Synthesis and structural, magnetic and electrochemical characterization of PtCo nanoparticles prepared by water-in-oil microemulsion

Journal of Nanoparticle Research

Volumn 12, Issue 4, 2010, Pages 1149-1159

  Solla Gullon J ^a   Gómez, Elvira ^b   Vallés, Elisa ^b   Aldaz, Antonio ^a   Feliu, Juan M ^a  

^a UNIVERSITY OF ALICANTE   (Spain)

^b UNIVERSITY OF BARCELONA   (Spain)

Author keywords

Magnetic properties; Microemulsion; Production; PtCo nanoparticles; TEM; XRD

Indexed keywords

CELL PARAMETER; CRYSTALLINE LATTICE; CUBIC PHASE; ELECTROCATALYTIC ACTIVITY; ELECTROCHEMICAL CHARACTERIZATIONS; N-HEPTANES; OXALIC ACID; SUPERPARAMAGNETICS; TEM; THERMAL TREATMENT; WATER-IN-OIL MICROEMULSIONS; X-RAY DIFFRACTION STUDIES; XRD;

COBALT; MAGNETIC MATERIALS; MAGNETIC PROPERTIES; MICROEMULSIONS; NANOPARTICLES; PLATINUM; SUPERPARAMAGNETISM; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION;

NANOMAGNETICS;

COBALT; HEPTANE; MACROGOL; NANOPARTICLE; OXALIC ACID; PLATINUM; POLYETHYLENEGLYCOL DODECYL ETHER; SULFATE; UNCLASSIFIED DRUG; WATER;

ARTICLE; CATALYST; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; CHEMICAL REACTION; CHEMICAL STRUCTURE; ELECTROCHEMISTRY; HEAT TREATMENT; MAGNETISM; MICROEMULSION; OXIDATION; PARTICLE SIZE; PRIORITY JOURNAL; STRUCTURE ANALYSIS; SYNTHESIS; TECHNIQUE; X RAY DIFFRACTION;

EID: 77955089665     PISSN: 13880764     EISSN: 1572896X     Source Type: Journal    
DOI: 10.1007/s11051-009-9680-4     Document Type: Article

References (49)

