Simultaneous determination of pyrimethamine, sulfadoxine, mefloquine, and ibuprofen in pharmaceutical formulations by RP-HPLC

Medicinal Chemistry Research

Volumn 19, Issue 9, 2010, Pages 1043-1054

  Arayne, M Saeed ^a   Sultana, Najma ^a   Siddiqui, Farhan Ahmed ^a   Naseem, Sajida ^a   Qureshi, Faiza ^a  

^a UNIVERSITY OF KARACHI   (Pakistan)

Author keywords

Antimalarials; Ibuprofen; Mefloquine; NSAIDs; Pyrimethamine; RP HPLC; Sulfadoxine; UV detection

Indexed keywords

ACETONITRILE; DOLOFEN; FANSIMEF; IBUPROFEN; MEFLOQUINE; PHOSPHORIC ACID; PYRIMETHAMINE; SULFADOXINE; UNCLASSIFIED DRUG; WATER;

ACCURACY; ARTICLE; CONCENTRATION RESPONSE; DRUG DETERMINATION; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ROOM TEMPERATURE; SEPARATION TECHNIQUE; TABLET FORMULATION; ULTRAVIOLET RADIATION;

EID: 78650173784     PISSN: 10542523     EISSN: None     Source Type: Journal    
DOI: 10.1007/s00044-009-9250-4     Document Type: Article

References (50)

