Optimization of laser-induced breakdown spectroscopy for rapid geochemical analysis

Chemical Geology

Volumn 277, Issue 1-2, 2010, Pages 137-148

  Tucker, J M ^a   Dyar, M D ^a   Schaefer, M W ^b   Clegg, S M ^c   Wiens, R C ^c  

^a MOUNT HOLYOKE COLLEGE   (United States)

^b LOUISIANA STATE UNIVERSITY   (United States)

^c LOS ALAMOS NATIONAL LABORATORY   (United States)

Author keywords

Bulk analysis; ChemCam; Elemental analysis; LIBS; Mars; Quantitative analysis

Indexed keywords

BULK ANALYSIS; CHEMCAM; ELEMENTAL ANALYSIS; LIBS; MARS; QUANTITATIVE ANALYSIS;

ATOMIC EMISSION SPECTROSCOPY; CALIBRATION; FORECASTING; IGNEOUS ROCKS; MANGANESE OXIDE; MARTIAN SURFACE ANALYSIS; METADATA; OPTIMIZATION; ROCKS; SILICON COMPOUNDS; SODIUM;

ANALYTICAL GEOCHEMISTRY;

ATOMIC EMISSION SPECTROSCOPY; CALIBRATION; CHEMICAL COMPOSITION; IGNEOUS GEOCHEMISTRY; IGNEOUS ROCK; MARTIAN ATMOSPHERE; OPTIMIZATION; PLANETARY EVOLUTION; PREDICTION; QUANTITATIVE ANALYSIS;

EID: 77956615920     PISSN: 00092541     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chemgeo.2010.07.016     Document Type: Article

References (41)

