Novel sensitive determination of steryl glycosides in biodiesel by gas chromatography-mass spectroscopy

Journal of Chromatography A

Volumn 1217, Issue 42, 2010, Pages 6555-6561

  Pieber, Bartholomaeus ^a   Schober, Sigurd ^a   Goebl, Christoph ^a   Mittelbach, Martin ^a  

^a UNIVERSITY OF GRAZ   (Austria)

Author keywords

Biodiesel; Derivatization; Gas chromatography mass spectroscopy (GC MS); Single ion monitoring (SIM); Steryl glycosides (SG)

Indexed keywords

DERIVATIZATION REAGENT; DERIVATIZATIONS; EXISTING METHOD; FATTY ACID METHYL ESTER; GLUCOPYRANOSIDE; HYDROXYL GROUPS; INTERNAL STANDARDS; LIMITS OF QUANTIFICATION; MASS SPECTROSCOPY; PRE-TREATMENT; QUANTITATIVE ANALYSIS; RECOVERY RATE; ROUND ROBIN TEST; SAMPLE PREPARATION; SINGLE-ION MONITORING; STERYL GLYCOSIDES; SUGAR MOIETY; TRIMETHYLCHLOROSILANES; TRIMETHYLSILYL;

BIODIESEL; ESTERS; FATTY ACIDS; IONS; MASS SPECTROMETERS; MASS SPECTROMETRY; SPECTRUM ANALYSIS; SUGAR (SUCROSE);

GAS CHROMATOGRAPHY;

ACETAMIDE DERIVATIVE; BIODIESEL; CAMPESTEROL; CHLOROTRIMETHYLSILANE; CHOLESTERYL BETA DEXTRO GLUCOPYRANOSIDE; FATTY ACID ESTER; GLUCOPYRANOSIDE; GLYCOSIDE; HYDROXYL GROUP; N,O BIS(TRIMETHYLSILYL)ACETAMIDE; SITOSTEROL; STEROL GLYCOSIDE; STIGMASTEROL; UNCLASSIFIED DRUG;

ACCURACY; ANALYTIC METHOD; ANALYTICAL PARAMETERS; ARTICLE; CHEMICAL COMPOSITION; CHEMICAL STRUCTURE; CONTROLLED STUDY; DERIVATIZATION; HIGH TEMPERATURE PROCEDURES; MASS FRAGMENTOGRAPHY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; RETENTION TIME; SENSITIVITY ANALYSIS; SILYLATION; SOYBEAN; SYNTHESIS;

BIOFUELS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GLYCOSIDES; IMIDOESTERS; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PLANT OILS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; STEROLS; TRIMETHYLSILYL COMPOUNDS;

EID: 77957020474     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.08.006     Document Type: Article

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