Dynamic nuclear polarization experiments at 14.1 T for solid-state NMR

Physical Chemistry Chemical Physics

Volumn 12, Issue 22, 2010, Pages 5799-5803

  Matsuki, Yoh ^a   Takahashi, Hiroki ^a   Ueda, Keisuke ^a   Idehara, Toshitaka ^b   Ogawa, Isamu ^b   Toda, Mitsuru ^b   Akutsu, Hideo ^a   Fujiwara, Toshimichi ^a  

^a OSAKA UNIVERSITY   (Japan)

^b UNIVERSITY OF FUKUI   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

1 (TEMPO 4 OXY) 3 (TEMPO 4 AMINO)PROPAN 2 OL; 1-(TEMPO-4-OXY)-3-(TEMPO-4-AMINO)PROPAN-2-OL; AMINE OXIDE; CARBON; PROPANOL;

ARTICLE; CHEMISTRY; INSTRUMENTATION; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; TEMPERATURE;

CARBON ISOTOPES; CYCLIC N-OXIDES; MAGNETIC RESONANCE SPECTROSCOPY; PROPANOLS; TEMPERATURE;

EID: 77952930300     PISSN: 14639076     EISSN: None     Source Type: Journal    
DOI: 10.1039/c002268c     Document Type: Article

References (16)

1. I. Bertini, A. Bhaumik, G. D. Paëpe, R. G. Griffin, M. Lelli, J. R. Lewandowski, C. Luchinat, High-resolution solid-state NMR structure of a 17.6 kDa protein J. Am. Chem. Soc., 2010, 132, 1032-1040
2. A. Egawa, T. Fujiwara, T. Mizoguchi, Y. Kakitani, Y. Koyama, H. Akutsu, Structure of the light-harvesting bacteriochlorophyll c assembly in chlorosomes from chlorobium Limicola determined by solid-state NMR Proc. Natl. Acad. Sci. U. S. A., 2007, 104, 790-795
3. +-ATP synthase subunit c, by magic-angle spinning solid-state NMR J. Biomol. NMR, 2006, 36, 279-293
4. 2-microglobulin fragment probed by solid-state NMR Proc. Natl. Acad. Sci. U. S. A., 2006, 103, 18119-18124
5. T. Fujiwara, A. Ramamoorthy, How far can the sensitivity of NMR be increased? Annu. Rep. Nucl. Magn. Reson. Spectrosc., 2006, 58, 155-175
6. L. R. Becerra, G. J. Gerfen, B. F. Bellew, J. A. Bryant, D. A. Hall, S. J. Inati, R. T. Weber, S. Un, T. F. Prisner, A. E. McDermott, K. W. Fishbein, K. E. Kreisher, R. J. Temkin, D. J. Singel, R. G. Griffin, A Spectrometer for dynamic nuclear polarization and electron paramagnetic resonance at high frequencies J. Magn. Reson., Ser. A, 1995, 117, 28-40
7. V. S. Bajaj, M. K. Hornstein, K. E. Kreischer, J. R. Sirigiri, P. P. Woskov, M. L. Mak-Jurkauskas, J. Herzfeld, R. J. Temkin, R. G. Griffin, 250 GHz CW gyrotron oscillator for dynamic nuclear polarization in biological solid state NMR J. Magn. Reson., 2007, 189, 251-279
8. C. T. Farrar, D. A. Hall, G. J. Gerfen, S. J. Inati, R. G. Griffin, Mechanism of dynamic nuclear polarization in high magnetic fields J. Chem. Phys., 2001, 114, 4922-4933
9. T. Maly, G. T. Debelouchina, V. S. Bajaj, K.-N. Hu, C.-G. Joo, M. L. Mak-Jurkauskas, J. R. Sirigiri, P. C. A. van der Wel, J. Herzfeld, R. J. Temkin, R. G. Griffin, Dynamic nuclear polarization at high magnetic fields J. Chem. Phys., 2008, 128, 052211.
10. S. Sabchevski, T. Idehara, S. Mitsudo, T. Fujiwara, Conceptual design study of a novel gyrotron for NMR/DNP spectroscopy Int. J. Infrared Millimeter Waves, 2005, 26, 1241-1264
11. T. Idehara, I. Ogawa, La Agusu T. Kanamaki, S. Mitsudo, T. Saito, T. Fujiwara, H. Takahashi, Development of 394.6 GHz CW gyrotron (gyrotron FU CW II) for 600 MHz DNP/proton NMR Int. J. Infrared Millimeter Waves, 2007, 28, 433-442
12. La Agusu T. Idehara, I. Ogawa, T. Saito, T. Kanamaki, H. Takahashi, T. Fujiwara, Detailed consideration of experimental results of gyrotron FUCW II developed as a radiation source for DNP-NMR spectroscopy Int. J. Infrared Millimeter Waves, 2007, 28, 499-511
13. 79Br in KBr powder J. Magn. Reson., 2009, 196, 84-87
14. V. A. Atsarkin, Dynamic polarization of nuclei in solid dielectrics Sov. Phys. Usp., 1978, 21, 725-745
15. P. P. Woskov, V. S. Bajaj, M. K. Hornstein, R. J. Temkin, R. G. Griffin, Corrugated waveguide and directional coupler for CW 250 GHz gyrotron DNP experiments IEEE Trans. Microwave Theory Tech., 2005, 53, 1863-1869
16. Y. Matsuki, T. Maly, O. Ouari, H. Karoui, F. Le Moigne, E. Rizzato, S. Lyubenova, J. Herzfeld, T. Prisner, P. Tordo, R. G. Griffin, Dynamic nuclear polarization using a rigid biradical Angew. Chem., Int. Ed., 2009, 48, 4996-5000