1. Anzano J.M., Villoria M.A., Ruiz-Medina A., Lasheras R.J. Laser-induced breakdown spectroscopy for quantitative spectrochemical analysis of geological materials: effects of the matrix and simultaneous determination. Anal. Chim. Acta 2006, 575(2):230-235. 10.1016/j.aca.2006.05.077.
2. Arca G., Ciucci A., Palleschi V., Rastelli S., Tognoni E. Trace element analysis in water by the laser-induced breakdown spectroscopy technique. Appl. Spectrosc. 1997, 51:1102-1105.
3. Barrette L., Turmel S. On-line iron-ore slurry monitoring for real-time process control of pellet making precesses using laser-induced breakdown spectroscopy: graphitic vs. total carbon detection. Spectrochim. Acta B 2001, 56(6):715-723. 10.1016/S0584-8547(01)00227-0.
4. Body D., Chadwick B.L. Optimization of the spectral data processing in a LIBS simultaneous elemental analysis system. Spectrochim. Acta B 2001, 56:725-736.
5. Buckley S.G., Johnsen H.A., Hencken K.R., Hahn D.W. Implementation of laser-induced breakdown spectroscopy as a continuous emissions monitor for toxic metals. Waste Manage. 2000, 20(5-6):455-462. 10.1016/S0956-053X(00)00011-8.
6. Ciucci A., Palleschi V., Rastelli S., Barbini R., Colao F., Fantoni R., Palucci A., Ribezzo S., van der Steen H.J.L. Trace pollutants analysis in soil by a time-resolved laser-induced breakdown spectroscopy technique. Appl. Phys. B: Lasers Opt. 1996, 63(2):185-190. 10.1007/BF01095271.
7. Clegg S.M., Sklute E., Dyar M.D., Barefield J.E., Wiens R.C. Multivariate analysis of remote laser-induced breakdown spectroscopy spectra using partial least squares, principal component analysis, and related techniques. Spectrochim. Acta B 2009, 64(1):79-88. 10.1016/j.sab.2008.10.045.
8. Cremers D.A., Radziemski L.J. History and fundamentals of LIBS. Laser-Induced Breakdown Spectroscopy (LIBS), Fundamentals and Applications 2006, 1-39. Cambridge University Press, Cambridge, UK. A.W. Miziolek, V. Palleschi, I. Schechter (Eds.).
9. Effenberger A.J., Scott J.R. Effect of atmospheric conditions on LIBS spectra. Sensors 2010, 10:4907-4925. 10.3390/s100504907.
10. Fabre C., Boiron M.-C., Dubessy J., Chabiron A., Charoy B., Crespo T.M. Advances in lithium analysis in solids by means of laser-induced breakdown spectroscopy: an exploratory study. Geochim. Cosmochim. Acta 2002, 66(8):1401-1407. 10.1016/S0016-7037(01)00858-4.
11. Gottfried J.L., Harmon R.S., De Lucia F.C., Miziolek A.W. Multivariate analysis of laser-induced breakdown spectroscopy chemical signatures for geomaterial classification. Spectrochim. Acta B 2009, 64:1009-1019. 10.1016/j.sab.2009.07.005.
12. Harmon R.S., De Lucia F.C., Miziolek A.W., McNesby K.L., Walters R.A., French P.D. Laser-induced breakdown spectroscopy (LIBS) - an emerging field-portable sensor technology for real-time, in-situ geochemical and environmental analysis. Geochem. Explor. Environ. Anal. 2005, 5:21-28. 10.1144/1467-7873/03-059.
13. Harmon R.S., Remus J., McMillan N.J., McManus C., Collins L., Gottfried J.L., DeLucia F.C., Miziolek A.W. LIBS analysis of geomaterials: geochemical fingerprinting for the rapid analysis and discrimination of minerals. Appl. Geochem. 2009, 24:1125-1141. 10.1016/j.apgeochem.2009.02.009.
14. Knight A.K., Scherbarth N.L., Cremers D.A., Ferris M.J. Characterization of laser-induced breakdown spectroscopy (LIBS) for application to space exploration. Appl. Spectrosc. 2000, 54(3):331-340.
15. Le Maitre R.W., Streckeisen A., Zanettin B., Le Bas M.J., Bonin B., Bateman P., Bellieni G., Dudek A., Efremova S., Keller J., Lamere J., Sabine P.A., Schmid R., Sorensen H., Woolley A.R. Igneous Rocks: A Classification and Glossary of Terms, Recommendations of the International Union of Geological Sciences, Subcommission of the Systematics of Igneous Rocks 1989, Cambridge University Press, Cambridge, UK.
16. Liias, R.A., 1986. Geochemistry and petrogenesis of basalts erupted along the Juan de Fuca Ridge. Ph.D. thesis, Dept. of Geol., Univ. of Massachusetts, Amherst.
17. Malinowski E.R. Factor Analysis in Chemistry 2002, John Wiley and Sons, Inc., New York. 3rd ed.
18. Martens H., Næs T. Multivariate Calibration 1989, John Wiley and Sons Ltd., Chichester, UK.
19. Martin M.Z., Labbe N., Rials T.G., Wullschlegger S.W. Analysis of preservative-treated wood by multivariate analysis of laser-induced breakdown spectroscopy spectra. Spectrochim. Acta B 2005, 60:1179-1185. 10.1016/j.sab.2005.05.022.
