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85030583189
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4 and isolated by column chromatography or recrystallization. In the case of compound 20, 2 mmol of benzo-18- crown-6 is reacted with 1 mmol of compound 7
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4 and isolated by column chromatography or recrystallization. In the case of compound 20, 2 mmol of benzo-18-crown-6 is reacted with 1 mmol of compound 7.
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18
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85030574462
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Alternatively, hydride transfer might occur after arylation and formation of the carbocation intermediate. Products 25-27 could not be separated; their identities and relative yields were established by GC-MS, GC-FID, and 1H NMR analysis of the crude product mixture
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Alternatively, hydride transfer might occur after arylation and formation of the carbocation intermediate. Products 25-27 could not be separated; their identities and relative yields were established by GC-MS, GC-FID, and 1H NMR analysis of the crude product mixture.
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19
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85030580088
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3: 40.1, 63.5 (q, JC-F = 24 Hz), 111.8, 124.8, 127.1 (q, JC-F = 284 Hz), 129.2, 130.1, 130.3, 131.8, 132.5, 132.7, 140.7, 150.4. LR MS: 495/493/491 (M+), 426/424/422, 175. HRMS, C22H16NCl43 calcd 490.99888, found 490.99808.
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Characterization of Data of New Compounds
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