1. Antolini E, Salgado JRC, Gonzalez ER (2006) The stability of Pt-M (M = first row transition metal) alloy catalysts and its effect on the activity in low temperature fuel cells. A literature review and tests on a Pt-Co catalyst. J Power Sources 160(2 SPEC. ISS):957-968
2. Antonietti M, Basten R, Lohmann S (1995) Polymerization in microemulsions: a new approach to ultrafine, highly functionalized polymer dispersions. Macromol Chem Phys 196:441-466
3. Bell AT (2003) The impact of nanoscience on heterogeneous catalysis. Science 299:1688-1691
4. 2 slurry reactor. Appl Catal B Environ 39:221-231
5. 3 catalyst to improve the ozonation of oxalic acid in water. Appl Catal B Environ 47:101-109
6. Boutonnet M, Kizling J, Stenius P, G. Marie G (1982) The preparation of monodisperse colloidal metal particles from microemulsions. Colloids Surf 5:209-225
7. Burda C, Chen XB, Narayanan R, El-Sayed MA (2005) Chemistry and properties of nanocrystals of different shapes. Chem Rev 105:1025-1102
8. Chang CL, Fogler HS (1996) Kinetics of silica particle formation in nonionic w/o microemulsions from TEOS. AlChE J 42:3153-3163
9. Chhabra V, Lal M, Maitra AN, Ayyub P (1995) Preparation of ultrafine high density gamma ferric oxide using aerosol OT microemulsions and its characterization. Colloid Polym Sci 273:939-946
10. Cui X, Shi J, Zhang L, Ruan M (2009) PtCo supported on ordered mesoporous carbon as an electrode catalyst for methanol oxidation. Carbon 47:186-194
11. Drake C, Deshpand S, Bera D, Seal S (2007) Metallic nanostructured materials based sensors. Int Mater Rev 52: 289-316
12. El-Sayed MA (2001) Some interesting properties of metals confined in time and nanometer space of different shapes. Acc Chem Res 34:257-264
13. Fender JH (1980) Microemulsions, micelles, and vesicles as media for membrane mimetic photochemistry. J Phys Chem 84:1485
14. Gandini D, Mahe E, Michaud PA, Haenni W, Perret A, Ch Comninellis (2000) Oxidation of carboxylic acids at boron-doped diamond electrodes for wastewater treatment. J Appl Electrochem 30:1345-1350
15. Gasteiger HA, Markovic N, Ross PN, Cairns EJ (1994) CO electrooxidation on well-characterized Pt-Ru alloys. J Phys Chem 98:617-625
16. Geho DH, Jones CD, Petricoin EF, Liotta LA (2006) Nanoparticles: potential biomarker harvesters. Curr Opin Chem Biol 10:56-61
17. Gennes PG, Taupin C (1982) Microemulsions and the flexibility of oil/water interfaces. J Phys Chem 86:2294
18. 2 particles in water-in-oil microemulsions. J Phys Chem 98:7628-7635
19. Jung OJ (2001) Destruction of 2-chlorophenol from wastewater and investigation of by-products by ozonation. Bull Korean Chem Soc 22:850-856
20. Jusys Z, Kaiser J, Behm RJ (2002) Composition and activity of high surface area PtRu catalysts towards adsorbed CO and methanol electrooxidation: a DEMS study. Electrochim Acta 47:3693-3706
21. 4 ultrafine particles in microemulsions. J Mater Sci 29:3739-3801
22. López-Quintela MA, Rivas J (1993) Chemical reactions in microemulsions: a powerful method to obtain ultrafine particles. J Colloid Interface Sci 158:446-451
23. López-Quintela MA, Rivas J, Blanco MC, Tojo C (2003) Synthesis of nanoparticles in microemulsions. In: Liz- Marzá,n LM, Kamat PV (eds) Nanoscale materials. Kluwer Academic, Boston, p 135
24. Luo X, Morrin A, Killard AJ, Smyth MR (2006) Application of nanoparticles in electrochemical sensors and biosensors. Electroanalysis 18:319-326
25. Martinez-Huitle CA, Ferro S, De Battisti A (2004) Electrochemical incineration of oxalic acid: role of electrode material. Eletrochim Acta 49:4027-4034
26. Martinez-Huitle CA, Ferro S, De Battisti A (2005) Electrochemical incineration of oxalic acid: reactivity and engineering parameters. J Appl Electrochem 35:1087-1093
27. Nagy J (1989) Multinuclear NMR characterization of microemulsions: preparation of monodisperse colloidal metal boride particles. Colloids Surf 35:201-220
28. 2 nanoparticles in a non-ionic reverse micellar system. Colloids Surf 50:321-339
29. Pera-Titus M, García-Molina V, Baños M, Jiménez J, Esplugas S (2004) Degradation of chlorophenols by means of advanced oxidation processes: a general review. Appl Catal B Environ 47:219-256
30. Pérez A, Dupuis V, Tuaillon-Comes J, Bardotti L, Prével B, Mélinon P, Jamet M, Wernsdorfer W, Barbara B (2003) Magnetic nanostructures. In: Liz-Marzá,n LM, Kamat PV (eds) Nanoscale materials. Kluwer Academic, Boston, pp 371-394
31. Pileni MP (1989) Structure and reactivity in reverse micelles. Elsevier, Amsterdam
32. Qian Y, Wen W, Adcock PA, Jiang Z, Hakim N, Saha MS, Mukerjee S (2008) PtM/C catalyst prepared using reverse micelle method for oxygen reduction reaction in PEM fuel cells. J Phys Chem C 112:1146-1157
33. Scherrer P (1918) Bestimmung der gröbe und der inneren struktur von kolloidteilchen mittels Röntgenstrahlen. Nachr.Ger.Wiss. Göttingen Math-Phys, KL 2:96-100
34. Singhal M, Chhabra V, Kang P, Shah DO (1997) Synthesis of ZnO nanoparticles for varistor application using Zn-substituted aerosol OT microemulsion. Mater Res Bull 32:239-243
35. Sires I, Cabot PL, Centelles F, Garrido JA, Rodriguez RM, Arias C, Brillas E (2006) Electrochemical degradation of clofibric acid in water by anodic oxidation. Comparative study with platinum and boron-doped diamond electrodes. Eletrochim Acta 52:75-85
36. Solla-Gullón J, Montiel V, Aldaz A, Clavilier J (2000) Electrochemical characterization of platinum nanoparticles prepared by microemulsion: how to clean them without loss of crystalline surface structure. J Electroanal Chem 491:69-77
37. Solla-Gullón J, Montiel V, Aldaz A, Clavilier J (2003a) Synthesis and electrochemical decontamination of platinum- palladium nanoparticles prepared by water-in-oil microemulsion. J Electrochem Soc 150:E104-E109
38. Solla-Gullón J, Rodes A, Montiel V, Aldaz A, Clavilier J (2003b) Electrochemical characterisation of platinum-palladium nanoparticles prepared in a water-in-oil microemulsion. J Electroanal Chem 554:273-284
39. Solla-Gullón J, Vidal-Iglesias FJ, Montiel V, Aldaz A (2004) Electrochemical characterization of platinum-ruthenium nanoparticles prepared by water-in-oil microemulsion. Electrochim Acta 49:5079-5088
40. Solla-Gullón J, Rodríguez P, Herrero E, Aldaz A, Feliu JM (2008) Surface characterization of platinum electrodes. Phys Chem Chem Phys 10:1359-1373
41. Somorjai GA, Tao F, Park JY (2008) The nanoscience revolution: merging of colloid science, catalysis and nanoelectronics. Top Catal 47:1-14
42. Sperling RA, Rivera Gil P, Zhang F, Zanella M, Parak WJ (2008) Biological applications of gold nanoparticles. Chem Soc Rev 37:1896-1908
43. Sun X, Jia ZY, Huang YH, Harrell JW, Nikes DE (2004) Synthesis and magnetic properties of CoPt nanoparticles. J Appl Phys 95:6747-6749
44. Tourode R, Girard P, Marie G, Kizling J, Boutonnet-Kizling M, Stenius P (1992) Preparation of colloidal platinum/ palladium alloy particles from non-ionic microemulsions: characterization and catalytic behaviour. Colloids Surf 67:9-19
45. Trasatti S, Petrii OA (1991) Real surface area measurements in electrochemistry. Pure Appl Chem 63:711-734
46. Wieckowski A, Savinova E, Vayenas CC (2003) Catalysis and electrocatalysis at nanoparticle surfaces. Marcel Dekker, New York
47. Woods R (1976) Chemisorption at electrodes. Hydrogen and oxygen on noble metals and their alloys. In: Bard AJ (ed) Electroanalytical chemistry, vol 9. Marcel Dekker, New York, pp 1-162
48. Wu ML, Chen DH, Huang TC (2001) Synthesis of Au/Pd bimetallic nanoparticles in reverse micelles. Langmuir 17:3877-3883
49. Zhang L, Gu FX, Chan JM, Wang AZ, Langer RS, Farokhzad OC (2008) Nanoparticles in medicine: therapeutic applications and developments. Clin Pharmacol Ther 83: 761-769