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Volumn 49, Issue 35, 2010, Pages 6178-6181

Preparation of ligand-stabilized [P4O4]2+ by controlled hydrolysis of a janus head type diphosphorus trication

Author keywords

Cascade reactions; Electrostatic activation; Phosphorus; Polycations; Structure elucidation

Indexed keywords

BUILDING BLOCKES; CASCADE REACTIONS; CATIONIC RINGS; CLUSTER SYSTEMS; CONTROLLED HYDROLYSIS; DICATIONS; EFFICIENT METHOD; LIGAND-STABILIZED; NEW OPPORTUNITIES; POLYCATIONS; STEPWISE HYDROLYSIS; STRUCTURE ELUCIDATION;

EID: 77956041260     PISSN: 14337851     EISSN: 15213773     Source Type: Journal    
DOI: 10.1002/anie.201001363     Document Type: Article
Times cited : (31)

References (42)
  • 10
    • 77956027256 scopus 로고
    • 239; Angew. Chem. Int. Ed. Engl. 1992, 31 216
    • R.Weiss, S. Engel, Angew. Chem. 1992, 104, 239; Angew. Chem. Int. Ed. Engl. 1992, 31, 216.
    • (1992) Angew. Chem. , vol.104
    • Weiss, R.1    Engel, S.2
  • 26
    • 77956014844 scopus 로고    scopus 로고
    • A full description of the technical and experimental details and X-ray diffraction data for 1[OTf]3 and 2[OTf]2 are given in the Supporting Information. CCDC 766183 (1[OTf] 3) and 766184 (2[OTf] 2) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
    • A full description of the technical and experimental details and X-ray diffraction data for 1[OTf]3 and 2[OTf]2 are given in the Supporting Information. CCDC 766183 (1[OTf] 3) and 766184 (2[OTf] 2) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac. uk/datarequest/cif.
  • 27
    • 0003337777 scopus 로고
    • Phosphane 6 was prepared according to a modified procedure
    • Phosphane 6 was prepared according to a modified procedure: S. Fischer, L.K. Peterson, Can.J. Chem. 1974, 52, 3981.
    • (1974) Can.J. Chem. , vol.52 , pp. 3981
    • Fischer, S.1    Peterson, L.K.2
  • 28
    • 77956014417 scopus 로고    scopus 로고
    • Seven contacts; shortest: dPO=2.665(2)
    • Seven contacts; shortest: dPO=2.665(2).
  • 33
    • 77956053824 scopus 로고    scopus 로고
    • The Supporting Information provides a full description of the computational details, a comparison of the theoretical and experimentally obtained 31P chemical shifts, and a summary of the NBO analysis
    • The Supporting Information provides a full description of the computational details, a comparison of the theoretical and experimentally obtained 31P chemical shifts, and a summary of the NBO analysis.
  • 36
    • 77956026839 scopus 로고
    • The 31P NMR spectrum of dissolved 2[OTf]2 shows very small amounts of a second product (<2%; d=86.8 ppm), which we tentatively assign to the cis isomer.[14] a) S. Berger, S. Braun, H.-O. Kalinowski, 31P NMR-Spektroskopie, Georg Thieme, Stuttgart
    • The 31P NMR spectrum of dissolved 2[OTf]2 shows very small amounts of a second product (<2%; d=86.8 ppm), which we tentatively assign to the cis isomer.[14] a) S. Berger, S. Braun, H.-O. Kalinowski, 31P NMR-Spektroskopie, Georg Thieme, Stuttgart
    • (1993) , vol.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.