Reversed-phase high performance liquid chromatographic profile of organic fractions extracted by solvents with different polarity as a tool to evaluate the hydrophobic character of soil under different management

Soil and Tillage Research

Volumn 109, Issue 1, 2010, Pages 36-40

  Marinari, S ^a   Liburdi, K ^a   Corradini, D ^b   Grego, S ^a  

^a UNIVERSITY OF TUSCIA   (Italy)

^b CNR   (Italy)

Author keywords

Methodology; Organic solvent extractions; SOM fingerprint

Indexed keywords

AGRICULTURAL SYSTEM; AMPHIPHILLICS; ARABLE LAND; CATION EXCHANGE CAPACITIES; CENTRAL ITALY; CHROMATOGRAPHIC PROFILES; CONTINUOUS INPUT; DIFFERENT SOLVENTS; ETHYL ACETATES; FRESH PLANTS; HUMIC MATERIALS; HYDROPHOBIC CHARACTER; HYDROPHOBIC SOLVENT; LINEAR GRADIENT ELUTION; METHODOLOGICAL APPROACH; METHODOLOGY; N-HEXANE; ORGANIC FARMING; ORGANIC FRACTIONS; ORGANIC MATTER; ORGANIC SOIL; ORGANIC SUBSTANCES; PCA ANALYSIS; REVERSED-PHASE HIGH PERFORMANCE; REVERSED-PHASE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY; RP-HPLC; SANDY CLAY LOAM; SOIL ANALYSIS; SOIL ORGANIC MATTERS; SOIL SAMPLE; SOIL STRUCTURAL STABILITY; SOXHLET APPARATUS; STABLE AGGREGATES;

ACETONITRILE; AGRICULTURE; BIOGEOCHEMISTRY; BIOLOGICAL MATERIALS; DICHLOROMETHANE; ESTERS; HEXANE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHOBICITY; LIQUIDS; ORGANIC SOLVENTS; QUALITY CONTROL; SOILS; STABILITY;

SOLVENT EXTRACTION;

AGRICULTURAL LAND; HYDROPHOBICITY; LIQUID CHROMATOGRAPHY; ORGANIC FARMING; PH; SANDY CLAY LOAM; SOIL ANALYSIS; SOIL MANAGEMENT; SOIL ORGANIC MATTER; SOIL STRUCTURE; SOLVENT;

ITALY;

EID: 77955058258     PISSN: 01671987     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.still.2010.04.004     Document Type: Article

References (41)

