Hydrolysis of phosphoryl trichloride (POCl3): Characterization, in situ detection, and safe quenching of energetic metastable intermediates

Organic Process Research and Development

Volumn 14, Issue 6, 2010, Pages 1490-1500

  Achmatowicz, Micha M ^a   Thiel, Oliver R ^a   Colyer, John T ^a   Hu, Jack ^a   Elipe, Maria Victoria Silva ^a   Tomaskevitch, Joe ^a   Tedrow, Jason S ^a   Larsen, Robert D ^a  

^a AMGEN INC   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ANALYTICAL TECHNIQUES; EXOTHERMIC EVENTS; IN-SITU; LARGE SCALE PREPARATION; METASTABLE INTERMEDIATE; REACTIVE INTERMEDIATE; REACTIVE PHOSPHORUS; REACTIVE SPECIES; SEMI-BATCH; TEMPERATURE CONDITIONS; TIME-COURSE EXPERIMENTS;

CHLORINE; DIFFERENTIAL SCANNING CALORIMETRY; PHOSPHORUS; RAMAN SPECTROSCOPY;

HYDROLYSIS;

EID: 78649652778     PISSN: 10836160     EISSN: 1520586X     Source Type: Journal    
DOI: 10.1021/op1001484     Document Type: Article

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