Synthesis and characterization of electrocatalytically active platinum atom clusters and monodisperse single crystals

Journal of Physical Chemistry C

Volumn 114, Issue 32, 2010, Pages 13515-13525

  St John, Samuel ^a   Dutta, Indrajit ^a   Angelopoulos, Anastasios P ^a  

^a UNIVERSITY OF CINCINNATI   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AGGLOMERATION; ATOMIC BEAMS; ATOMS; CATALYST ACTIVITY; CHLORINE COMPOUNDS; CRYSTAL ATOMIC STRUCTURE; ELECTROCATALYSIS; ELECTROLYTIC REDUCTION; INORGANIC ACIDS; OXYGEN; PLATINUM; PLATINUM COMPOUNDS; PRECIPITATION (CHEMICAL); ROTATING DISKS; SINTERING; SURFACE ACTIVE AGENTS; SUSPENSIONS (FLUIDS); SYNTHESIS (CHEMICAL); TRANSMISSION ELECTRON MICROSCOPY;

ACTIVE AREA; ATOMIC CLUSTERS; CATALYTIC ACTIVITY; CLUSTER TRANSITIONS; COMMERCIAL CATALYST; ELECTRODE STRUCTURE; HAADF-STEM; HIGH CURRENT DENSITIES; HIGH-ANGLE ANNULAR DARK FIELDS; MASS ACTIVITY; MONODISPERSE; NONREGULAR STRUCTURES; ORGANIC RESIDUES; ORGANIC SURFACTANTS; OXYGEN REDUCTION REACTION; PARTICLE AGGREGATION; PERCHLORIC ACIDS; PLATINUM ATOMS; PLATINUM DISPERSION; PT LOADING; PT PARTICLE; REACTION MECHANISM; REVERSIBLE HYDROGEN ELECTRODES; ROTATING DISK ELECTRODES; SCANNING TRANSMISSION ELECTRON MICROSCOPY; STABILIZED SUSPENSION; STABILIZING AGENTS; STANNOUS CHLORIDE; SYNTHESIS AND CHARACTERIZATIONS; SYNTHESIS TECHNIQUES; TAFEL SLOPES; UNDERPOTENTIAL DEPOSITION;

SINGLE CRYSTALS;

EID: 77956146111     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/jp103848n     Document Type: Article

References (77)