1. J Appelgate 1983 Clinical pharmacology of sulfonamides Mod Vet Pract 64 667 669
2. H Astier C Renard V Cheminel O Soares C Mounier F Peyron JF Chaulet 1997 Simultaneous determination of pyrimethamine and sulphadoxine in human plasma by high-performance liquid chromatography after automated liquid-solid extraction J Chromatogr B Biomed Sci Appl 698 1-2 217 223 1:CAS:528:DyaK2sXlslemsL4%3D 10.1016/S0378-4347(97)00264-8 9367211 (Pubitemid 27412524)
3. KN Bangchang P Tan-ariya R Ubalee B Kamanikom J Karbwang 1997 Alternative method for determination of pyrimethamine in plasma by high-performance liquid chromatography J Chromatogr B Biomed Sci Appl 689 2 433 437 10.1016/S0378- 4347(96)00327-1 (Pubitemid 27091374)
4. Y Bergqvist U Hellgren FC Churchill 1988 High-performance liquid chromatographic assay for the simultaneous monitoring of mefloquine and its acid metabolite in biological samples using protein precipitation and ion-pair extraction J Chromatogr 432 253 263 1:CAS:528:DyaL1MXjtlagtQ%3D%3D 10.1016/S0378-4347(00)80650-7 3265419
5. Y Bergqvist S Eckerbom H Larsson M Malekzadeh 1991 Reversed-phase liquid chromatographic method for the simultaneous determination of the antimalarial drugs sulfadoxine, pyrimethamine, mefloquine and its major carboxylic metabolite in plasma J Chromatogr 571 1-2 169 177 1:CAS:528:DyaK38XhsFansQ%3D%3D 1810945
6. Y Bergqvist J al Kabbani C Pettersson NH Huynh 1993 Enantioselective high-performance liquid chromatographic determination of (SR)- and (RS)-mefloquine in plasma using N-benzyloxycarbonyl-glycyl-L-proline as chiral counter ion J Chromatogr 620 2 217 224 1:CAS:528:DyaK2cXivV2htLs%3D 10.1016/0378-4347(93)80007-Q 8300789 (Pubitemid 23332751)
7. Y Bergqvist M Doverskog JA Kabbani 1994 High-performance liquid chromatographic determination of (SR)- and (RS)-enantiomers of mefloquine in plasma and capillary blood sampled on paper after derivatization with (-)-1-(9-fluorenyl)ethyl chloroformate J Chromatogr 652 1 73 81 1:CAS:528:DyaK2cXitlGht7g%3D 10.1016/0378-4347(93)E0386-5 8014230 (Pubitemid 24079351)
8. SI Bhoir IC Bhoir AM Bhagwat M Sundaresan 2001 Determination of sulfadoxine in human blood plasma using packed-column supercritical fluid chromatography J Chromatogr B Biomed Sci Appl 757 1 39 47 1:CAS:528: DC%2BD3MXjtFCku78%3D 10.1016/S0378-4347(01)00061-5 11419747 (Pubitemid 32424456)
9. R Bhushan J Martens 1998 Resolution of enantiomers of ibuprofen by liquid chromatography: a review J Biomed Chromatogr 12 6 309 316 1:CAS:528: DyaK1cXnvVKqu7s%3D 10.1002/(SICI)1099-0801(199811/12)12:6<309::AID- BMC763>3.0.CO;2-K (Pubitemid 28542595)
10. PS Bonato MP Del Lama R de Carvalho 2003 Enantioselective determination of ibuprofen in plasma J Chromatogr B Anal Technol Biomed Life Sci 796 2 413 420 1:CAS:528:DC%2BD3sXosVyitrY%3D 10.1016/j.jchromb.2003.08.031 (Pubitemid 37329684)
11. M Bonini F Mokofio S Argilas 1981 Contribution to the determination of four antimalarial molecules (chloroquine, quinine, pyrimethamine, sulfadoxime) mixed in biological fluids. I. Spectrophotometry UV Toxicol Eur Res 3 3 119 123 1:CAS:528:DyaL3MXltVygs7s%3D 7281163
12. British Pharmacopoeia (2003) Stationary Office under license from the controller of Her Majesty's Stationary Office for the Department of Health on behalf of the Health Ministers, London
13. R Canaparo E Muntoni GP Zara C Dellapepa E Berno M Costa M Eandi 2000 Determination of ibuprofen in human plasma by high-performance liquid chromatography: validation and application in pharmacokinetic study Biomed Chromatogr 14 4 219 226 1:CAS:528:DC%2BD3cXkt1arurs%3D 10.1002/1099-0801(200006) 14:4<219::AID-BMC969>3.0.CO;2-Z 10861732 (Pubitemid 30348991)
14. M Castillo PC Smith 1993 Direct determination of ibuprofen and ibuprofen acyl glucuronide in plasma by high-performance liquid chromatography using solid-phase extraction J Chromatogr 614 1 109 116 1:CAS:528:DyaK3sXktVSiurY%3D 10.1016/0378-4347(93)80229-W 8496270 (Pubitemid 23122486)
15. A Ducret M Trani P Pepin R Loriet 1998 Chiral high performance liquid chromatography resolution of ibuprofen esters J Pharm Biomed Anal 16 7 1225 1231 1:CAS:528:DyaK1cXit1egtL8%3D 10.1016/S0731-7085(97)00212-4 9571540 (Pubitemid 28141099)
