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Crystal structure determination of [ZnL.DMF]DMF: the crystal was mounted with grease on a glass pin which was fixed on the goniometer head. The X-ray data were collected on a Xcalibur 3 diffractometer from Oxford diffraction. The structure was solved by direct methods using the WinGX-package [L.J. Farrugia, J. Appl. Cryst. 32 (1999, 837; (b) G.M. Sheldrick, SHELX-97, Program for the Refinement of Crystal Structures, University of Göttingen, Göttingen (Germany, 1997] and refined by on F2 by full matrix least-squares with SHELX-97, Parkin, B. Moezzi, H. Hope, J. Appl. Cryst. 28 (1995) 53, All the hydrogen atoms were placed on calculated positions and refined using a riding model. Empirical formula C32H28N6O4Zn, Temperature 170(2)K, Monoclinic, P21/n, Unit cell dimension: a, 5.7764(4) Å, b, 35.119(3) Å, c, 14.563(1) Å, β, 96.090(7)°; Z, 4, absorption coefficient 0.88
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