Continuous hydrothermal synthesis of Fe2O3 nanoparticles using a central collision-type micromixer for rapid and homogeneous nucleation at 673 K and 30 MPa

Industrial and Engineering Chemistry Research

Volumn 49, Issue 18, 2010, Pages 8841-8846

  Sue, Kiwamu ^a   Sato, Toshiyuki ^b   Kawasaki, Shin Ichiro ^a   Takebayashi, Yoshihiro ^a   Yoda, Satoshi ^a   Furuya, Takeshi ^a   Hiaki, Toshihiko ^b  

^a NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY AIST   (Japan)

^b NIHON UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

AVERAGE PARTICLE SIZE; HETEROGENEOUS NUCLEATION; HOMOGENEOUS NUCLEATION; INNER WALLS; MICRO MIXERS; MOLALITIES; MONOMODAL DISTRIBUTION; RESIDENCE TIME; STARTING SOLUTIONS;

CRYSTAL STRUCTURE; MIXERS (MACHINERY); NANOPARTICLES; NUCLEATION;

HYDROTHERMAL SYNTHESIS;

EID: 77956396504     PISSN: 08885885     EISSN: 15205045     Source Type: Journal    
DOI: 10.1021/ie1008597     Document Type: Article

References (15)

1. Galindo, I. R.; Viveros, T.; Chadwick, D. Synthesis and Characterization of Titania-Based Ternary and Binary Mixed Oxides Prepared by the Sol-Gel Method and Their Activity in 2-Propanol Dehydration Ind. Eng. Chem. Res. 2007, 46, 1138
2. Widiyastuti, W.; Balgis, R.; Iskandar, F.; Okuyama, K. Nanoparticle Formation in Spray Pyrolysis under Low-pressure Conditions Chem. Eng. Sci. 2010, 65, 1846
3. 3 Nanoparticles in KOH Solution J. Mater. Sci. Technol. 2010, 26, 33
4. Chung, J. W.; Yang, H. K.; Moon, B. K.; Choi, B. C.; Jeong, J. H.; Bae, J. S.; Kim, K. H. The dependence of temperature synthesis of GdVO4:Eu3+ nanoparticle phosphors by solvothermal method Curr. Appl. Phys. 2009, 9, S222
5. Adschiri, T.; Kanazawa, K.; Arai, K. Rapid and continuous hydrothermal crystallization of metal oxide particles in supercritical water J. Am. Ceram. Soc. 1992, 75, 1019
6. Adschiri, T.; Hakuta, Y.; Sue, K.; Arai, K. Hydrothermal synthesis of metal oxide nanoparticles at supercritical conditions J. Nanopart. Res. 2001, 3, 227
7. Adschiri, T.; Hakuta, Y.; Arai, K. Hydrothermal synthesis of metal oxide nanoparticles at supercritical conditions Ind. Eng. Chem. Res. 2000, 39, 4901
8. Mae, K.; Suzuki, A.; Maki, T.; Hakuta, Y.; Sato, H.; Arai, K. A new micromixer with needle adjustment for instant mixing and heating under high pressure and high temperature J. Chem. Eng., Jpn. 2007, 40, 1101
9. Lester, E.; Blood, P.; Denyer, J.; Giddings, D.; Azzopardi, B.; Poliakoff, M. Reaction engineering: The supercritical water hydrothermal synthesis of nano-particles J. Supercrit. Fluids 2006, 37, 209
10. Wakashima, Y.; Suzuki, A.; Kawasaki, S.-I.; Matsui, K.; Hakuta, Y. Development of a new swirling micro mixer for continuous hydrothermal synthesis of nano-size particles J. Chem. Eng., Jpn. 2007, 40, 622
11. Sue, K.; Suzuki, M.; Arai, K.; Ohashi, T.; Ura, H.; Matsui, K.; Hakuta, Y.; Hayashi, H.; Watanabe, M.; Hiaki, T. Size-controlled synthesis of metal oxide nanoparticles with a flow-through supercritical water method Green Chem. 2006, 6, 634
12. Kawasaki, S.-I.; Sue, K.; Ookawara, R.; Wakashima, Y.; Suzuki, A.; Arai, K. Engineering study of continuous supercritical hydrothermal method using a T-shaped mixer: Experimental synthesis of NiO nanoparticles and CFD simulation J. Supercrit. Fluids 2006, 54, 96-102
13. 3, NiO, and CuO nanoparticles by superrapid heating using a T-type micro mixer at 673 K and 30 MPa. Submitted to Chem. Eng. J.
14. Sato, T.; Sue, K.; Suzuki, W.; Suzuki, M.; Matsui, K.; Hakuta, Y.; Hayashi, H.; Arai, K.; Kawasaki, S.-I.; Kawai-Nakamura, A.; Hiaki, T. Rapid and continuous production of ferrite nanoparticles by hydrothermal synthesis at 673 K and 30 MPa Ind. Eng. Chem. Res. 2008, 47, 1855
15. Chlistunoff, J.; Ziegler, K. J.; Lasdon, L.; Johnston, K. P. Nitric/Nitrous Acid Equilibria in Supercritical Water J. Phys. Chem. A 1999, 103, 1678