Simultaneous determination of nine flavonoids in Polygonum hydropiper L. samples using nanomagnetic powder three-phase hollow fibre-based liquid-phase microextraction combined with ultrahigh performance liquid chromatography-mass spectrometry

Journal of Pharmaceutical and Biomedical Analysis

Volumn 54, Issue 2, 2011, Pages 311-316

  Yang, Xian ^a   Wang, Bo Chu ^a   Zhang, Xue ^b   Yang, Shui Ping ^c   Li, Wei ^a   Tang, Qian ^a   Singh, Gurinder K ^a  

^a CHONGQING UNIVERSITY   (China)

^b CHONGQING ACADEMY OF CHINESE MATERIA MEDICA   (China)

^c SOUTHWEST UNIVERSITY   (China)

Author keywords

Nanomagnetic powder; Polygonum hydropiper L.; Three phase HF LPME; UPLC MS

Indexed keywords

ACETIC ACID ETHYL ESTER; CATECHIN; EPICATECHIN; FLAVONOID; HYPERIN; ISOQUERCITRIN; ISORHAMNETIN; KAEMPFEROL; QUERCETIN; QUERCITRIN; RUTOSIDE;

ACCURACY; AQUEOUS SOLUTION; ARTICLE; CALIBRATION; CORRELATION COEFFICIENT; DRUG DETERMINATION; DRUG STRUCTURE; ELECTROSPRAY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HOLLOW FIBER; LIQUID CHROMATOGRAPHY; LIQUID PHASE MICROEXTRACTION; MASS SPECTROMETRY; MEDICINAL PLANT; NONHUMAN; PHYSICAL CHEMISTRY; POLYGONUM; POLYGONUM EXTRACT; PRIORITY JOURNAL; QUALITY CONTROL; ULTRAHIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

CALIBRATION; CHEMICAL FRACTIONATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FLAVONOIDS; HYDROGEN-ION CONCENTRATION; LIMIT OF DETECTION; MASS SPECTROMETRY; MOLECULAR STRUCTURE; POLYGONUM; POWDERS; QUALITY CONTROL; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLVENTS; WATER;

EID: 78650191612     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2010.08.026     Document Type: Article

References (23)

