A one-pot sulfide to sulfone oxidation with m-chloroperoxybenzoic acid and sodium permanganate

Tetrahedron Letters

Volumn 51, Issue 32, 2010, Pages 4211-4213

  Dishington, Allan ^a   Fillery, Shaun ^a   Finlay, M Raymond V ^a  

^a ASTRAZENECA   (United Kingdom)

Author keywords

m Chloroperoxybenzoic acid; Pyrimidines; Sodium permanganate; Sulfide oxidation; Sulfone

Indexed keywords

3 CHLOROPERBENZOIC ACID; MORPHOLINE DERIVATIVE; PERMANGANATE POTASSIUM; PERMANGANATE SODIUM; PYRIMIDINE DERIVATIVE; SULFIDE; SULFONE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL REACTION; CHEMICAL STRUCTURE; ONE POT SYNTHESIS;

EID: 77955303907     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2010.06.020     Document Type: Article

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7. 3) and MeCN as eluents. Fractions containing the desired compound were evaporated to dryness to afford the pure product.