-
3
-
-
31944452077
-
-
Huang Y.B., Chen J.X., Lan T.Y., Lu X.Q., Wei C.X., Li Z.S., and Zhang Z.C. J. Mol. Struct. 783 (2006) 168
-
(2006)
J. Mol. Struct.
, vol.783
, pp. 168
-
-
Huang, Y.B.1
Chen, J.X.2
Lan, T.Y.3
Lu, X.Q.4
Wei, C.X.5
Li, Z.S.6
Zhang, Z.C.7
-
4
-
-
67651039728
-
-
Chen L.F., Hu J.C., Mal S.S., Kortz U., Jaensch H., Mathys G., and Richards R.M. Chem. Eur. J. 15 (2009) 7490
-
(2009)
Chem. Eur. J.
, vol.15
, pp. 7490
-
-
Chen, L.F.1
Hu, J.C.2
Mal, S.S.3
Kortz, U.4
Jaensch, H.5
Mathys, G.6
Richards, R.M.7
-
5
-
-
0035819645
-
-
Judd D.A., Nettles J.H., Nevins N., Snyder J.P., Liotta D.C., Tang J., Ermolieff J., Schinazi R.F., and Hill C.L. J. Am. Chem. Soc. 123 (2001) 886
-
(2001)
J. Am. Chem. Soc.
, vol.123
, pp. 886
-
-
Judd, D.A.1
Nettles, J.H.2
Nevins, N.3
Snyder, J.P.4
Liotta, D.C.5
Tang, J.6
Ermolieff, J.7
Schinazi, R.F.8
Hill, C.L.9
-
8
-
-
36248982556
-
-
Hasegawa T., Kasahara Y., Yoshida S., Kurashina T., Aoki S., Yoza K., and Nomiya K. Inorg. Chem. Commun. 10 (2007) 1416
-
(2007)
Inorg. Chem. Commun.
, vol.10
, pp. 1416
-
-
Hasegawa, T.1
Kasahara, Y.2
Yoshida, S.3
Kurashina, T.4
Aoki, S.5
Yoza, K.6
Nomiya, K.7
-
9
-
-
0142042819
-
-
Chambers R.C., Osburn Atkinson E.J., McAdams D., Hayden E.J., and Ankeny Brown D.J. Chem Commun. (2003) 2456
-
(2003)
Chem Commun.
, pp. 2456
-
-
Chambers, R.C.1
Osburn Atkinson, E.J.2
McAdams, D.3
Hayden, E.J.4
Ankeny Brown, D.J.5
-
12
-
-
28244435756
-
-
Laurencin D., Villanneau R., Herson P., Thouvenot R., Jeannin Y., and Proust A. Chem. Commun. (2005) 5524
-
(2005)
Chem. Commun.
, pp. 5524
-
-
Laurencin, D.1
Villanneau, R.2
Herson, P.3
Thouvenot, R.4
Jeannin, Y.5
Proust, A.6
-
14
-
-
0001696992
-
-
Keana J.F.W., Ogan M.D., Lu Y.X., Beer M., and Varkey J. J. Am. Chem. Soc. 108 (1986) 7957
-
(1986)
J. Am. Chem. Soc.
, vol.108
, pp. 7957
-
-
Keana, J.F.W.1
Ogan, M.D.2
Lu, Y.X.3
Beer, M.4
Varkey, J.5
-
16
-
-
0042029693
-
-
Bareyt S., Piligkos S., Hasenknopf B., Gouzerh P., Lacte E., Thorimbert S., and Malacria M. Angew. Chem. Int. Ed. 42 (2003) 3404
-
(2003)
Angew. Chem. Int. Ed.
, vol.42
, pp. 3404
-
-
Bareyt, S.1
Piligkos, S.2
Hasenknopf, B.3
Gouzerh, P.4
Lacte, E.5
Thorimbert, S.6
Malacria, M.7
-
17
-
-
18644372125
-
-
Bareyt S., Piligkos S., Hasenknopf B., Gouzerh P., Lacte E., Thorimbert S., and Malacria M. J. Am. Chem. Soc. 127 (2005) 6788
-
(2005)
J. Am. Chem. Soc.
, vol.127
, pp. 6788
-
-
Bareyt, S.1
Piligkos, S.2
Hasenknopf, B.3
Gouzerh, P.4
Lacte, E.5
Thorimbert, S.6
Malacria, M.7
-
18
-
-
41549114182
-
-
Boglio C., Micoine K., Derat E., Thouvenot R., Hasenknopf B., Thorimbert S., Lacôte E., and Malacria M. J. Am. Chem. Soc. 130 (2008) 4553
-
(2008)
J. Am. Chem. Soc.
, vol.130
, pp. 4553
-
-
Boglio, C.1
Micoine, K.2
Derat, E.3
Thouvenot, R.4
Hasenknopf, B.5
Thorimbert, S.6
Lacôte, E.7
Malacria, M.8
-
19
-
-
70349972722
-
-
Micoine K., Hasenknopf B., Thorimbert S., Lacôte E., and Malacria M. Angew. Chem. Int. Ed. 48 (2009) 3466
-
(2009)
Angew. Chem. Int. Ed.
, vol.48
, pp. 3466
-
-
Micoine, K.1
Hasenknopf, B.2
Thorimbert, S.3
Lacôte, E.4
Malacria, M.5
-
27
-
-
34547199031
-
-
Nahum I.B., Ettedgui J., Konstantinovski L., Kogan V., and Neumann R. Inorg. Chem. 46 (2007) 5798
-
(2007)
Inorg. Chem.