1. Kocha, S. S. In Handbook of Fuel Cells; Vielstich, W., Lamm, A., Gasteiger, H. A., Eds.; Wiley: Chichester, U.K., 2003; Vol.3, p 538.
2. Ralph, T. R.; Hogarth, M. P. Platinum Met. Rev. 2002, 46, 117.
3. Gasteiger, H. A.; Kocha, S. S.; Sompalli, B.; Wagner, F. T. Appl. Catal. B 2005, 56, 9.
4. Gasteiger, H. A.; Gu, W.; Makharia, R.; Mathias, M.; Sompalli, B. In Handbook of Fuel Cells; Vielstich, W., Lamm, A., Gasteiger, H. A., Eds.; Wiley: Chichester, U.K., 2003; p 593.
5. Kinoshita, K. J. Electrochem. Soc. 1990, 137, 845.
6. Markovic, N. M.; Gasteiger, H. A.; Ross, P. N. J. Phys. Chem. 1995, 99, 3411.
7. Markovic, N. M.; Gasteiger, H. A.; Ross, P. N. J. Phys. Chem. 1996, 100, 6715.
8. Markovic, N. M.; Adzic, R. R.; Cahan, B. D.; Yeager, E. B. J. Electroanal. Chem. 1994, 377, 249.
9. Markovic, N.; Gasteiger, H.; Ross, P. N. J. Electrochem. Soc. 1997, 144, 1591.
10. Mayrhofer, K. J. J.; Blizanac, B. B.; Arenz, M.; Stamenkovic, V. R.; Ross, P. N.; Markovic, N. M. J. Phys. Chem. B 2005, 109, 14433.
11. Wang, J. X.; Markovic, N. M.; Adzic, R. R. J. Phys. Chem. B 2004, 108, 4127.
12. Van Hardeveld, R.; Hartog, F. Surf. Sci. 1969, 15, 189.
13. Panchenko, A.; Koper, M. T. M.; Shubina, T. E.; Mitchell, S. J.; Roduner, E. J. Electrochem. Soc. 2004, 151, A2016.
14. Chen, W.; Chen, S. Angew. Chem., Int. Ed. 2009, 48.
15. Haruta, M.; Yamada, N.; Kobayashi, T.; Iijima, S. J. Catal. 1989, 115, 301.
16. Valden, M.; Lai, X.; Goodman, D. Science 1998, 281, 1647.
17. Hayden, B.; Pletcher, D.; Rendall, M.; Suchsland, J. J. Phys. Chem. C 2007, 111, 17044.
18. Boccuzzi, F.; Cerrato, G.; Pinna, F.; Strukul, G. J. Phys. Chem. B 1998, 102, 5733.
19. Yagi, I.; Ishida, T.; Uosaki, K. Electrochem. Commun. 2004, 6, 773.
20. Hernandez, J.; Solla-Gullon, J.; Herrero, E.; Aldaz, A.; Feliu, J. J. Phys. Chem. C 2007, 111.
21. Chen, W.; Ny, D.; Chen, S. J. Power Sources 2010, 195, 412.
22. Tracy, J.; Kalyuzhny, G.; Crowe, M.; Balasubramanian, R.; Choi, J.; Murray, R. J. Am. Chem. Soc. 2007, 129, 6706.
23. Yamamoto, K.; Imaoka, T.; Chun, W.; Enoki, O.; Katoh, H.; Takenaga, M.; Sonoi, A. Nat. Chem. 2009, 1, 397.
24. Tada, T. In Handbook of Fuel Cells; Vielstich, W., Lamm, A., Gasteiger, H. A., Eds.; Wiley: Chichester, U.K., 2003; Vol.3, p 481.
25. Sarkar, A.; Murugan, A. V.; Manthiram, A. Langmuir 2009.
26. Murray, C. B.; Norris, D. J.; Bawendi, M. G. J. Am. Chem. Soc. 1993, 115, 8706.
27. Bond, G. C. Platinum Met. Rev. 1975, 19, 126.
28. Watanabe, M.; Saegusa, S.; Stonehart, P. Chem. Lett. 1988, 17, 1487.
29. Yano, H.; Inukai, J.; Uchida, H.; Watanabe, M.; Babu, P.; Kobayashi, T.; Chung, J.; Oldfield, E.; Wieckowski, A. Phys. Chem. Chem. Phys. 2006, 8, 4932.
30. Wang, C.; Daimon, H.; Onodera, T.; Koda, T.; Sun, S. Angew. Chem., Int. Ed 2008, 47, 3588.
31. Yoo, S.; Jeon, T.; Lee, K.; Park, K.; Sung, Y. Chem. Commun. 2010, 46, 794.
32. Han, B.; Miranda, C.; Ceder, G. Phys. Rev. B 2008, 77, 75410.
33. Norskov, J.; Rossmeisl, J.; Logadottir, A.; Lindqvist, L.; Kitchin, J.; Bligaard, T.; Jonsson, H. J. Phys. Chem. B 2004, 108, 17886.
34. Takasu, Y.; Ohashi, N.; Zhang, X.; Murakami, Y.; Minagawa, H.; Sato, S.; Yahikozawa, K. Electrochim. Acta 1996, 41, 2595.
35. Tsung, C.-K.; Kuhn, J. N.; Huang, W.; Aliaga, C.; Hung, L.-I.; Somorjai, G. A.; Yang, P. J. Am. Chem. Soc. 2009, 131, 5816.
36. Komanicky, V.; Iddir, H.; Chang, K.-C.; Menzel, A.; Karapetrov, G.; Hennessy, D.; Zapol, P.; You, H. J. Am. Chem. Soc. 2009, 131, 5732.
37. Thompsett, D. In Handbook of Fuel Cells; Vielstich, W., Lamm, A., Gasteiger, H. A., Eds.; Wiley: Chichester, U.K., 2003; Vol.3, p 467.
38. Zhang, J.; Sasaki, K.; Sutter, E.; Adzic, R. R. Science 2007, 315, 220.
39. Adzic, R.; Zhang, J.; Sasaki, K.; Vukmirovic, M.; Shao, M.; Wang, J.; Nilekar, A.; Mavrikakis, M.; Valerio, J.; Uribe, F. Top. Catal. 2007, 46, 249.