16. J Eljaschewitsch J Padberg D Scharmann B Ruf 1996 High-performance liquid chromatography determination of pyrimethamine, dapsone, monoacetyldapsone, sulfadoxine, and N-acetyl-sulfadoxine after rapid solid-phase extraction Ther Drug Monit 18 5 592 597 1:CAS:528:DyaK28XmsFWitrw%3D 10.1097/00007691-199610000- 00012 8885125 (Pubitemid 26330482)
17. H Farrar L Letzig M Gill 2002 Validation of a liquid chromatographic method for the determination of ibuprofen in human plasma J Chromatogr B Analyt Technol Biomed Life Sci 780 2 341 348 1:CAS:528:DC%2BD38Xptlans70%3D 10.1016/S1570-0232(02)00543-3 12401360 (Pubitemid 35223570)
18. Florey K (ed) (1985) Analytical profiles of drug substances, vol 14. Academic Press, San diego, p 160
19. AI Gasco-Lopez R Izquierdo-Hornillos A Jimenez 1999 LC method development for ibuprophen and validation in different pharmaceuticals J Pharm Biomed Anal 21 1 143 149 1:CAS:528:DyaK1MXmtVyisbc%3D 10.1016/S0731-7085(99)00127-2 10701921 (Pubitemid 29430150)
20. PS Gong SL Jeng YF Hsu CC Lin SY Lin 2002 Research note: development of a method for the determination of pyrimethamine concentrations in feeds by ion-pairing high-performance liquid chromatography J Food Prot 65 4 688 691 1:CAS:528:DC%2BD38XjsFWhsrk%3D 11952221
21. MD Green Y Bergqvist DL Mount S Corbett MJ D'Souza 1999 Improved validated assay for the determination of mefloquine and its carboxy metabolite in plasma, serum and whole blood using solid-phase extraction and high-performance liquid chromatography J Chromatogr B Biomed Sci Appl 727 159 165 1:CAS:528:DyaK1MXjsVWnsr8%3D 10.1016/S0378-4347(99)00080-8 10360435 (Pubitemid 29189288)
22. SH Kang SY Chang KC Do SC Chi DS Chung 1998 High-performance liquid chromatography with a column-switching system and capillary electrophoresis for the determination of ibuprofen in plasma J Chromatogr B Biomed Sci Appl 712 1-2 153 160 1:CAS:528:DyaK1cXks1Ohtrk%3D 10.1016/S0378-4347(98)00134-0 9698237 (Pubitemid 28322430)
23. J Karbwang P Molunto KN Bangchang D Bunnag 1989 Determination of mefloquine in biological fluids using high performance liquid chromatography Southeast Asian J Trop Med Public Health 20 1 55 60 1:CAS:528:DyaL1MXls1Klurg%3D 2788925 (Pubitemid 19190847)
24. DR Kepp UG Sidelmann J Tjarnelund SH Hansen 1997 Simultaneous quantitative determination of the major phase I and II metabolites of ibuprofen in biological fluids by high-performance liquid chromatography on dynamically modified silica J Chromatogr B Biomed Sci Appl 696 2 235 241 1:CAS:528:DyaK2sXltVCrurs%3D 10.1016/S0378-4347(97)00239-9 9323543 (Pubitemid 27387449)
25. JM Lamant P Kintz A Tracqui P Mangin AA Lugnier AJ Chaumont 1988 Simultaneous determination of mefloquine and chloroquine in biological fluids using high-performance liquid chromatography Ann Biol Clin (Paris) 46 9 722 724 1:STN:280:DyaL1M7jtlWmsA%3D%3D
26. CH Lemko G CaillAc RT Foster 1993 Stereospecific high-performance liquid chromatographic assay of ibuprofen: improved sensitivity and sample processing efficiency J Chromatogr 619 2 330 335 1:CAS:528:DyaK3sXms1Wqsbc%3D 10.1016/0378-4347(93)80126-O 8263108 (Pubitemid 23293695)
27. AL Liboux H Duquesne G Montay D Chassard E Pichard JJ Thebault A Frydman J Gaillot 1991 Pharmacokinetics of pyrimethamine in healthy young volunteers using a new solid phase extraction/HPLC method Eur J Drug Metab Pharmacokinet 3 284 290
28. SY Lin SL Jeng 2002 Comparison of ion-pairing and ion-suppressing liquid chromatographic methods for the determination of pyrimethamine and ormetoprim in chicken feed J Chromatogr Sci 40 6 331 336 1:CAS:528:DC%2BD38XlsVGmtL0%3D 12137205
29. K Makino Y Itoh D Teshima R Oishi 2004 Determination of nonsteroidal anti-inflammatory drugs in human specimens by capillary zone electrophoresis and micellar electrokinetic chromatography Electrophoresis 25 10-11 1488 1495 1:CAS:528:DC%2BD2cXlt1Oiu7k%3D 10.1002/elps.200305870 15188231
30. Martindale W, Westcott W (1996) Martindale: the extra pharmacopoeia, 31st edn. Royal Pharmaceutical Society of Great Britain, London, pp 50-51
