Application of moment analysis to mass transfer kinetics of reversed-phase liquid chromatography: 2. A new understanding of the external mass transfer coefficient

Journal of Chromatographic Science

Volumn 48, Issue 9, 2010, Pages 742-749

  Gao, Hong ^a,b,c   Wu, Xiuhong ^a,b   Lin, Bingchang ^a,b  

^a DALIAN UNIVERSITY OF TECHNOLOGY   (China)

^b UNIVERSITY OF SCIENCE AND TECHNOLOGY LIAONING   (China)

^c ANSHAN NORMAL UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 77958019291     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/48.9.742     Document Type: Article

References (31)

1. G. Guiochon, A. Felinger, A. M. Katti, and D. G. Shirazi. Fundamentals of Preparative and Nonlinear Chromatography, 2nd ed., Academic Press, Amsterdam, 2006.
2. 18-silica monolithic columns. Anal. Chem. 75:6975-6986 (2003).
3. K. Miyabe, S. Sotoura, and G. Guiochon. Retention and mass transfer characteristics in reversed-phase liquid chromatography using a tetrahydrofuran-water solution as the mobile phase. J. Chromatogr. A 919:231-244 (2001).
4. K. Miyabe and G. Guiochon. Kinetic study of the concentration dependence of the mass transfer rate coefficient in anionexchange chromatography of bovine serum albumin. Biotechnol. Prog. 15:740-752 (1999).
5. K. Miyabe and G. Guiochon. Measurement of the parameters of the mass transfer kinetics in high performance liquid chromatography. J. Sep. Sci. 26:155-1 73 (2003).
6. K. Miyabe and G. Guiochon. Fundamental interpretation of the peak profiles in linear reversed-phase liquid chromatography. Adv. Chromatogr. 40:1-113 (2000).
7. K. Kaczmarski, D. Antos, H. Sajonz, P. Sajonz, and G. Guiochon. Comparative modeling of breakthrough curves of bovine serum albumin in anion-exchange chromatography. J. Chromatogr. A 925:1-17 (2001).
8. A. Cavazzini, K. Kaczmarski, P. Szabelski, D. Zhou, X. Liu, and G. Guiochon. Modeling of the separation of the enantiomers of 1-phenyl-1-propanol on cellulose tribenzoate. Anal. Chem. 73:5704-5715 (2001).
9. Z. Li, Y. Gu and T. Gu. Mathematical modeling and scale-up of size-exclusion chromatography. Biochem. Eng. J. 2:145-155 (1998).
10. T. Gu and Y. Zheng. A study of the scale-up of reversed-phase liquid chromatography. Sep. Purif. Technol. 15:41-58 (1999).
11. J.-H. Koh, PC. Wankat, and N.-H. L. Wang. Pore and surface diffusion and bulk-phase mass transfer in packed and fluidized beds. Ind. Eng. Chem. Res. 37:228-239 (1998).
12. Z. Ma, R. D. Whitley, and N.-H. L. Wang. Pore and surface diffusion in multicomponent adsorption and liquid chromatography systems. AIChEJ. 42:1244-1262 (1996).
13. C. R. Wilke and P. Chang. Correlation of diffusion coefficients in dilute solutions. AIChEJ. 1:264-270 (1955).
14. E. J. Wilson and C. J. Geankoplis. Liquid mass transfer at very low Reynolds numbers in packed beds. Ind. Eng. Chem. Fund. 5:9-14 (1966).
15. H. Gao, X. Wu, and B. Lin. Application of Moment Analysis to Mass Transfer Kinetics of Reversed-Phase Liquid Chromatography: Part 1. Experimental Investigation of Measurement of the Third Central Moment. J. Chromatogr. Sci. 48:478-483 (2010).
16. E. Kucera. Contribution to the theory of chromatography: linear non-equilibrium elution chromatography. J. Chromatogr. 19:237-248 (1965).
17. M. Kubin. Contribution to the theory of chromatography: influence of the diffusion outside and the adsorption within the sob-grains. Collect. Czech. Chem. Commun. 30:2900-2907 (1965).
18. M. Suzuki and J. M. Smith. Kinetic studies by chromatography. Chem. Eng. Sci. 26:221-235 (1971).
19. K. Miyabe and G. Guiochon. The moment equations of chromatography for monolithic stationary phases. J. Phys. Chem. B 106:8898-8909 (2002).
20. H. Guan and G. Guiochon. Study of physico-chemical properties of some packing materials: I. Measurements of the external porosity of packed columns by inverse size-exclusion chromatography. J. Chromatogr. A 731:27-40 (1996).
21. D. M. Ruthven. Principles of Adsorption and Adsorption Processes, John Wiley & Sons, New York, NY, 1984, chapter 7.
22. P. N. Dwivedi and S. N. Upadhyay. Particle-fluid mass transfer in fixed and fluidized beds. Ind. Eng. Chem. Proc. Des. Dev. 16:157-165 (1977).
23. T Koloini, M. Sopcic, and M. Zumer. Mass transfer in liquidfluidized beds at low Reynolds numbers. Chem. Eng. Sci. 32:637-641 (1977).
24. K. Rahman and M. Streat. Mass transfer in liquid fluidized beds of ion exchange particles. Chem. Eng. Sci. 36:293-300 (1981).
25. M. Bar-Ilan and W. Resnick. Gas-phase mass transfer in fixed beds at low Reynolds numbers. Ind. Eng. Chem. 49:313-320 (1957).
26. J. E. Williamson, K. E. Bazaire, and C. J. Geankoplis. Liquid-phase mass transfer at low Reynolds numbers. Ind. Eng. Chem. Fund. 2:126-129 (1963).
27. A. J. Karabelas, T. H. Wegner, and T. J. Hanratty. Use of asymptotic relations to correlate mass transfer data in packed beds. Chem. Eng Sci. 26:1581-1589 (1971).
28. J. D. Acetis and G. Thodos. Mass and heat transfer in flow of gases through spherical packings. Ind. Eng. Chem. 52:1003-1006 (1960).
29. L. K. McCune and R. H. Wilhelm. Mass and momentum transfer in a solid-liquid system. Ind. Eng. Chem. 41:1124-1134 (1949).
30. R. Pfeffer. Heat and mass transport in multiparticle systems. Ind. Eng. Chem. Fund. 3:380-383 (1964).
31. L. Hong, F. Gritti, G. Gulochon, and K. Kaczmarski. Rate constants of mass transfer kinetics in reversed phase liquid chromatography. AIChE J. 51:3122-3133 (2005).