40. Sanchez, S. I.; Small, M. W.; Zuo, J.-m.; Nuzzo, R. G. J. Am. Chem. Soc. 2009, 131, 8683.
41. O'Sullivan, E. J. M.; Horkans, J.; White, J. R.; Roldan, J. M. IBM J. Res. Dev. 1988, 32, 591.
42. Angelopoulos, A. P.; Jones, G. W.; Malek, R. W.; Marcello, H.; McKeveny, J.; IBM Corp.: U.S. Patent 5,866,237, 1999.
43. Angelopoulos, A. P.; Jones, G. W.; Malek, R. W.; Marcello, H.; McKeveny, J.; IBM Corp.: U.S. Patent 6,025,057, 2000.
44. Angelopoulos, A. P.; Jones, G. W.; Matienzo, L. J.; Miller, T. R.; Markovic, V.; IBM Corp.: U.S. Patent 5,935,652, 1999.
45. Angelopoulos, A. P.; Jones, G. W.; Matienzo, L. J.; Miller, T. R.; Taylor, W. D.; IBM Corp.: U.S. Patent 6,447,914 B1, 2002.
46. Angelopoulos, A. P.; Matienzo, L. J.; Benziger, J. B. J. Colloid Interface Sci. 1999, 212, 419.
47. Angelopoulos, A. P.; Benziger, J. B.; Wesson, S. P. J. Colloid Interface Sci. 1997, 185, 147.
48. Cohen, R. L.; West, K. W. J. Electrochem. Soc. 1973, 120, 502.
49. Shipley, C. R.; Shipley Company, Inc.: U.S. Patent 3,011,920, 961.
50. Meek, R. L. J. Electrochem. Soc. 1975, 122, 1177.
51. Cohen, R. L.; West, K. W. J. Electrochem. Soc. 1972, 119, 433.
52. Watanabe, M.; Uchida, M.; Motoo, S. J. Electroanal. Chem. 1987, 229, 395.
53. Petrow, H. G.; Allen, R. J.; Prototech Company: U.S. Patent 4,044,193, 1977.
54. Bailar, J. C., Ed. The Chemistry of the Co-ordination Compounds; Reinhold: New York, NY, 1956.
55. Iler, R. K. U.S. Patent 3,485,658, 1969.
56. Wang, L.; Luo, J.; Schadt, M. J.; Zhong, C. J. Langmuir 2009.
57. Alazemi, M.; Dutta, I.; Wang, F.; Blunk, R. H.; Angelopoulos, A. P. Adv. Funct. Mater. 2009, 19, 1118.
58. Farhat, T. R.; Hammond, P. T. Chem. Mater. 2005, 18, 41.
59. Angelopoulos, A. P.; Peters, S. L.; GM Global Technology Operations, Inc.: U.S. Patent 2007/0141238, 2007.
60. Angelopoulos, A. P.; Matienzo, L. J.; Jones, G. W. Langmuir 2000, 16, 1078.
61. Wang, F.; Peters, S.; Guzda, J.; Blunk, R.; Angelopoulos, A. Langmuir 2009, 25, 4384.
62. Sobkowski, J.; Franaszczuk, K.; Piasecki, A. J. Electroanal. Chem. 1985, 196, 145.
63. Uchida, H.; Ikeda, N.; Watanabe, M. J. Electroanal. Chem. 1997, 424, 5.
64. Cleveland, C. L.; Landman, U.; Schaaff, T. G.; Shafigullin, M. N.; Stephens, P. W.; Whetten, R. L. Phys. Rev. Lett. 1997, 79, 1873.
65. Ward, E. P. W.; Arslan, I.; Bleloch, A.; Thomas, J. M.; Midgley, P. A. J Phys: Conf. Ser. 2006, 26, 207.
66. Ward, E. P. W.; Arslan, I.; Midgley, P. A.; Bleloch, A.; Thomas, J. M. Chem. Commun. 2005, 46, 5808.
67. Philip, R.; Kumar, G.; Sandhyarani, N.; Pradeep, T. Phys. Rev. B 2000, 62, 13160.
68. Hache, F.; Ricard, D.; Flytzanis, C.; Kreibig, U. Appl. Phys. A: Mater. Sci. Process. 1988, 47, 347.
69. Hache, F.; Ricard, D.; Girard, C. Phys. Rev. B 1988, 38, 7990.
70. Ferreira, P. J.; la O, G. J.; Shao-Horn, Y.; Morgan, D.; Makharia, R.; Kocha, S.; Gasteiger, H. A. J. Electrochem. Soc. 2005, 152, A2256.
71. Merzougui, B.; Swathirajan, S. J. Electrochem. Soc. 2006, 153, A2220.
72. Damjanovic, A.; Genshaw, M. Electrochim. Acta 1970, 15, 1281.
73. Tarasevich, M. Elektrokhimiya 1973, 9, 599.
74. Uribe, F. A.; Wilson, M. S.; Springer, T. E.; Gottesfeld, S. In Proceedings of the Workshop on Structural Electrocatalysis and Oxygen Electrochemistry; The Electrochemical Society: Pennington, NJ, 1993; Vol.92-11, p 494.
75. Decher, G. In Multilayer Thin Films: Sequential Assembly of Nanocomposite Materials; Decher, G., Schlenoff, J. B., Eds.; Wiley-VCH: Weinheim, Germany, 2003; p 1.
76. Kavanov, V. In Multilayer Thin Films: Sequential Assembly of Nanocmposite Materials; Decher, G., Schlenoff, J. B., Eds.; Wiley-VCH: Weinheim, Germany, 2003; p 47.
77. Joanny, J. F.; Castelnovo, M. In Multilayer Thin Films: Sequential Assembly of Nanocomposite Materials; Decher, G., Schlenoff, J. B., Eds.; Wiley, VCH: Weinheim, Germany, 2003; p 87.