Determination of antioxidants in polyolefins using total dissolution methodology followed by RPLC

Journal of Separation Science

Volumn 33, Issue 22, 2010, Pages 3455-3462

  Green, Shayne ^a   Bai, Snow ^a   Cheatham, Mike ^a   Cong, Rongjuan ^a   Yau, Wallace ^a  

^a DOW CHEMICAL COMPANY   (United States)

Author keywords

Antioxidants; Dissolution reprecipitation extraction; Liquid chromatography; Polyethylene; Polypropylene

Indexed keywords

ANALYTICAL METHOD; ANTIOXIDANTS; DIRECT ANALYSIS; DISSOLUTION/REPRECIPITATION EXTRACTION; HIGH-THROUGHPUT; MANUAL LABORS; O-XYLENE; POLYOLEFIN RESINS; PRODUCT LIFETIME; WORK PROCESS;

AROMATIC HYDROCARBONS; DISSOLUTION; FOURIER TRANSFORM INFRARED SPECTROSCOPY; FOURIER TRANSFORMS; LIQUID CHROMATOGRAPHY; LIQUIDS; METHANOL; POLYETHYLENES; RESINS; THERMOFORMING; THERMOPLASTICS; XYLENE;

SOLVENT EXTRACTION;

3 (2,4 DI TERT BUTYLPHENYL)PHOSPHITE; 3 (3,5 DI TERT BUTYL 4 HYDROXYPHENYL)PROPIONIC ACID OCTADECYL ESTER; ANTIOXIDANT; METHANOL; ORTHO XYLENE; PENTAERYTHRITOL TETRA 3 (3,5 DI TERT BUTYL 4 HYDROXYPHENYL)PROPIONATE; PHOSPHITE; POLYETHYLENE; POLYOLEFIN; POLYPROPYLENE; PROPIONIC ACID DERIVATIVE; RESIN; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CALIBRATION; CHEMICAL STRUCTURE; DISSOLUTION; EXTRACTION; PRECIPITATION; PRIORITY JOURNAL; REVERSED PHASE LIQUID CHROMATOGRAPHY;

EID: 78649682818     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201000491     Document Type: Article

References (25)

1. Pfaendner, R., Polym. Degrad. Stab. 2006, 91, 2249-2256.
2. ASTM D6953-03, Standard test method for determination of antioxidants and erucamide slip additives in polyethylene using liquid chromatography (LC), 2003.
3. ASTM D7210-06, Standard practice for extraction of additives in polyolefin plastics, 2006.
4. ASTM D5818-95, Standard test method for determination of phenolic antioxidants and erucamide slip additives in linear low-density polyethylene using liquid chromatography (LC), 1995
5. ASTM D1996-97, Standard test method for determination of phenolic antioxidants and erucamide slip additive in low density polyethylene using liquid chromatography (LC), 2003.
6. Nielson, R. C., J. Liq. Chromatogr. 1993, 16, 1625-1638.
7. Nielson, R. C., J. Liq. Chromatogr. 1991, 14, 503-519.
8. Bart, F. C. J., Polym. Degrad. Stab. 2003, 82, 197-205.
9. Ashton, H. C., Angew. Makromol. Chem. 1998, 261/262, 9-23.
10. Marcato, B., Vianello, M., J. Chromatogr. A, 2000, 869, 285-300.
11. Vandenburg, H. J., Clifford, A. A., Bartle, K. D., Carroll, J. C., Newton, I. D., Analyst 1999, 124, 397-400.
12. Vandenburg, H. J., Clifford, A. A., Bartle, K. D., Carlson, R. E., Carroll, J. C., Newton, I. D., Analyst, 1999, 124, 1707-1710.
13. Vandenburg, H. J., Clifford, A. A., Bartle, K. D., Zhu, S. A., Carroll, J., Newton, I. D., Garden, L. M., Anal. Chem. 1998, 70, 1943.
14. Vandenburg, H. J., Clifford, A. A., Bartle, K. D., Carroll, J., Newton, I., Garden, L. M., Dean, J. R., Costley, C. T., Analyst 1997, 122, 101R.
15. Bartle, K. D., Clifford, A. A., Hawthorne, S. B., Lagenfield, J. J., Miller, D.J., Robinson, R., J. Supercrit. Fluids 1990, 3, 143.
16. Thilen, M., Shishoo, R., J. Appl. Polym. Sci. 2000, 76, 938-946.
17. Thomas, M. P., J. Vinyl Addit. Technol. 1996, 2, 330-338.
18. Ritter, A., Michel, E., Schmid, M., Affolter, S., Polymer Testing, 2005, 24, 498-506.
19. David, F., Sandra, P., LC/GC 1993, 11, 282, 284- 287.
20. David, F., Application note 8, Agilent Technologies, 1991.
21. Duderstadt, R. E., Fischer, S. M., J. Chromatogr. A 2008, 1193, 70-78.
22. Block, C., Wynants, L., Kelchtermans, M., De Boer, R., Compernolle, F., Polym. Degradation Stability 2006, 91, 3163-3173.
23. Wang, C., Luan, W., Woodman, M., Application note 5989-5850EN, Agilent Technologies, 2007.
24. Luan, W., Wang, C., Woodman, M., Application note 5989-5849EN, Agilent Technologies, 2007.
25. Lee, P. J., Di Gioia, A. J., Application note 720002488EN, Waters Corporation, 2008.