Mono- and dinuclear NiII and CoII complexes that feature chelating guanidine ligands: Structural characteristics and molecular magnetism

European Journal of Inorganic Chemistry

Volumn , Issue 30, 2010, Pages 4770-4782

  Roquette, Pascal ^a   König, Carolin ^a   Hübner, Olaf ^a   Wagner, Arne ^a   Kaifer, Elisabeth ^a   Enders, Markus ^a   Himmel, Hans Jörg ^a  

^a UNIVERSITY OF HEIDELBERG   (Germany)

Author keywords

Cobalt; Guanidines; Molecular magnetism; Nickel; Structure elucidation

Indexed keywords

COBALT COMPOUNDS; CRYSTALLINE MATERIALS; LIGANDS; NICKEL COMPOUNDS; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; QUANTUM CHEMISTRY; SINGLE CRYSTALS; SQUIDS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION;

CRYSTALLINE STATE; DINUCLEAR; DINUCLEAR COMPLEX; GUANIDINE; MOLECULAR MAGNETISM; MONONUCLEAR COMPLEXES; STRUCTURAL CHARACTERISTICS; STRUCTURE ELUCIDATION; SYNTHESISED; X- RAY DIFFRACTIONS;

CHELATION;

EID: 78249287501     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.201000315     Document Type: Article

References (50)

