Testing the sensitivity limits of 33S NMR: An ultra-wideline study of elemental sulfur

Journal of Magnetic Resonance

Volumn 207, Issue 2, 2010, Pages 345-347

  O'Dell, Luke A ^a   Moudrakovski, Igor L ^a  

^a NATIONAL RESEARCH COUNCIL CANADA   (Canada)

Author keywords

33S solid state NMR; CASTEP; Electric field gradient tensors; Ultra wideline; WURST pulses

Indexed keywords

CASTEP; ELECTRIC FIELD GRADIENT TENSORS; SOLID STATE NMR; ULTRA-WIDELINE; WURST PULSES;

ELECTRIC FIELDS; MAGNETIC FIELDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLID STATE PHYSICS; SULFUR; TENSORS;

NUCLEAR MAGNETIC RESONANCE;

SULFUR; SULFUR DERIVATIVE;

ALGORITHM; ARTICLE; CHEMISTRY; CRYSTALLIZATION; CRYSTALLOGRAPHY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; TEMPERATURE;

ALGORITHMS; CRYSTALLIZATION; CRYSTALLOGRAPHY; MAGNETIC RESONANCE SPECTROSCOPY; SULFUR; SULFUR COMPOUNDS; SULFUR ISOTOPES; TEMPERATURE;

EID: 78649442825     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2010.08.022     Document Type: Article

References (28)

1. H. Eckert, and J.P. Yesinowski Sulfur-33 NMR at natural abundance in solids J. Am. Chem. Soc. 108 1986 2140 2146
2. T.J. Bastow, and S.N. Stuart NMR of the zinc chalcogenides (ZnX, XO, S, Se, Te) Phys. Status Solidi B 145 1988 719 728
3. 33S NMR with high-speed magic-angle spinning J. Magn. Reson. A 123 1996 219 221
4. 33S NMR of inorganic sulfides J. Magn. Reson. 161 2003 191 197
5. 33S NMR of inorganic sulfates J. Magn. Reson. 170 2004 336 344
6. 33S solid state NMR of sulfur speciation in silicate glasses Solid State Nucl. Magn. Reson. 26 2004 203 208
7. Q in a variable temperature study J. Magn. Reson. 180 2006 170 177
8. 33S solid-state NMR to cement chemistry Cem. Concr. Res. 36 2006 1781 1783
9. 33S MAS NMR: characterization of transition-metal MS bonds in ammoniumtetrathiometallates Chem. Commun. 2007 1629 1631
10. 33S MAS NMR spectroscopy employing adiabatic inversion pulses to the satellite transitions J. Magn. Reson. 190 2008 316 326
11. 33S MAS NMR of a disordered sulfur-doped silicate: signal enhancement via RAPT, QCPMG and adiabatic pulses Appl. Magn. Reson. 35 2008 247 259
12. 33S solid-state NMR study of layered transition metal disulfides at ultrahigh magnetic field Chem. Commun. 2009 186 188
13. 4 Phys. Chem. Chem. Phys. 11 2009 6981 6986
14. 33S solid-state NMR spectra of a disordered tetrathio transition-metal anion J. Magn. Reson. 202 2010 173 179
15. 33S solid state NMR and first principles calculations in potassium sulfates J. Phys. Chem. A 114 2010 309 316
16. F.H. Larsen, H.J. Jakobsen, P.D. Ellis, and N.C. Nielsen Sensitivity-enhanced quadrupolar-echo NMR of half-integer quadrupolar nuclei. Magnitudes and relative orientation of chemical shielding and quadrupolar coupling tensors J. Phys. Chem. A 101 1997 8597 8606
17. R. Siegel, T.T. Nakashima, and R.E. Wasylishen Sensitivity enhancement of NMR spectra of half-integer quadrupolar nuclei in the solid state via population transfer Concept Magn. Reson. A 26 2005 47 61
18. K. Torii, and Y. Iitaka Crystal structures and molecular conformations of l-methionine and l-norleucine Acta Crystallogr., Sect. B: Struct. Sci. 29 1973 2799 2807
19. 8 Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 43 1987 2260 2262
20. 35 Phys. Rev. 91 1953 313 314
21. R. Bhattacharyya, and L. Frydman Quadrupolar nuclear magnetic resonance spectroscopy in solids using frequency-swept echoing pulses J. Chem. Phys. 127 2007 194503
22. L.A. O'Dell, and R.W. Schurko QCPMG using adiabatic pulses for faster acquisition of ultra-wideline NMR spectra Chem. Phys. Lett. 464 2008 97 102
23. E. Kupče, and R. Freeman Adiabatic pulses for wideband inversion and broadband decoupling J. Mag. Reson. A 115 1995 273 276
24. D. Massiot, F. Fayon, M. Capron, I. King, S. Le Calvé, B. Alonso, J.O. Durand, B. Bujoli, Z. Gan, and G. Hoatson Modelling one- and two-dimensional solid-state NMR spectra Magn. Reson. Chem. 40 2002 70 76
25. A.C. Gallacher, and A.A. Pinkerton A redetermination of monoclinic γ-sulfur Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 49 1993 125 126
26. J. Donohue, A. Caron, and E. Goldish Crystal structure of rhombohedral sulphur Nature 182 1958 518
27. S.J. Clark, M.D. Segall, C.J. Pickard, P.J. Hasnip, M.J. Probert, K. Refson, and M.C. Payne First principles methods using CASTEP Z. Kristallogr. 220 2005 567 570
28. S. Adiga, D. Aebi, and D.L. Bryce EFGShield - a program for parsing and summarizing the results of electric field gradient and nuclear magnetic shielding tensor calculations Can. J. Chem. 85 2007 496 505