20. Munson C.A., de Lucia F.C., Piehler T., McNesby K.L., Miziolek A.W. Investigation of statistics strategies for improving the discriminating power of laser-induced breakdown spectroscopy for chemical and biological warfare agent simulants. Spectrochim. Acta B 2005, 60:1217-1224. 10.1016/j.sab.2005.05.017.
21. Norrish K., Chappell B.W. X-ray fluorescent spectrography. Physical Methods in Determinative Mineralogy 1967, 161-214. Academic, San Diego. J. Zussman (Ed.).
22. Norrish K., Hutton J.T. An accurate X-ray spectrographic method for the analysis of a wide range of geological samples. Geochim. Cosmochim. Acta 1969, 33(4):431-453. 10.1016/0016-7037(69)90126-4.
23. Pakhomov A.V., William N., Jacek B. Laser-induced breakdown spectroscopy for detection of lead in concrete. Appl. Spectrosc. 1996, 50(7):880-884. 10.1366/0003702963905538.
24. Palanco S., López-Moreno C., Laserna J.J. Design, construction, and assessment of a field-deployable laser-induced breakdown spectrometer for remote elemental sensing. Spectrochim. Acta B 2006, 61(1):88-95. 10.1016/j.sab.2005.12.004.
25. Pasquini C., Cortez J., Silva L.M.C., Gonzaga F.B. Laser induced breakdown spectroscopy. J. Braz. Chem. Soc. 2007, 18:463-512. 10.1590/S0103-50532007000300002.
26. Radziemski L.J., Loree T.R., Cremers D.A., Hoffman N.M. Time-resolved laser-induced breakdown spectrometry of aerosols. Anal. Chem. 1983, 55(8):1246-1252. 10.1021/ac00259a016.
27. Rehse S.J., Jeyasingham N., Diedrich J., Palchaudhuri S. A membrane basis for bacterial identification and discrimination using laser-induced breakdown spectroscopy. J. Appl. Phys. 2009, 105:102034. 10.1063/1.2116141.
28. Reynolds R.C. Estimation of mass absorption coefficients by Compton scattering: improvements and extension of the method. Am. Mineral. 1967, 52:1493-1502.
29. Rhodes J.M. Geochemistry of the 1984 Mauna Loa eruption: implications for magma storage and supply. JGR-Solid Earth 1988, 93(B5):4453-4466.
30. Rhodes J.M. Geochemical stratigraphy of lava flows sampled by the Hawaii Scientific Drilling Project. JGR-Solid Earth 1996, 101(B5):11729-11746.
31. Rhodes J.M., Vollinger M.J. Composition of basaltic lavas sampled by phase-2 of the Hawaii Scientific Drilling Project: geochemical stratigraphy and magma types. Geochem. Geophys. Geosyst. 2004, 5:Q03G13. 10.1029/2002GC000434.
32. Rosenwasser S., Asimellis G., Bromley B., Hazlett R., Martin J., Pearce T., Zigler A. Development of a method for automated quantitative analysis of ores using LIBS. Spectrochim. Acta B 2001, 56(6):707-714. 10.1016/S0584-8547(01)00191-4.
33. Runge E.F., Minck R.W., Bryan F.R. Spectrochemical analysis using a pulsed laser source. Spectrochim. Acta 1964, 20:733-735. 10.1016/0371-1951(64)80070-9.
34. Schaefer M.W., Dyar M.D., Clegg S.M., Wiens R.C. An IDL Routine for Preprocessing and Analysis of LIBS Data. 39th Lunar and Planetary Science Conference, Lunar and Planetary Institute, League City, Tex. Abstr. 2171 2008.
35. Sirven J.-B., Bousquet B., Canioni L., Sarger L. Laser-induced breakdown spectroscopy of composite samples: Comparison of advanced chemometrics methods. Anal. Chem. 2006, 78:1462-1469. 10.1021/ac051721p.
36. Sirven J.-B., Sallé B., Mauchien P., Lacour J.-L., Maurice S., Manhes G. Feasibility study of rock identification at the surface of Mars by remote laser-induced breakdown spectroscopy and three chemometric methods. J. Anal. At. Spectrom. 2007, 22:1471-1480. 10.1039/b704868h.
37. Thompson J.R., Wiens R.C., Barefield J.E., Vaniman D.T., Newsom H.E., Clegg S.M. Remote laser-induced breakdown spectroscopy analyses of Dar al Gani 476 and Zagami Martian meteorites. J. Geophys. Res. 2006, 111:E05006. 10.1029/2005JE002578.
38. Tognoni E., Palleschi V., Corsi M., Cristoforetti G., Omenetto N., Gornushkin I., Smith B.W., Wineforder J.D. From sample to signal in laser-induced breakdown spectroscopy: a complex route to quantitative analysis. Laser-Induced Breakdown Spectroscopy (LIBS), Fundamentals and Applications 2006, 122-170. Cambridge University Press, Cambridge, UK. A.W. Miziolek, V. Palleschi, I. Schechter (Eds.).
39. Walker D. Behavior of mass absorption coefficients near absorption edges: Reynolds' method revisited. Am. Mineral. 1973, 58:1069-1072.
40. Whitehouse A.I., Young J., Botheroyd I.M., Lawson S., Evans C.P., Wright J. Remote material analysis of nuclear power station steam generator tubes by laser-induced breakdown spectroscopy. Spectrochim. Acta B 2001, 56(6):821-830. 10.1016/S0584-8547(01)00232-4.
41. Yin W.B., Zhang L., Dong L., Ma W.G., Jia S.T. Design of a laser-induced breakdown spectroscopy system for on-line quality analysis of pulverized coal in power plants. Appl. Spectrosc. 2009, 63(8):865-872.