Simultaneous determination of atenolol and amiloride in pharmaceutical preparations by capillary zone electrophoresis with capacitively coupled contactless conductivity detection

Biomedical Chromatography

Volumn 24, Issue 9, 2010, Pages 948-953

  Al Azzam, Khaldun M ^a   Saad, Bahruddin ^a   Aboul Enein, Hassan Y ^b  

^a SCHOOL OF PHYSICS   (Malaysia)

^b NATIONAL RESEARCH CENTRE   (Egypt)

Author keywords

Amiloride; Atenolol; Capillary zone electrophoresis; Drug analysis

Indexed keywords

CAPILLARY ELECTROPHORESIS; DRUG PRODUCTS; ELECTROLYTES; FUSED SILICA;

AMILORIDE; ANALYTES; ATENOLOL; CAPACITIVELY COUPLED; CAPACITIVELY COUPLED CONTACTLESS CONDUCTIVITY DETECTION; CAPILLARY-ZONE ELECTROPHORESIS; CONTACTLESS CONDUCTIVITY DETECTOR; DRUG ANALYSIS; PHARMACEUTICAL PREPARATIONS; SIMULTANEOUS DETERMINATIONS;

AMINO ACIDS;

ACETIC ACID; AMILORIDE; AMILORIDE PLUS ATENOLOL PLUS CHLORTHALIDONE; APO ATENOL; ATENOLOL; ATENOLOL PLUS CHLORTALIDONE; ATENOLOL PLUS CHLORTHALIDONE; BUFFER; CHLORTALIDONE; ELECTROLYTE; HYPOTEN; NORMATEN; NOTEN; SILICON DIOXIDE; TEKLO; TENEDONE; TENORET 50; TERNOLOL; UNCLASSIFIED DRUG; VALINE;

ACCURACY; ARTICLE; CAPACITIVELY COUPLED CONTACTLESS CONDUCTIVITY DETECTOR; CAPILLARY ZONE ELECTROPHORESIS; DRUG DETERMINATION; DRUG FORMULATION; DRUG STRUCTURE; ELECTRIC CONDUCTIVITY; ELECTRIC POTENTIAL; HUMAN; HYDRODYNAMICS; SENSITIVITY AND SPECIFICITY; SEPARATION TECHNIQUE; STANDARD; TABLET; ULTRAVIOLET RADIATION; VALIDATION PROCESS;

EID: 77957202371     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.1390     Document Type: Article

References (39)

