Development and validation of a sensitive gas chromatography-ammonia chemical ionization mass spectrometry method for the determination of tabun enantiomers in hemolysed blood and plasma of different species

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 878, Issue 17-18, 2010, Pages 1290-1296

  Tenberken, Oliver ^a   Worek, Franz ^a   Thiermann, Horst ^a   Reiter, Georg ^a  

^a BUNDESWEHR INSTITUTE OF PHARMACOLOGY AND TOXICOLOGY   (Germany)

Author keywords

Analysis; Blood; Enantiomers; Plasma; Solid phase extraction; Tabun

Indexed keywords

AMMONIA; BLOOD; CHROMATOGRAPHY; ENANTIOMERS; GAS CHROMATOGRAPHY; IONIZATION; IONIZATION OF GASES; MASS SPECTROMETRY; PHASE SEPARATION; PHOSPHORUS COMPOUNDS; PLASMAS; STEREOCHEMISTRY;

ANALYSIS; CHEMICAL IONIZATION MASS SPECTROMETRY; LIMIT OF DETECTION; LIMIT OF QUANTIFICATIONS; ORGANOPHOSPHORUS COMPOUNDS; POSITIVE CHEMICAL IONIZATIONS; SOLID-PHASE EXTRACTION; TABUN;

EXTRACTION;

BETA CYCLODEXTRIN; TABUN; CHEMICAL WARFARE AGENT; ORGANOPHOSPHATE;

ANALYTIC METHOD; ARTICLE; BLOOD ANALYSIS; CHEMICAL ANALYSIS; CHIRALITY; CONTROLLED STUDY; ENANTIOMER; GAS CHROMATOGRAPHY; HEMOLYSIS; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS SPECTROMETRY; NONHUMAN; PLASMA; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; SPECIES DIFFERENCE; SWINE; VALIDITY; ANIMAL; BLOOD; CHEMISTRY; DRUG STABILITY; GUINEA PIG; HUMAN; MASS FRAGMENTOGRAPHY; METHODOLOGY; RAT; STATISTICAL MODEL; STEREOISOMERISM;

SUIDAE;

ANIMALS; CHEMICAL WARFARE AGENTS; DRUG STABILITY; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GUINEA PIGS; HUMANS; LINEAR MODELS; PHOSPHORIC ACID ESTERS; RATS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; SPECIES SPECIFICITY; STEREOISOMERISM; SWINE;

EID: 77955485248     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2009.09.002     Document Type: Article

References (42)

