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66749137090
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For initial syntheses of soluble poly(p -phenylene) derivatives by SPC, see
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For initial syntheses of soluble poly(p -phenylene) derivatives by SPC, see: Rehahn, M.; Schlüter, A. D.; Wegner, G.; Feast, W. J. Polymer 1989, 30, 1060
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0025479879
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For example, see the following review describing the "Durham route" to polyacetylene
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For example, see the following review describing the "Durham route" to polyacetylene: Feast, W. J.; Friend, R. H. J. Mater. Sci. 1990, 25, 3796
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For discussion on this issue, see: McKean, D. R.; Stille, J. K. Macromolecules 1987, 20, 1787 and ref 8
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For improvement of the Ballard approach, see
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For improvement of the Ballard approach, see: Gin, D. L.; Conticello, V. P.; Grubbs, R. H. J. Am. Chem. Soc. 1994, 116, 10934
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0000273314
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The universal calibration was obtained with an online viscometer. For the principle, see
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The universal calibration was obtained with an online viscometer. For the principle, see: Grubisic, Z.; Rempp, P.; Benoit, H. J. Polym. Sci., Part B 1967, 5, 753
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0030192215
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n = 8 kg/mol, which were underestimated in comparison to those from the universal calibration. Note that, for poly(p -phenylene)s, it is known that this conventional method tends to overestimate the molar mass. For details, see
-
n = 8 kg/mol, which were underestimated in comparison to those from the universal calibration. Note that, for poly(p -phenylene)s, it is known that this conventional method tends to overestimate the molar mass. For details, see: Vanhee, S.; Rulkens, R.; Lehmann, U.; Rosenauer, C.; Schulze, M.; Köhler, W.; Wegner, G. Macromolecules 1996, 29, 5136
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70349102968
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For a few cases of successful peak assignments, see
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For a few cases of successful peak assignments, see: Sangvikar, Y.; Fischer, K.; Schmidt, M.; Schlüter, A. D.; Sakamoto, J. Org. Lett. 2009, 11, 4112
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Jayakannan, M.; van Dongen, J. L. J.; Janssen, R. A. J. Macromolecules 2001, 34, 5386
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Trimpin, S.1
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33750540397
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For a related study, see:;,. This paper refers to desilylation on a film of poly[2-(3-dimethyldodecylsilylphenyl)-1, 4-phenylenevinylene]. The desilylation was assumed to be completed by dipping the film in a 1:1 mixture of trifluoroacetic acid/hexane at ambient temperature for 24 h. However, no experimental data is provided in order to inspect the degree of desilylation
-
For a related study, see: Naidu, B. V. K.; Jin, S.-H.; Kim, S.-C.; Shin, W.-S.; Lee, J. W.; Gal, Y.-S. J. Polym. Sci., Part A: Polym. Chem. 2006, 44, 6498. This paper refers to desilylation on a film of poly[2-(3- dimethyldodecylsilylphenyl)-1,4-phenylenevinylene]. The desilylation was assumed to be completed by dipping the film in a 1:1 mixture of trifluoroacetic acid/hexane at ambient temperature for 24 h. However, no experimental data is provided in order to inspect the degree of desilylation
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J. Polym. Sci., Part A: Polym. Chem.
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Naidu, B.V.K.1
Jin, S.-H.2
Kim, S.-C.3
Shin, W.-S.4
Lee, J.W.5
Gal, Y.-S.6
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