1. Peng Z.F., Strack D., Baumert A., Subramaniam R., Goh N.K., Chia T.F., Tan S.N., Chia L.S. Antioxidant flavonoids from leaves of Polygonum hydropiper L. Phytochemistry 2003, 62:219-228.
2. Haginaka J. Protein-based chiral stationary phases for high-performance liquid chromatography enantioseparations. J. Chromatogr. A 2001, 906:253-273.
3. Sanchez-Gallego J.I., Lopez-Revuelta A., Sardina J.L., Hernandez-Hernandez A., Sanchez-Yague J., Llanillo M. Membrane cholesterol contents modify the protective effects of Quercetin and Rutin on integrity and cellular viability in oxidized erythrocytes. Free Radic. Biol. Med. 2010, 48:1444-1454.
4. Iacopini P., Baldi M., Storchi P., Sebastiani L. Catechin, epicatechin, quercetin, rutin and resveratrol in red grape: content, in vitro antioxidant activity and interactions. J. Food Compost. Anal. 2008, 21:589-598.
5. Arthur C.L, Killam L.M., Buchholz K.D., Pawliszyn J., Berg J.R. Automation and optimization of solid-phase microextraction. Anal. Chem. 1992, 64:1960-1966.
6. Pena-Pereira F., Lavilla I., Bendicho C. Miniaturized preconcentration methods based on liquid-liquid extraction and their application in inorganic ultratrace analysis and speciation: a review. Spectrochim. Acta B 2009, 64:1-15.
7. Chen P.S., Huang S.D. Coupled two-step microextraction devices with derivatizations to identify hydroxycarbonyls in rain samples by gas chromatography-mass spectrometry. J. Chromatogr. A 2006, 1118:161-167.
8. Xia L.B., Wu Y., Hu B.L. Hollow-fiber liquid-phase microextraction prior to low-temperature electrothermal vaporization ICP-MS for trace element analysis in environmental and biological samples. J. Mass Spectrom. 2007, 42:803-810.
9. Sobhi H.R., Yamini Y., Abadi R.H.H.B. Extraction and determination of trace amounts of chlorpromazine in biological fluids using hollow fiber liquid phase microextraction followed by high-performance liquid chromatography. J. Pharm. Biomed. Anal. 2007, 45:769-774.
10. Payán M.R., López M.Á.B., Fernández-Torres R., Bernal J.L.P., Mochón M.C. HPLC determination of ibuprofen, diclofenac and salicylic acid using hollow fiber-based liquid phase microextraction (HF-LPME). Anal. Chim. Acta 2009, 653:184-190.
11. Ye G., Li Y.Z., Li Y.Y., Guo H.Z., Guo D.A. SPE-HPLC method for the determination and pharmacokinetic studies on paeoniflorin in rat serum after oral administration of traditional Chinese medicinal preparation Guan-Xin-Er-Hao decoction. J. Pharm. Biomed. Anal. 2003, 33:521-527.
12. Poole C.F. New trends in solid-phase extraction. Trends Anal. Chem. 2003, 22:362-373.
13. Esrafili A., Yamini Y., Shariati S. Hollow fiber-based liquid phase microextraction combined with high-performance liquid chromatography for extraction and determination of some antidepressant drugs in biological fluids. Anal. Chim. Acta 2007, 604:127-133.
14. Ouyang G.F., Zhao W.N., Pawliszyn J. Automation and optimization of liquid-phase microextraction by gas chromatography. J. Chromatogr. A 2007, 1138:47-54.
15. Gjelstad A., Andersen T.M., Rasmussen K.E., Pedersen-Bjergaard S. Microextraction across supported liquid membranes forced by pH gradients and electrical fields. J. Chromatogr. A 2007, 1157:38-45.
16. Duan J.K., Hu B. Separation and determination of seleno amino acids using gas chromatography hyphenated with inductively coupled plasma mass spectrometry after hollow fiber liquid phase microextraction. J. Mass Spectrom. 2009, 44:605-612.
17. Yang C.L., Guo L.Y., Liu X.Y., Zhang H.X., Liu M.C. Determination of tetrandrine and fangchinoline in plasma samples using hollow fiber liquid-phase microextraction combined with high-performance liquid chromatography. J. Chromatogr. A 2007, 1164:56-64.
18. Yazdi A.S., Es'haghi Z. Surfactant enhanced liquid-phase microextraction of basic drugs of abuse in hair combined with high performance liquid chromatography. J. Chromatogr. A 2005, 1094:1-8.
19. Aguirre-Hernández E., González-Trujano M., Martínez A.L., Moreno J., Kite G., Terrazas T., Soto-Hernándezb M. HPLC/MS analysis and anxiolytic-like effect of quercetin and kaempferol flavonoids from Tilia americana var. mexicana. J. Ethnopharmacol. 2010, 127:91-97.
20. Yang R.Z., Wei X.L., Gao F.F., Wang L.S., Zhang H.J., Xu Y.J., Li C.H., Ge Y.X., Zhang J.J., Zhang J. Simultaneous analysis of anthocyanins and flavonols in petals of lotus (Nelumbo) cultivars by high-performance liquid chromatography-photodiode array detection/electrospray ionization mass spectrometry. J. Chromatogr. A 2009, 1216:2063-2070.
21. Wang Y.L., Qiao X.N., Li W.C., Zhou Y.H., Jiao Y., Yang C., Dong C., Inoue Y., Shuang S.M. Study on the complexation of isoquercitrin with β-cyclodextrin and its derivatives by spectroscopy. Anal. Chim. Acta 2009, 650:124-130.
22. Liu A.L., Zhang S.B., Chen W., Huang L.Y., Lin X.H., Xia X.H. Study of the electrochemical behavior of isorhamnetin on a glassy carbon electrode and its application. Talanta 2008, 77:314-318.
23. Koh E., Wimalasiri K.M.S., Chassy A.W., Mitchell A.E. Content of ascorbic acid, quercetin, kaempferol and total phenolics in commercial broccoli. J. Food Compost. Anal. 2009, 22:637-643.