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Crystallographic data for 3 have been deposited with the Cambridge Crystallographic Data Centre (deposition number CCDC 759772). Copies of the data can be obtained, free of charge, on application to the director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: +44 1223 336033 or e-mail: deposit@ccdc.cam.ac.uk)
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