31. The Merck Index (2001) An encyclopedia of chemicals, drugs and biologicals, 13th edn. Merck Research Laboratories, Whitehouse Station, p 876
32. Physicians' Desk Reference (2000) 54th ed. Medical Economics, Montvale, p 2648
33. Prescott JF, Baggott JD (1993) Antimicrobial therapy in veterinary medicine, 2nd edn. Iowa State University Press, Ames, pp 19-26
34. Y Qiu S Kitamura JK Guillory 1992 A high-performance liquid chromatographic method for the quantitative enantioselective analysis of mefloquine stereoisomers Pharm Res 9 12 1640 1643 1:CAS:528:DyaK3sXksFKgsrY%3D 10.1023/A:1015832912774 1488410
35. MG Quagila E Donati S Fanali P Catarcini 2003 Ibuprofen quality control by electrochromatography Farmaco 58 9 699 705 10.1016/S0014-827X(03)00097-1 (Pubitemid 37122641)
36. Remington's Pharmaceutical Sciences (1995) 19th edn, vol 2. Mack, Plainview, pp 890-893
37. N Rifai M Sakamoto T Law V Galpchian N Harris AA Colin 1996 Use of a rapid HPLC assay for determination of pharmacokinetic parameters of ibuprofen in patients with cystic fibrosis Clin Chem 42 11 1812 1816 1:CAS:528: DyaK28Xms1ams7o%3D 8906081
38. WL Roberts KM Reynolds R Heimer PI Jatlow PM Rainey 1995 Pyrimethamine analysis by enzyme inhibition and HPLC assays Am J Clin Pathol 104 1 82 88 1:CAS:528:DyaK2MXnsVegu7o%3D 7611189
39. TK Save DV Parmar PV Devarajan 1997 High-performance thin-layer chromatographic determination of ibuprofen in plasma J Chromatogr B Biomed Sci Appl 690 1-2 315 319 1:CAS:528:DyaK2sXhtlyhsr4%3D 10.1016/S0378-4347(96)00326-X 9106058 (Pubitemid 27136484)
40. J Sochor J Klimes M ZahradnAcek J SedlAicek 1984 High-performance liquid chromatographic assay for ibuprofen in whole blood using solid-phase extraction J Chromatogr B Biomed Appl 654 2 282 286 10.1016/0378-4347(94)00018-2
41. J Sochor J Klimes J SedlAicek M ZahradnAcek 1995 Determination of ibuprofen in erythrocytes and plasma by high performance liquid chromatography J Pharm Biomed Anal 13 7 899 903 1:CAS:528:DyaK2MXnsV2gtbk%3D 10.1016/0731-7085(95)01306-6 8562614
42. E Souri H Farsam F Jamali 1997 Stereospecific determination of mefloquine in biological fluids by high-performance liquid chromatography J Chromatogr B Biomed Sci Appl 700 1-2 215 222 1:CAS:528:DyaK2sXntVOgtbk%3D 10.1016/S0378-4347(97)00322-8 9390732 (Pubitemid 27473995)
43. M Spraul M Hofmann P Dvortsak JK Nicholson ID Wilson 1993 High-performance liquid chromatography coupled to high-field proton nuclear magnetic resonance spectroscopy: application to the urinary metabolites of ibuprofen Anal Chem 65 4 327 330 1:CAS:528:DyaK3sXltFOmtw%3D%3D 10.1021/ac00052a004 8382454
44. U Timm E Weidekamm 1982 Determination of pyrimethamine in human plasma after administration of fansidar of fansidar-mefloquine by means of high-performance liquid chromatography with fluorescence detection J Chromatogr 230 1 107 114 1:CAS:528:DyaL38XksV2iu7o%3D 10.1016/S0378-4347(00)81435-8 6980889
45. A Tracqui I Mikail P Kintz P Mangin 1993 Nonfatal prolonged overdosage of pyrimethamine in an infant: measurement of plasma and urine levels using HPLC with diode-array detection J Anal Toxicol 17 4 248 250 1:CAS:528: DyaK3sXlsFWmt78%3D 8371558
46. AM Van Miert 1994 The sulfonamide-diaminopyrimidine story J Vet Pharmacol Ther 17 309 10.1111/j.1365-2885.1994.tb00251.x 7966552
47. B Vermeulen JP Remon 2000 Validation of a high-performance liquid chromatographic method for the determination of ibuprofen enantiomers in plasma of broiler chickens J Chromatogr B Biomed Sci Appl 749 2 241 243 10.1016/S0378-4347(00)00428-X
48. MR Whelan JL Ford MW Powell 2002 Simultaneous determination of ibuprofen and hydroxypropylmethylcellulose (HPMC) using HPLC and evaporative light scattering detection J Pharm Biomed Anal 30 4 1355 1359 1:CAS:528: DC%2BD38Xot1Cjsbk%3D 10.1016/S0731-7085(02)00394-1 12408926 (Pubitemid 35284344)
49. Windholz M (1976) The Merck index, 9th edn. Merck and Co., Rahway, p 1036
50. TH Zytkovicz J Salter L Hennigan R Timperi J Maguire R Hoff 1991 Isocratic reversed-phase HPLC method to measure pyrimethamine extracted from plasma of infants treated for toxoplasmosis Clin Chem 37 7 1281 1283 1:CAS:528:DyaK3MXlsleqt7Y%3D 1855303