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78649331730
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note
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2fip (0.1 mmol) and 4, 4′-bipy (0.1 mmol) in methanol (2 mL). The resultant mixture was stirred for 30 min and filtered to allow the evaporation of the filtrates. Qualified single crystals were obtained after several days. Yield: 50-60%. Further experiment details are given in the Supporting Information.
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36
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78649332502
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note
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o). Crystal structures were solved by direct methods and SHELXTL[15] was used for structure solution and least-squares refinement.
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38
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13844267412
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The Pr-O bonds distances are in good agreement with those in other PrIII coordination frameworks, for example: B. Zhao, L. Yi, Y. Dai, X.Y. Chen, P. Cheng, D.Z. Liao, S.P. Yan, and Z.H. Jiang Inorg. Chem. 44 2005 911
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