1. See, for example:, F. T. Edelmann, Adv. Organomet. Chem. 2008, 57, 183 - 352.
2. S. Herres-Pawlis, Nachr. Chem. 2009, 57, 20 - 23.
3. See, for example:, S. Herres-Pawlis, A. Neuba, O. Seewald, T. Seshadri, H. Egold, U. Flörke, G. Henkel, Eur. J. Org. Chem. 2005, 4879 - 4890.
4. M. Kawahata, K. Yamaguchi, T. Ho, T. Ishikawa, Acta Crystallogr., Sect. E: Struct. Rep. Online 2006, 62, o3301-o3302.
5. A. Peters, U. Wild, O. Hübner, E. Kaifer, H.-J. Himmel, Chem. Eur. J. 2008, 14, 7813 - 7821.
6. M. Reinmuth, U. Wild, E. Kaifer, M. Enders, H. Wadepohl, H.-J. Himmel, Eur. J. Inorg. Chem. 2009, 4795 - 4808.
7. P. Roquette, A. Maronna, A. Peters, E. Kaifer, H.-J. Himmel, C. Hauf, V. Herz, E.-W. Scheidt, W. Scherer, Chem. Eur. J. 2010, 16, 1336 - 1350.
8. V. Raab, J. Kipke, R. M. Gschwind, J. Sundermeyer, Chem. Eur. J. 2002, 8, 1682 - 1693.
9. U. Wild, O. Hübner, A. Maronna, M. Enders, E. Kaifer, H. Wadepohl, H.-J. Himmel, Eur. J. Inorg. Chem. 2008, 4440 - 4447.
10. J. Börner, S. Herres-Pawlis, U. Flörke, K. Huber, Eur. J. Inorg. Chem. 2007, 5645 - 5651.
11. A. Neuba, R. Hasse, M. Bernard, U. Floeke, S. Herres-Pawlis, Z. Anorg. Allg. Chem. 2008, 634, 2511 - 2517.
12. D. Petrovic, T. Glöge, T. Bannenberg, C. G. Hrib, S. Randoll, P. G. Jones, M. Tamm, Eur. J. Inorg. Chem. 2007, 3472 - 3475.
13. D. Petrovic, T. Bannenberg, S. Randoll, P. G. Jones, M. Tamm, Dalton Trans. 2007, 2812 - 2822.
14. J. Börner, U. Flörke, T. Glöge, T. Bannenberg, M. Tamm, M. D. Jones, A. Döring, D. Kuckling, S. Herres-Pawlis, J. Mol. Catal. A 2010, 316, 139 - 145.
15. T. Isobe, K. Fukuda, T. Ishikawa, J. Org. Chem. 2000, 65, 7770 - 7773.
16. H. Wittmann, Dissertation, 1999, Philipps-University Marburg.
17. A. Peters, E. Kaifer, H.-J. Himmel, Eur. J. Org. Chem. 2008, 5907 - 5914.
18. V. Vitske, C. König, O. Hübner, E. Kaifer, H.-J. Himmel, Eur. J. Inorg. Chem. 2010, 115 - 126.
19. C. Trumm, O. Hübner, E. Kaifer, H.-J. Himmel, Eur. J. Inorg. Chem. 2010, 3102 - 3108.
20. A. Peters, C. Trumm, M. Reinmuth, D. Emeljanenko, E. Kaifer, H.-J. Himmel, Eur. J. Inorg. Chem. 2009, 3791 - 3800.
21. In modification of the following:, H. Scheytza, O. Rademacher, H.-U. Reißig, Eur. J. Org. Chem. 1999, 2373 - 2381.
22. In modification of the following:, D. Chen, A. E. Martell, Y. Sun, Inorg. Chem. 1989, 28, 2647 - 2652.
23. The Cambridge Structural Database: a quarter of a million crystal structures and rising:, F. H. Allen, Acta Crystallogr., Sect. B 2002, 58, 380 388.
24. R. Bauernschmitt, R. Ahlrichs, Chem. Phys. Lett. 1996, 256, 454 - 464.
25. D. F. Evans, J. Chem. Soc. 1959, 2003 - 2005.
26. D. F. Evans, G. V. Fazakerley, R. F. Phillips, J. Chem. Soc. A 1971, 1931 - 1934.
27. J. Löliger, R. Schefflod, J. Chem. Educ. 1972, 49, 646 - 647.
28. D. H. Grant, J. Chem. Educ. 1995, 72, 39 - 40.
29. C. Piguet, J. Chem. Educ. 1997, 74, 815 - 816.
30. For an instructive derivation, see
31. R. Boča, Theoretical Foundations of Molecular Magnetism, Lausanne, Elsevier Science S. A., Lausanne, 1999.
32. R. Boča, Coord. Chem. Rev. 2004, 248, 757 815.
33. Program julX written by E. Bill:.
34. P. Roquette, A. Maronna, M. Reinmuth, M. Enders, H.-J. Himmel, J. Am. Chem. Soc., submitted for publication.
35. P. Fernández, H. Pritzkow, J. Carbó, P. Hofmann, M. Enders, Organometallics 2007, 26, 4402 - 4412.
36. DENZO-SMN, Data Processing Software, Nonius 1998,.
37. G. M. Sheldrick, SHELXS-97, Program for Crystal Structure Solution, University of Göttingen, 1997,.
38. G. M. Sheldrick, SHELXL-97, Program for Crystal Structure Refinement, University of Göttingen, 1997,.
39. International Tables for X-ray Crystallography, Kynoch Press, Birmingham, U.K., 1974, vol. 4.
40. L. Zsolnai, G. Huttner, XPMA, University of Heidelberg, 1994,.
41. R. Ahlrichs, M. Bär, M. Häser, H. Horn, C. Kölmel, Chem. Phys. Lett. 1989, 162, 165 - 169.
42. O. Treutler, R. Ahlrichs, J. Chem. Phys. 1995, 102, 346 - 354.
43. A. D. Becke, Phys. Rev. A 1988, 38, 3098 - 3100.
44. J. P. Perdew, Phys. Rev. B 1986, 33, 8822 - 8824.
45. P. J. Stephens, F. J. Devlin, C. F. Chabalowski, M. J. Frisch, J. Phys. Chem. 1994, 98, 11623 - 11627.
46. A. D. Becke, J. Chem. Phys. 1993, 98, 5648 - 5652.
47. C. Lee, W. Yang, R. G. Parr, Phys. Rev. B 1988, 37, 785 - 789.
48. F. Weigend, R. Ahlrichs, Phys. Chem. Chem. Phys. 2005, 7, 3297 - 3305.
49. K. Eichkorn, O. Treutler, H. Öhm, M. Häser, R. Ahlrichs, Chem. Phys. Lett. 1995, 242, 652 - 660.
50. F. Weigend, Phys. Chem. Chem. Phys. 2006, 8, 1057 - 1065.