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77954217428
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note
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4: C, 15.04%; H, 1.44%; N, 37.58%. Found: C, 14.95%; H, 1.35%; N, 37.68%. IR (solid KBr pellet/cm-1): 3480(m), 3452(s), 3345(m), 3211(m), 3040(m), 1626(s), 1591(s), 1513(s), 1443(m), 1427(m), 1295(w), 1218(m), 1131(m), 1075 (m), 1017(m), 841(m), 812(m), 750(m), 726(s), 638(s), 447(m). Caution! Sodium azide is potentially explosive, and it should be handled with care.
-
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47
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77954216105
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note
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eq(C) for phenylene ring. In this structure, the phenylene rings is located on a twofold axis, causing a twofold disorder over two positions with equal site occupancy. Additionally, large voids were found in this structure resulting in the disorder of phenylene rings when no other solvent molecules were filled in the voids.
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