosci. Biotechnol. Biochem. 2004, 68, 454.
23. www.iofi.org.
24. http://www3.interscience.wiley.com/journal/4029/home/ForAuthors.html.
25. http://pubs.acs.org/page/jafcau/submission/authors.html.
26. W. Herres. HRGC-FTIR: Capillary Gas Chromatography-Fourier Transform Infrared Spectroscopy. Theory and Applications. Huethig: Heidelberg, Germany, 1987.
27. C. A. Cramers, H. G. Janssen, M. M. Van Deursen, P. A. Leclercq. J. Chromatogr. A. 1999, 856, 315.
28. F. David, D. R. Gere, F. Scanlan, P. Sandra. J. Chromatogr. A. 1999, 842, 309.
29. C. Bicchi, C. Brunelli, M. Galli, A. Sironi. J. Chromatogr. A. 2001, 931, 129, and references cited therein.
30. M. Proot, P. Sandra. J. High Res. Chromatogr. 1986, 9, 618.
31. L. M. Blumberg, M. S. Klee. In Proceedings of the 20th International Symposium of Capillary Chromatography, P. Sandra, A. J. Rackstaw (eds), Riva del Garda, Italy, 1998, and references cited therein.
32. P. Magni, R. Facchetti, D. Cavagnino, S. Trestianu. In Proceedings of the 25th International Symposium of Capillary Chromatography, P. Sandra (ed.), Riva del Garda, Italy, 2002, and references cited therein.
33. C. Bicchi, C. Brunelli, C. Cordero, P. Rubiolo, M. Galli, A. Sironi. J. Chromatogr. A. 2004, 1024, 195.
34. Agilent website: http://www.chem.agilent.com.
35. K. Maštovská, S. J. Lehotay. J. Chromatogr. A. 2003, 1000, 153, and references cited therein.
36. P. Rubiolo, E. Liberto, B. Sgorbini, R. Russo, J. L. Veuthey, C. Bicchi. J. Sep. Sci. 2008, 31, 1074.
37. C. Bicchi, E. Liberto, C. Cagliero, C. Cordero, B. Sgorbini, P. Rubiolo. J. Chromatogr. A. 2008, 1212, 114.
38. E. Kováts. Helv. Chim. Acta. 1958, 41, 1915.
39. H. Van den Dool, P. D. Kratz. J. Chromatogr. 1963, 11, 463.
40. L. Mondello, P. Dugo, A. Basile, G. Dugo, K. Bartle. J. Microcol. Sep. 1995, 7, 581.
41. R. Shellie, P.Marriott, G. Zappia, L.Mondello, G. Dugo. J. Essent. Oil Res. 2003, 15, 305.
42. FFNSC MS Library ver. 1.3, Chromaleont, Messina, Italy.
43. R. P. Adams. Identification of Essential Oil Components by Gas Chromatography/Mass Spectrometry. Allured: Carol Stream, IL, 2007.
44. NIST 05-NIST/EPA/NIH Mass Spectral Library. National Institute of Standards and Technology: Gaithersburg, MD.
45. AMDIS, ver. 2.65, 2007: http://chemdata.nist.gov/mass-spc/amdis/.
46. A. Van Asten. Trac-Trends Anal. Chem. 2002, 21, 698.
47. R Costa, M. De Fina,M. R. Valentino, P. Dugo, L.Mondello. Nat. Product Commun. 2007, 2, 413.
48. L. M. Blumberg, M. S. Klee. Anal. Chem. 1998, 70, 3828.
49. Flavors RTL Databases for GC-FID and GC-MS, Agilent Technologies, Santa Clara, USA, 2004.
50. D. Sybilska, T. Koscielski. J. Chromatogr. 1983, 261, 357.
51. Z. Juvancz, G. Alexander, J. Szejtli. J. High Res. Chromatogr. 1987, 10, 105.
52. V. Schurig, H. P. Nowotny. J. Chromatogr. 1988, 441, 155.
53. H. P. Nowotny, D. Schmalzing, D. Wistuba, V. Schurig. J. High Res. Chromatogr. 1989, 12, 383.
54. C. Bicchi, V. Manzin, A. D'Amato, P. Rubiolo. Flavour Fragr. J. 1995, 10, 127.
55. C. Bicchi, A. D'Amato, V. Manzin. In Flavours and Fragrances, K. Swift (ed.), Royal Society of Chemistry: Cambridge, 1997, 57.
56. C. Bicchi, A. D'Amato, P. Rubiolo. J. Chromatogr. A. 1999, 843, 99.
57. W. A. König, D. H. Hochmuth. J. Chromatogr. Sci. 2004, 42, 423.
58. M. Jung, D. Schmalzing, V. Schurig. J. Chromatogr. 1991, 552, 43.
59. V. Schurig, H. P. Nowotny. Angew. Chem. Int. Ed. Engl. 1990, 29, 939.
60. C. Bicchi, G. Artuffo, A. D'Amato, A. Galli, M. Galli. J. High Resolut. Chromatogr. 1991, 14, 301.
61. G. Schomburg, H. Husmann, E. Hübinger, W. A. König. J. High Res. Chromatogr. 1984, 7, 404.
62. A. Bernreuther, N. Christoph, P. Schreier. J. Chromatogr. 1989, 481, 363.
63. A.Mosandl, U. Hener, U. Hagenauer-Hener, A. Kustermann. J. High Res. Chromatogr. 1989, 12, 532.
64. L.Mondello,M. Catalfamo, G. Dugo, P. Dugo. J. Chromatogr. Sci. 1998, 36, 201.
65. R. Shellie, P. Marriott. Anal. Chem. 2002, 74, 5426.
66. R. Shellie, L. Mondello, G. Dugo, P. Marriot. Flavour Fragr. J. 2004, 19, 582.
67. E. Liberto, C. Cagliero, B. Sgorbini, C. Bicchi, D. Sciarrone, B. D'Acampora Zellner, L. Mondello, P. Rubiolo. J. Chromatogr. A. 2008, 1195, 117.
68. J. C. Giddings. J. High Res. Chromatogr. 1987, 10, 319.
69. D. R. Deans. Chromatographia 1968, 1, 18.
70. G. Schomburg, F.Weeke, F. Müller, M. Oréans. Chromatographia 1982, 16, 87.
71. Z. Liu, J. B. Phillips. J. Chromatogr. Sci. 1991, 29, 227.
72. A. Mosandl. Food Rev. Int. 1995, 7, 597.
73. C. Bicchi, E. Liberto, M. Matteodo, B. Sgorbini, L. Mondello, B. d'Acampora Zellner, R. Costa, P. Rubiolo. Flavour Fragr. J. 2008, 23, 382.
74. R. G. Brereton. Applied Chemometrics for Scientists. Wiley: Chichester, UK, 2007, Chapter 5.
75. H. Van den Dool. PhD Thesis, Groningen, The Netherlands, 1974.
76. R. Costa, B. d'Acampora Zellner, M. L. Crupi, M. R. De Fina, M. R. Valentino, P. Dugo, G. Dugo, L. Mondello. Flavour Fragr. J. 2008, 23, 40.
77. Eurachem Guide. The Fitness for Purpose of Analytical Methods. A Laboratory Guide to Method Validation and Related Topics, 1st internet English edn. Eurachem: http://www.eurachem.org/guides/valid.pdf, 1998.
78. EURACHEM website: http://www.eurachem.org/guides/Citac%20Eurachem%20guide.pdf.
79. V. Gold, K. L. Loening, A. D. McNaught. Compendium of Chemical Terminology; IUPAC Recommendations. Blackwell Scientific: Oxford, UK, 1987.