Sunflower oil coating on the nanoparticles of iron(III) oxides

Inorganic Chemistry Communications

Volumn 13, Issue 12, 2010, Pages 1402-1405

  Turta, Constantin ^a   Melnic, Silvia ^a   Prodius, Denis ^a   MacAev, Fliur ^a   Stoeckli Evans, Helene ^b   Ruiz, Patricia ^c   Muraviev, Dmitry ^c   Pogrebnoi, Serghei ^a   Ribkovskaia, Zinaida ^a   Mereacre, Valeriu ^d   Lan, Yanhua ^d   Powell, Annie K ^d  

^a INSTITUTE OF CHEMISTRY   (Moldova)

^b UNIVERSITY OF NEUCHÂTEL   (Switzerland)

^c UNIVERSITAT AUTÒNOMA DE BARCELONA   (Spain)

^d UNIVERSITY OF KARLSRUHE   (Germany)

Author keywords

Iron(III) furoate cluster; Iron(III) oxide nanoparticles; M ssbauer spectroscopy

Indexed keywords

EID: 78649322678     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.07.046     Document Type: Article

References (29)

1. R. Jin Angew. Chem. Int. Ed. 47 2008 6750
2. S. Laurent, D. Forge, M. Port, A. Roch, C. Robic, L. Vander Elst, and R.N. Muller Chem. Rev. 108 2008 2064
3. K.Y. Choi, K.H. Min, J.H. Na, K. Choi, K. Kim, J.H. Park, I.C. Kwon, and S.Y. Jeong J. Mater. Chem. 19 2009 4102
4. K.E. Scarberry, E.B. Dickerson, J.F. McDonald, and Z.J. Zhang J. Am. Chem. Soc. 130 2008 10258
5. S. Kakuta, and T. Abe J. Mater. Sci. 44 2009 2890
6. A. Gervasini, C. Messi, A. Ponti, S. Cenedese, and N. Ravasio J. Phys. Chem. C 112 2008 4635
7. C. Xu, and S. Sun Dalton Trans. 2009 5583 and references therein
8. C. Boyer, V. Bulmus, P. Priyanto, W.Y. Teoh, R. Amal, and T.P. Davis J. Mater. Chem. 19 2009 111
9. S. Sun, and H. Zeng J. Am. Chem. Soc. 124 2002 8204
10. S. Sun, H. Zeng, D.B. Robinson, S. Raoux, P.M. Rice, S.X. Wang, and G. Li J. Am. Chem. Soc. 126 2004 273
11. W.W. Yu, J.C. Falkner, C.T. Yavuz, and V.L. Colvin Chem. Comm. 2004 2306
12. J. Rockenberger, E.C. Scher, and A.P. Alivisatos J. Am. Chem. Soc. 121 1999 11595
13. F.X. Redl, C.T. Black, G.C. Papaefthymiou, R.L. Sandstrom, M. Yin, H. Zeng, C.B. Murray, and S.P. O'Brien J. Am. Chem. Soc. 126 2004 14583
14. U. Poth Drying oils and related products Ullmann's Encyclopedia of Industrial Chemistry 2002 Wiley-VCH Weinheim 31
15. - 1): 3129b, 1597sh, 1567b, 1469 s, 1416b, 1372b, 1231w, 1203 s, 1140 m, 1076w, 1014 m, 935 m, 884 m, 825w, 799w, 776sh, 757b, 630 m, 600sh, 510b.
16. 3. A mixture was slightly heated up to full dissolution. Hexadecylamine (3.00 g) was fused in a round-bottom flask with three necks, and a current of argon was passed through it during 5 min, then the oily solution was flowed into the flask. The flask was placed in the heating device and the mix was heated up during 2 hours, at the beginning gradually increasing, and then reducing the temperature in the range of 140-320 °C. The substance obtained as a result of the synthesis was dissolved in 50 ml of hexane. The solution was filtered and added to 50 ml of ethanol. In three days the received dark-brown precipitate was centrifuged (10,000 rotations, 10 min), and then it was again dissolved in hexane and ethanol was added. The newly obtained precipitate (N1) was centrifuged (10,000 rotations, 10 min) and washed out in ether.
17. 3. The mixture was slightly heated up to full dissolution. This oily solution was flowed into a round-bottom flask with three necks, and a current of argon was passed through it during 5 minutes. A flask was placed in the heating device and during 2 hours it was heated up at the beginning gradually increasing, and then reducing the temperature in the range of 140-320 °C. The substance obtained as a result of the synthesis was dissolved in 50 ml hexane. The solution was filtered and added to 50 ml of ethanol. The oily fraction (N2), which had dropped out during three day, was dissolved in hexane.
18. Ligand 2-(5-sulfanyl-1, 3, 4-oxadiazol-2-yl)phenol (0.2 g) was dissolved in 20 ml of ethanol and flowed into 20 ml of the received hexane solution N2 from P2. In a day the precipitate (N3) had dropped. It was centrifuged (10,000 rotations, 10 min) and washed out in ether.
19. F. Macaev, G. Rusu, S. Pogrebnoi, A. Gudima, E. Stingaci, L. Vlad, N. Shvets, F. Kandemirli, A. Dimoglo, and R. Reynolds Bioorg. Med. Chem. 13 2005 4842
20. G.A. Jeffrey, and W. Saenger Hydrogen Bonding in Biological Structures 1991 Springer-Verlag Berlin 20
21. N.K. Singh, R.J. Butcher, P. Tripathi, A.K. Srivastava, and M.K. Bharty Acta Cryst. E63 2007 o782
22. R. Zboril, M. Mashlan, and D. Petridis Chem. Mater. 14 2002 969
23. P. Ayyub, M. Multani, M. Barma, V.R. Palkar, and R.J. Vijayaraghavan Phys. C: Solid State Phys. 21 1988 2229
24. P.P. Vaishnava, U. Senaratne, E.C. Buc, R. Naik, V.M. Naik, G.M. Tsoi, and L.E. Wenger Phys. Rev. B 76 2007 024413
25. T. Ninjbadgar, S. Yamamoto, and T. Fukuda Solid State Sci. 6 2004 879
26. C. Cannas, G. Concas, D. Gatteschi, A. Falqui, A. Musinu, G. Piccaluga, C. Sangregorio, and G. Spano Phys. Chem. Chem. Phys. 3 2001 832
27. L. Machala, R. Zboril, and A. Gedanken J. Phys. Chem. B 111 2007 4003
28. Q.A. Pankhurst, J. Connolly, S.K. Jones, and J. Dobson J. Phys. D: Appl. Phys. 36 2003 R167
29. C. Kittel Introduction to Solid State Physics 8th ed 2005 Wiley New York 449