1. Al Azzam K, Elbashir AA, Elbashir MA, Saad B and Abdul Hamid S. Simultaneous determination of atenolol and chlorthalidone in pharmaceutical preparations by capillary - zone electrophoresis. Analytical Letters 2009; 42: 1458-1470.
2. Arias R, Jimenez RM, Alonso RM, Telez M, Arrieta I, Flores P andOrtiz-Lastra E. Determination of the β-blocker atenolol in plasma by capillary zone electrophoresis. Journal of Chromatography A 2001; 916: 297-304.
3. Balesteros MR, Faria AF and Oliveira AL. Determination of losartan associated with chlorthalidone or hydrochlorothiazide in capsules by capillary zone electrophoresis. Journal of Brazilian Chemical Society 2007; 18: 554-558.
4. Bonazzi D, Gotti R, Andrisano V and Cavrini V. Derivative UV spectrophotometric determination of atenolol and metoprolol in single- and multi-component pharmaceutical dosage forms. II Farmaco 1996; 51: 733-738. (Pubitemid 27076929)
5. Chen CG, Li LG, Si YJ and Li YP. AC impedance characteristics of capacitively coupled contactless conductivity detector cell in capillary electrophoresis. Electrochimica Acta 2009; 54: 6959-6962.
6. Dadgar D and Kelly MT. Determination of chlorthalidone in human plasma by reversed-phase micellar liquid chromatography. Analyst 1988; 113: 1223-1227.
7. Degen PH and Schweizer A.. Quantitative determination of drugs in biological materials by means of extractive alkylation and gas-liquid chromatography. Journal of Chromatography 1977; 142: 549-57.
8. El-Gindy A, Emara S and Mostafa A. HPLC and chemometric-assited spectrophotometric methods for simultaneous determination of atenolol, amiloride hydrochloride and chlorthalidone. II Farmaco 2005; 60: 269-278. (Pubitemid 40387409)
9. El-Gindy A, Sallam S and Abdel-salam RA. HPLC method for the simultaneous determination of atenolol and chlorthalidone in human breast milk. Journal of Separation Science 2008; 31: 677-682. (Pubitemid 351419572)
10. Fan Y, Gan X, Li S and Qin W. A rapid CE-potential gradient detection method for determination of quinolones. Electrophoresis 2007; 28: 4101-4107. (Pubitemid 350192885)
11. 4D). Journal of Pharmaceutical and Biomedical Analysis 2006; 40: 1288-1292.
12. Ferraro MCF, Castellano PM and Kaufman TS. Chemometrics-assisted simultaneous determination of atenolol and chlorthalidone in synthetic binary mixtures and pharmaceutical dosage forms. Analytical and Bioanalytical Chemistry 2003; 377: 1159-1164.
13. Ferraro MCF, Castellano PM and Kaufman TS. Chemometric determination of amiloride hydrochloride, atenolol, hydrochlorothiazide and timolol maleate in synthetic mixtures and pharmaceutical formulations. Journal of Pharmaceutical and Biomedical Analysis 2004; 34: 305-314.
14. Giachetti C, Tenconi A, Canali S, Zanolo G. Simultaneous determination of atenolol and chlorthalidone in plasma by high-performance liquid chromatography application to pharmacokinetics studies in man. Journal of Chromatography B 1997; 698: 187-194. (Pubitemid 27412520)
15. Henchoz Y , Schappler J, Geiser L, Prat J. Carrupt P-A and Veuthey JL. Rapid determination of pKa values of 20 amino acids by CZE with UV and capacitively coupled contactless conductivity detections. Analytical and Bioanalytical Chemistry 2007; 389: 1869-1878; http://www.camlab.co.uk/sitefiles/ Tech-papers/TempCondMeas.pdf
16. International Conference Harmonization. 1995. Guideline for Industry: Text on Validation of Analytical Procedures, Q2A.
17. Johnson RD and Lewis RJ. Quantitation of atenolol, metoprolol, and propranolol in postmortem human fluid and tissue specimens via LC/APCI-MS. Forensic Science International 2006; 156: 106-117.
18. Khuroo A, Mishra S, Singh O, Saxena S and Monif T. Simultaneous determination of atenolol and chlorthalidone by LC-MS-MS in human plasma. Chromatographia 2008; 68: 721-729.
19. Kubáň P and Hauser PC. Ten years of axial capacitively coupled contactless conductivity detection for CZE - a review. Electrophoresis 2009; 30: 176-188.
20. Kubáň P and Hauser PC. A review of the recent achievements in capacitively coupled contactless conductivity detection. Analytica Chimica Acta 2008; 607: 15-29. (Pubitemid 50012737)
21. Kubáň P, Abad-Villar EM and Hauser PC. Evaluation of contactless conductivity detection for the determination of UV absorbing and non-UV absorbing species in reversed-phase high-performance liquid chromatography. Journal of Chromatography A 2006; 1107: 159-164. (Pubitemid 43184217)
22. Magnar E and Klas G. Application of the extractive alkylation technique to the gas chromatographic determination of chlorthalidone in plasma in nanogram quantities. Analytical Chemistry 1974; 46: 39-42.
23. Maguregui MI, Alonso RM and Jimenez RM. Capillary zone electrophoretic method for the quantitative determination of the β-blocker atenolol in human urine. Journal of Liquid Chromatography and Related Technologies 1997; 20: 3377-3387.
24. Maguregui MI, Alonso RM and Jimenez RM. Simultaneous determination of the β-blocker atenolol and several complementary antihypertensive agents in pharmaceutical formulations and urine by capillary zone electrophoresis. Journal of Chromatographic Science 1998 36: 516-522.
25. McMurry J. Organic Chemistry, 4th edn. Brooks/Cole Publishing Co.: Pacific Grove, CA, 1996; 942-943.
26. Mohamed AEL-MI and Salem H.. Determination of antihypertensive mixtures by use of a chemometrics-assisted spectrophotometric method. Analytical and Bioanalytical Chemistry 2005; 382: 1066-1072.
27. Moraes CF, Souza ER, Souza VC, Medeiros EFF, Goncalves TF, Toledo JO, Karnikowski M, Gomes L, Karnikowski MGO, Cordova C and Nobrega OT. A common polymorphism in the rennin angiotensin system is associated with differential outcome of antihypertensive pharmacotherapy prescribed to Brazilian older women. Clininica Chimica Acta 2008; 396: 70-75.
28. Muirhead DC and Christie RB. Simple, sensitive and selective high-performance liquid chromatographic method for analysis of chlorthalidone in whole blood. Journal of Chromatography 1987; 416: 420-425. (Pubitemid 17083433)
29. 4D). Journal of Pharmaceutical and Biomedical Analysis 2009; 49: 333-337.
30. Pormsila W, Krähenbühl S and Hauser PC. Capillary electrophoresis with contactless conductivity detection for uric acid determination in biological fluids. Analytica Chimica Acta 2009; 636: 224-228.
31. Quek NM, Law WS, Lau HF, Zhao JH, Hauser PC and Li SFY. Determination of pharmaceuticals classified as emerging pollutants using capillary electrophoresis with capacitively coupled contactless conductivity detection. Electrophoresis 2008; 29: 3701-3709
32. Rapado-Martinez I, Garcia-Alvarez-Coque MC and Villanueva-Camanas RM. Liquid chromatographic procedure for the evaluation of β-blockers in pharmaceuticals using hybrid mobile phases. Journal of Chromatography A 1997; 765: 221-231. (Pubitemid 27152233)
33. Salem H. High-performance thin-layer chromatography for the determination of certain antihypertensive mixtures. Scientia Pharmaceutica 2004; 72: 157-174. (Pubitemid 38902215)
34. Sa'sa SI, Jalal IM and Khalil HS. Determination of atenolol combinations with hydrochlorothiazide and chlorthalidone in tablets formulations by reverse-phase HPLC. Journal of Liquid Chromatography 1988; 11: 1673-1696.
35. Šolínová V and Kašička V. Recent applications of conductivity detection in capillary and chip electrophoresis. Journal of Separation Science 2006; 29: 1743-1762.
36. Tanyanyiwa J and Hauser PC. High-voltage contactless conductivity detection of metal ions in capillary electrophoresis. Electrophoresis 2002; 23: 3781-3786. (Pubitemid 35469562)
37. Vetuschi C and Ragno G. Fourth UV derivative spectrophotometry for the simultaneous assay of atenolol and chlorthalidone in pharmaceuticals. International Journal of Pharmaceutics 1990; 65: 177-181.
38. Wehner W. Determination of atenolol/chlortalidone during dissolution of tablets with UV multicomponent analysis. Pharmazie 2000; 55: 543-544. (Pubitemid 30471444)
39. Yang Z and Qin W. Separation of fluoroquinolones in acidic buffer by capillaryelectrophoresis with contactless conductivity detection. Journal of Chromatography A 2009; 1216: 5327-5332.