1. AOAC method 920.151. 1990. Official methods of analysis (15th ed.). Arlington, VA: Association of Official Analytical Chemists.
2. Almendros G., Guadalix M.E., Gonzalez-Vila F.J., Martin F. Preservation of aliphatic macromolecules in soil humins. Org. Geochem. 1996, 24:651-659.
3. Bachmann J., Guggenberger G., Baumgartl T., Ellerbrock R.H., Urbanek E., Goebel M.-O., Kaiser K., Fischer W.R. Physical carbon-sequestration mechanisms under special consideration of soil wettability. J. Plant Nutr. Soil Sci. 2008, 171(1):14-26.
4. Barwick V.J. Strategies for solvent selection-a literature review. Trends Anal. Chem. 1997, 16(6):293-309.
5. Capriel P. Hydrophobicity of the organic matter in arable soils: influence of management. Eur. J. Soil Sci. 1997, 48:457-462.
6. Conte P., Piccolo A. Conformational arrangement of dissolved humic substances. Influence of solution composition on association of humic molecules. Environ. Sci. Technol. 1999, 33:1682-1690.
7. Corradini D., Grego S., Liburdi K., Marinari S., Tonci M. A combined approach employing Soxhlet extraction and linear gradient elution reversed-phase HPLC for the fingerprinting of soil organic matter according to hydrophobicity. Chromatography 2006, 63:S11-S16.
8. Dinel H., Schnitzer M., Mehuys G.R. Soil lipids: origin, nature, content, decomposition and effect on soil physical properties. Soil Biochemistry 1990, 397-429. Marcel Dekker Inc., New York. J.-M. Bollag, G. Stotzky (Eds.).
9. Doran J.W. Soil microbial and biochemical changes associated with reduced tillage. Soil Sci. Soc. Am. 1980, 44:765-771.
10. Feng G., Runyi Y. New approach on similarity analysis of chromatographic fingerprint of herbal medicine. J. Chromatogr. A 2006, 1104:100-105.
11. Franco C.M.M., Tate M.E., Oades J.M. Studies on non-wetting sands. I. The role of intrinsic particulate organic matter in the development of water-repellency in non-wetting sands. Aust. J. Soil Res. 1995, 33:253-263.
12. Guggenberger G., Zech W., Schulten H.R. Formation and mobilization pathway of dissolved organic matter: evidence from chemical structural studies of organic matter fractions in acid forest floor solution. Org. Geochem. 1994, 21:51-66.
13. Hanza M.A., Anderson W.K. Soil compaction in cropping systems: a review of the nature, causes and possible solutions. Soil Till. Res. 2005, 82:121-145.
14. Horne D.J., McIntosh J.C. Hydrophobic compounds in sands in New Zealand-extraction, characterization and proposed mechanisms for repellency expression. J. Hydrol. 2000, 231:35-46.
15. ISO 659, 1988 (E). Intern. Org. Stand.
16. Huang W., Peng P., Yu Z., Fu J. Effects of organic matter heterogeneity on sorption and desorption of organic contaminants by soils and sediments. Appl. Geochem. 2003, 18(7):955-972.
17. Jouany C. Surface free energy components of clay-synthetic humic acid complex from contact angle measurement. Clays Clay Miner. 1991, 39:43-49.
18. 13C-enrichment of organic components from wheat crop soils: evidence for the in situ origin of soil organic matter. Org. Geochem. 1995, 23:865-868.
19. Marinari S., Liburdi K., Masciandaro G., Ceccanti B., Grego S. Humification-mineralization pyrolytic indices and carbon fractions of soil under organic and conventional management in central Italy. Soil Till. Res. 2007, 92(1-2):10-17.
20. Marinari S., Mancinelli R., Campiglia E., Grego S. Chemical and biological indicators of soil quality in organic and conventional farming systems in Central Italy. Ecol. Ind. 2006, 6:701-711.
21. McKissock I., Gilkes R.J., van Bronswijk W. The relationship of water repellency to aliphatic C and kaolin measured using DRIFT. Aust. J. Soil Res. 2003, 41:251-265.
22. Melnitchouck A., Leinweber P., Eckhardt K.U., Beese R. Qualitative differences between day- and night-time rhizodeposition in maize (Zea mays L.) as investigated by pyrolysis-field ionization mass spectrometry. Soil Biol. Biochem. 2005, 37:155-162.
23. Michel J.C., Rivière L.M., Bellon-Fontaine M.N. Measurement of the wettably of organic materials in relation to water content by the capillary rise method. Eur. J. Soil Sci. 2001, 52:459-468.
24. Miller R.H., Wilkinson J.F. Nature of soil organic coating on sand grains of non wettable golf greens. Soil Sci. Soc. Am. J. 1977, 41:1203-1204.
25. Murage E.W., Karauja N.K., Smithson P.C., Woomer P.L. Diagnostic indicators of soil quality in productive and non-productive small-holders fields of Kenya's Central Highlands. Agric. Ecosyst. Environ. 2000, 79:1-8.
26. Piccolo A., Spaccini R., Haberhauer G., Gerzabek M.H. Increased sequestration of organic carbon in soil by hydrophobic protection. Naturwissenschaften 1999, 86:496-499.
27. Piccolo A. Metodi chimici e spettroscopici per lo studio della struttura e reattività della sostanza organica del suolo. Ciclo della Sostanza Organica nel Suolo: Aspetti Agronomici Chimici Ecologici e Selvicolturali 1993, 247-303. Pàtron, Bologna, Italy. P. Nannipieri (Ed.).
28. Piccolo A. Humus and soil conservation. Humic Substances in Terrestrial Ecosystems 1996, 225-264. Elsevier, Amsterdam, Netherlands. A. Piccolo (Ed.).
29. Qualls R., Hines B.L. Geochemistry of dissolved organic nutrient in water percolating through a forest ecosystem. Soil Sci. Soc. Am. J. 1991, 55:1112-1123.
30. Sihufe G.A., Zorrilla S.E., Rubiolo A.C. The effects of trichloroacetic acid on water-soluble fractions from Fynbo cheese. Food Chem. 2005, 93:305-310.
31. Šimon T. Characterization of soil organic matter in long-term fallow experiment with respect to the soil hydrophobicity and wettability. Soil Water Res. 2007, 2:96-103.
32. Šimon T., Javůrek M., Mikanová O., Vach M. The influence of tillage systems on soil organic matter and soil hydrophobicity. Soil Till. Res. 2009, 105:44-48.
33. Snyder L.R. Classification of the solvent properties of common liquids. J. Chromatogr. Sci. 1978, 16:223-234.
34. Spaccini R., Piccolo A., Conte P., Haberhauer G., Gerzabek M.H. Increased soil organic carbon sequestration through hydrophobic protection by humic substances. Soil Biol. Biochem. 2002, 34:1839-1851.
35. 13C distribution and CPMAS-NMR spectra. Eur. J. Soil Sci. 2000, 51:583-594.
36. Stevenson F.J. Humus Chemistry: Genesis, Composition, Reactions 1994, John Wiley and Sons, New York. 2nd ed.
37. Tschapek M., Pozzo Ardizzi J., Bussetti S.G.D. Wettability of humic acid and its salts. Zeitschrift für Pflanzenernährung und Bodenkunde 1973, 135:16-31.
38. US EPA Method 8100, 1986. US Government Printing Office, Washington, DC, USA.
39. Wardle D.A. Community and Ecosystems. Linking the Aboveground and Belowground Components 2002, Princeton University Press, Princeton.
40. Watson C.A., Atkinson D., Gosling P., Jackson L.R., Rayns F.W. Managing soil fertility in organic farming systems. Soil Use Manage. 2002, 18:239-247.
41. Wiesenberg G.L.B., Schwark L., Schmidt M.W.I. Improved automated extraction and separation procedure for soil lipid analyses. Eur. J. Soil Sci. 2004, 55:349-355.