A study of some practical aspects of high temperature liquid chromatography in pharmaceutical applications

Journal of Pharmaceutical and Biomedical Analysis

Volumn 54, Issue 3, 2011, Pages 458-462

  Berta, Renáta ^a   Babják, Mónika ^a   Gazdag, Mária ^a  

^a GEDEON RICHTER LTD   (Hungary)

Author keywords

Elevated temperature; Fast chromatography; Levonorgestrel; Steroids; Zirconia based column

Indexed keywords

10BETA HYDROXYLEVONORGESTREL; 6BETA HYDROXYLEVONORGESTREL; DELTA8(14) LEVONORGESTREL; LEVODION; LEVONORGESTREL; LEVONORGESTREL ABC TRIENE; METHANOL; UNCLASSIFIED DRUG; ZIRCONIUM OXIDE;

ANALYTIC METHOD; ARTICLE; DRUG IMPURITY; DRUG STRUCTURE; FLOW RATE; HIGH TEMPERATURE LIQUID CHROMATOGRAPHY; HIGH TEMPERATURE PROCEDURES; LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; SEPARATION TECHNIQUE;

CHROMATOGRAPHY; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, LIQUID; CONTRACEPTIVES, ORAL, SYNTHETIC; HOT TEMPERATURE; LEVONORGESTREL; PARTICLE SIZE; PHARMACEUTICAL PREPARATIONS; PRESSURE; ZIRCONIUM;

EID: 78149495902     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2010.09.012     Document Type: Article

References (28)

1. Maggs R.J. Advances in Chromatgraphy 1969, 303-309. Preston, Evanston, IL. A. Zlatkis (Ed.).
2. Antia F.D., Horvath Cs. High-performance liquid chromatography at elevated temperatures: examination of conditions for the rapid separation of large molecules. J. Chromatogr. 1988, 435:1-15.
3. Greibrokk T., Andersen T. High-temperature liquid chromatography. J. Chromatogr. A 2003, 1000:743-755.
4. McNeff C.V., Yan B., Stoll D.R., Henry R.A. Practice and theory of high temperature liquid chromatography. J. Sep. Sci. 2007, 30:1672-1685.
5. Vanhoenacker G., Pereira A.D.S., Kotsuka T., Cabooter D., Desmet G., Sandra P. Evaluation of a new polymeric stationary phase with reversed-phase properties for high temperature liquid chromatography. J. Chromatogr. A 2009, 1217:3217-3222.
6. Fields S.M., Ye C.Q., Zhang D.D., Branch B.R., Zhang X.J., Okafe N. Superheated water as eluent in high-temperature high-performance liquid chromatograph. J. Chromatogr. A 2001, 913:197-204.
7. Teutenberg T., Goetze H.-J., Tuerk J., Ploeger J., Kiffmeyer T.K., Schmidt K.G., Kohorst W.gr., Rohe T., Jansen H.-D., Weber H. Development and application of a specially designed heating system for temperature-programmed high-performance liquid chromatography using subcritical water as the mobile phase. J. Chromatogr. A 2006, 1114:89-96.
8. Heinisch S., Rocca J.L. Sense and nonsense of high-temperature liquid chromatography. J. Chromatogr. A 2009, 1216:642-658.
9. Stella C., Rudaz S., Veuthey J.-L., Tchapla A. Silica and other materials as supports in liquid chromatography. Chromatographic tests and their importance for evaluating these supports. Part I-II. Chromatographia 2001, 53:113-140.
10. Yang Y. Stationary phases for high temperature liquid chromatography. LC GC Europe 2003, 6:37-41.
11. Nawrocki J., Dunlap C., McCorrnich A., Carr P.W., Pert I. Chromatography using ultra-stable metal oxide-based stationary phases for HPLC. J. Chromatogr. A 2004, 1028:1-30.
12. Nawrocki J., Dunlap C., Li J., Zhao J., McNeff C.V., McCormick A., Carr P.W., Part I.I. Chromatography using ultra-stable metal oxide-based stationary phases for HPLC. J. Chromatogr. A 2004, 1028:31-62.
13. Neff C.Mc., Zigan L., Johnson K., Carr P.W., Wang A., Weber-Main A.M. Analytical advantages of highly stable stationary phases for reversed-phase LC. LC GC 2000, 18:514-529.
14. Teutenberg T., Tuerk J., Holzhauser M., Giegold S. Temperature stability of reversed phase and normal phase stationary phases under aqueous conditions. J. Sep. Sci. 2007, 30:1101-1114.
15. Marin S.J., Jones B.A., Felix W.D., Clark J. Effect of high-temperature on high-performance liquid chromatography column stability and performance under temperature-programmed conditions. J. Chromatogr. A 2004, 1030:255-262.
16. Claessens H.A., van Straten M.A. Review on the chemical and thermal stability of stationary phases for reversed-phase liquid chromatography. J. Chromatogr. A 2004, 1060:23-41.
17. Wilke C.R., Chang P. Correlation of diffusion coefficients in dilute solutions. Am. Inst. Chem. Eng. J. 1955, 1:264-270.
18. Sandra P., Vanhoenacker G. Elevated temperature-extended column length conventional liquid chromatography to increase peak capacity for the analysis, of tryptic digest. J. Sep. Sci. 2007, 30:241-244.
19. Smith R.M. Superheated water chromatography-a green technology for the future. J. Chromatogr. A 2008, 1184:441-455.
20. Vanhoenacker G., Sandra P. High temperature liquid chromatography and liquid chromatography-mass spectroscopy analysis of octylphenol ethoxylates on different stationary phases. J. Chromatogr. A 2005, 1082:193-202.
21. Sanagi M.M., See H.H., Ibrahim W.A.W., Naim A.A. High temperature liquid chromatography of triazole fungicides on polybutadiene-coated zirconia stationary phase. J. Chromatogr. A 2004, 1059:95-101.
22. Sanagi M.M., Heng S.H., Ibrahim W.A.W., Naim A.A. High temperature high performance liquid chromatography of triazole fungicides on carbon-clad zirconia stationary phase. Malays. J. Chem. 2004, 6:55-66.
23. Riddle L.A., Guiochon G. Separation of free sterols by high temperature liquid chromatography. J. Chromatogr. A 2006, 1137:173-179.
24. Al-Khateeb L.A., Smith R.M. High temperature liquid chromatography of steroids on a bonded hybrid column. Anal. Bioanal. Chem. 2009, 394:1255-1260.
25. Li J., Carr P.W. Effect of temperature on the thermodynamic properties, kinetic performance, and stability of polybutadiene-coated zirconia. Anal. Chem. 1997, 69:837-843.
26. Liu Y., Grinberg N., Thompson K.C., Wenslow R.M., Neue U.D., Morrison D., Walter T.H., O'Gara J.E., Wyndham K.D. Evaluation of a C18 hybrid stationary phase using high-temperature chromatography. Anal. Chim. Acta 2005, 554:144-151.
27. Guillarme D., Heinisch S., Rocca J.L. Effect of temperature in reversed phase liquid chromatography. J. Chromatogr. A 2004, 1052:39-51.
28. Guiochon G., Fellinger A., Shirazi D.G., Katti A.M. Fundamentals of Preparative and Nonlinear Chromatography 2006, Academic Press, Amsterdam, pp. 60-62.