Controlled synthesis of lanthanide-lithium inverse crown ether complexes

Inorganic Chemistry Communications

Volumn 13, Issue 12, 2010, Pages 1566-1568

  Lu, Xin Hua ^a   Ma, Meng Tao ^a   Yao, Ying Ming ^a   Zhang, Yong ^a   Shen, Qi ^a  

^a SOOCHOW UNIVERSITY   (China)

Author keywords

Bis(phenolate) ligand; Inverse crown ether complex; Lanthanide complex; Synthesis

Indexed keywords

EID: 78649328572     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.09.013     Document Type: Article

References (15)

1. R.E. Mulvey Organometallics 25 2006 1060
2. M. Westerhausen Dalton Trans. 2006 4755
3. R.E. Mulvey Acc. Chem. Res. 42 2009 743
4. A.R. Kennedy, J. Klett, R.E. Mulvey, S. Newton, and D. Wright Chem. Commun. 2008 308
5. N.M. Clark, P. Garcia-Alvarez, A.R. Kennedy, C.T. O'Hara, and G.M. Robertson Chem. Commun. 2009 5835
6. J.C. Wu, X.B. Pan, N. Tang, and C.C. Lin Inorg. Chem. 49 2010 5362
7. H.C. Aspinall, and M.R. Tillotson Inorg. Chem. 35 1996 2163
8. T. Dube, S. Gambarotta, and G. Yap Organometallics 17 1998 3967
9. S. Barroso, J.L. Cui, J.M. Carretas, A. Cruz, I.C. Santos, M.T. Duarte, J.P. Telo, N. Marques, and A.M. Martins Organometallics 28 2009 3449
10. Y.M. Yao, M.T. Ma, X.P. Xu, Y. Zhang, Q. Shen, and W.T. Wong Organometallics 24 2005 4014
11. -1): 2953 (s), 2900 (s), 2872 (s), 1625 (m), 1527 (m), 1540 (m), 1458 (s), 1416 (m), 1360 (m), 1226 (s), 1195 (s), 1048 (m), 981 (m), 928 (m), 795 (m), 722 (m), 639 (s), 553 (m), 502 (s).
12. 2. Crystallographic data for the structural analysis have been deposited with the Cambridge Crystallographic Data Center CCDC No. 787033.
13. 1): 2956 (s), 2917 (s), 2871 (s), 1752 (m), 1605 (m), 1562 (m), 1451 (s), 1382 (m), 1027 (m), 864 (m), 826 (m), 524 (s).
14. -1): 2964 (s), 2913 (s), 2849 (s), 1779 (m), 1592 (m), 1548 (m), 1463 (s), 1403 (m), 1391 (m), 1347 (m), 1245 (m), 1149 (m), 1028 (m), 865 (m), 815 (m), 770 (m), 718 (m), 535 (s).
15. int = 0.0294), and 6422 were observed reflections (I > 2.0 σ(I)). The structure was solved as that described for complex 1. The CCDC No. is 787034.