1. H.P. Benschop, L.P.A. de Jong, Acc. Chem. Res. 21 (1988) 368.
2. G. Reiter, J. Mikler, I. Hill, K. Weatherby, H. Thiermann, F. Worek, J. Chromatogr. B 873 (2008) 86.
3. D. Noort, H.P. Benschop, R.M. Black, Toxicol. Appl. Pharmacol. 184 (2002) 116.
4. K.E. Holland, M.I. Solano, R.C. Johnson, V.L. Maggio, J.R. Barr, J. Anal. Toxicol. 32 (2008) 116.
5. M.J. van der Schans, M. Polhuijs, D.C. van Dijk, C.E. Degenhardt, K. Pleijsier, J.P. Langenberg, H.P. Benschop, Arch. Toxicol. 78 (2004) 508.
6. C.E. Degenhardt, K. Pleijsier, M.J. van der Schans, J.P. Langenberg, K.E. Preston, M.I. Solano, V.L. Maggio, J.R. Barr, J. Anal. Toxicol. 28 (2004) 364.
7. M.J. van der Schans, A. Fidder, A.G. Hulst, D. Noort, J. Anal. Toxicol. 32 (2008) 125.
8. N.H. Williams, J.M. Harrison, R.W. Read, R.M. Black, Arch. Toxicol. 81 (2007) 627.
9. R.M. Black, J. Anal. Toxicol. 32 (2008) 2.
10. W.J. Driskell, M. Shih, L.L. Needham, D.B. Barr, J. Anal. Toxicol. 26 (2002) 6.
11. J.R. Barr, J. Anal. Toxicol. 28 (2004) 305.
12. P.A. D'Agostino, L.R. Provost, J.Chromatogr. 598 (1992) 89.
13. W.R. Creasy, J.R. Stuff, B. Williams, K. Morrissey, J. Mays, R. Duevel, H.D. Durst, J. Chromatogr. A 774 (1997) 253.
14. P.A. Ďi{dotless}Agostino, J.R. Hancock, C.L. Chenier, C.R. Lepage, J. Chromatogr. A 1110 (2006) 86.
15. P.A. D'Agostino, J.R. Hancock, L.R. Provost, DRES TM 2000-04, Defence R&D Canada, Suffield, 2000.
16. P.A. D'Agostino, J.R. Hancock, L.R. Provost, J. Chromatogr. A 840 (1999) 289.
17. J.A. Törnes, A.M. Opstad, B.A. Johnsen, Int. J. Environ. Anal. Chem. 44 (1991) 209.
18. H.A. Lakso, Anal. Chem. 69 (1997) 1866.
19. C.E. Degenhardt, G.R. van den Berg, L.P. De Jong, H.P. Benschop, J. Am. Chem. Soc. 108 (1982) 8290.
20. G.R. van den Berg, H.C. Beck, H.P. Benschop, Bull. Environ. Contam. Toxicol. 33 (1984) 505.
21. J.R. Smith, J. Schlager, J. High Resolut. Chromatogr. 19 (1996) 151.
22. NCCLS Evaluation of Precision Performance of Clinical Chemistry Devices; Approved guideline NCCLS, Wayne, PA, 1999
23. L. Larsson, Acta Chem. Scand. 6 (1952) 1470.
24. L. Larsson, Acta Chem. Scand. 7 (1953) 306.
25. J. Epstein, Public Health Rep. 71 (1956) 955.
26. C.L. Copper, G.E. Collins, Electrophoresis 25 (2004) 897.
27. J. Benes, Acta Chem. Scand. 17 (1963) 1783.
28. H.P. Benschop, E.C. Bijleveld, M.F. Otto, C.E.A.M. Degenhardt, H.P. van Helden, L.P. De Jong, Anal. Biochem. 151 (1985) 242.
29. W.N. Aldridge, E. Reiner, Enzyme Inhibitors as Substrates, North-Holland Publishing Company, Amsterdam, London, 1972.
30. M. Polhuijs, J.P. Langenberg, H.P. Benschop, Toxicol. Appl. Pharmacol. 146 (1997) 156.
31. S.P. Harvey, J.E. Kolakowski, T.C. Cheng, V.K. Rastogi, J.J. DeFrank, F.M. Raushel, C. Hill, Enzyme Microb. Technol. 37 (2005) 547.
32. G. Reiter, M. Koller, H. Thiermann, F. Dorandeu, J. Mikler, F. Worek, J. Chromatogr. B 859 (2007) 9.
33. V.M.A. Häkkinen, J. High Resolut. Chromatogr. 14 (1991) 811.
34. E.M. Jakubowski, J.M.McGuire, R.A. Evans, J.L. Edwards, S.W. Hulet, B.J. Benton, J.S. Forster, D.C. Burnett, W.T. Muse, K. Matson, C.L. Crouse, R.J. Mioduszewski, S.A. Thomson, J. Anal. Toxicol. 28 (2004) 357.
35. C.E. Degenhardt, C.E. Kientz, J. Chromatogr. A 723 (1996) 210.
36. M. Polhuijs, H.P. Benschop, TNO Prins Maurits Laboratory, Report PML 1997-C68, Rijswijk, The Netherlands, 1997.
37. L.P.A. de Jong, C. van Dijk, Biochem. Pharmacol. 33 (1984) 663.
38. V.P. Shah, K.K. Midha, S. Dighe, I.J. McGilveray, J.P. Skelly, A. Yacobi, T. Layloff, C.T. Viswanathan, C.E. Cook, R.D. McDowall, Eur. J. Drug Metab. Pharmacokinet. 16 (1991) 249.
39. V.P. Shah, K.K. Midha, J.W. Findlay, H.M. Hill, J.D. Hulse, I.J. McGilveray, G. McKay, K.J. Miller, R.N. Patnaik, M.L. Poweil, A. Tonelli, C.T. Viswanathan, A. Yacobi, Pharm. Res. 17 (2000) 1551.
40. F. Eyer, P. Eyer, Hum. Exp. Toxicol. 17 (1998) 645.
41. M. Sogorb, I. Sanchez, M. Lopez-Rivadilla, V. Cespedes, E. Vilanova, Drug Metab. Dispos. 27 (1998) 27.
42. E. Erdös, L. Boggs, Nature 1960 (1961) 716.