, vol.46
, pp. 5798
-
-
Nahum, I.B.1
Ettedgui, J.2
Konstantinovski, L.3
Kogan, V.4
Neumann, R.5
-
28
-
-
60849096663
-
-
Piedra-Garza L.F., Dickman M.H., Moldovan O., Breunig H.J., and Kortz U. Inorg. Chem. 48 (2009) 411
-
(2009)
Inorg. Chem.
, vol.48
, pp. 411
-
-
Piedra-Garza, L.F.1
Dickman, M.H.2
Moldovan, O.3
Breunig, H.J.4
Kortz, U.5
-
30
-
-
0000224706
-
-
Wang X.H., Liu J.F., Chen Y.G., Liu Q., Liu J.T., and Pope M.T. J. Chem. Soc., Dalton Trans. 1139 (2000)
-
(2000)
J. Chem. Soc., Dalton Trans.
, vol.1139
-
-
Wang, X.H.1
Liu, J.F.2
Chen, Y.G.3
Liu, Q.4
Liu, J.T.5
Pope, M.T.6
-
32
-
-
39649091874
-
-
Li J.X., Zhai F.Y., Wang X.H., Li E.M., Zhang S.D., Zhang Q.L., and Du X.G. Polyhedron 27 (2008) 1150
-
(2008)
Polyhedron
, vol.27
, pp. 1150
-
-
Li, J.X.1
Zhai, F.Y.2
Wang, X.H.3
Li, E.M.4
Zhang, S.D.5
Zhang, Q.L.6
Du, X.G.7
-
39
-
-
0008452374
-
-
Krebs B., Droste E., Piepenbrink M., and Vollmer G. C.R. Acad. Sci. Paris, Serie IIc, Chimie: Chemistry 3 (2000) 205
-
(2000)
C.R. Acad. Sci. Paris, Serie IIc, Chimie: Chemistry
, vol.3
, pp. 205
-
-
Krebs, B.1
Droste, E.2
Piepenbrink, M.3
Vollmer, G.4
-
40
-
-
12544259703
-
-
Gerth H.U.V., Rompel A., Krebs B., Boos J., and Lanvers-Kaminsky C. Anti-Cancer Drugs 16 (2005) 101-106
-
(2005)
Anti-Cancer Drugs
, vol.16
, pp. 101-106
-
-
Gerth, H.U.V.1
Rompel, A.2
Krebs, B.3
Boos, J.4
Lanvers-Kaminsky, C.5
-
41
-
-
43149125181
-
-
Dolbecq A., Compain J.D., Mialane P., Marrot J., Rivière E., and Sécheresse F. Inorg. Chem. 47 (2008) 3371
-
(2008)
Inorg. Chem.
, vol.47
, pp. 3371
-
-
Dolbecq, A.1
Compain, J.D.2
Mialane, P.3
Marrot, J.4
Rivière, E.5
Sécheresse, F.6
-
42
-
-
0001099470
-
-
Loose I., Droste E., Bösing M., Pohlmann H., Dickman M.H., Rosu C., Pope M.T., and Krebs B. Inorg. Chem. 38 (1999) 2688
-
(1999)
Inorg. Chem.
, vol.38
, pp. 2688
-
-
Loose, I.1
Droste, E.2
Bösing, M.3
Pohlmann, H.4
Dickman, M.H.5
Rosu, C.6
Pope, M.T.7
Krebs, B.8
-
45
-
-
77952104162
-
-
α-Na9[SbW9O33]{bullet operator}19.5H2O was synthesized according to the literature and characterized by IR spectrum [11a, Organotins Cl3Sn(CH2)2COOCH3 and Cl3SnCH2CH(CH3)COOCH3 were prepared by the literature and characterized by IR [13b, Synthesis of 1. 0.62 g Cl3Sn(CH2)2COOCH3 (2.0 mmol) was dissolved in 10.0 mL H2O to form solution A, and 2.84 g Na9[SbW9O33]·19.5H2O (1.0 mmol) was dissolved in 10.0 mL H2O to form solution B. Then, solution A was added dropwise to solution B. The resulting solution was sealed in a 50 mL-beaker and stirred for 26 h at room temperature. After filtration, 3.16 g KCl solid was added to the filtrate, and white precipitate was immediately obtained. The white crude product was collected by filtration and
-
-1): 1624(s), 1310(w), 1266(s), 954(s), 852(sh), 802(s), 750(s), 526(w), 479(w), and 439(s).
-
-
-
-
46
-
-
77952103460
-
-
The crystal data were collected at 298 K on a Bruker Smart APEX II X-diffractometer equipped with graphite monochromated Mo-Kα radiation (λ, 0.71073 Å, An empirical absorption correction was applied using the SADABS program. The structure was solved by the direct method and refined by full-matrix least squares on F2 using the SHELXL-97 software [16, Cell parameters were obtained by the global refinement of the positions of all collected reflections. All the non-hydrogen atoms were refined anisotropically. Hydrogen atoms on C atoms were added in calculated positions. The crystal data and structure refinements of compounds 1 and 2 are summarized in Table S1. Selected bond lengths and angles are listed in Table S2 and S3. Crystal data for 1: C12H48K4Na6O90Sb2Sn4W18, M, 5954.32, Triclinic, space group Pī, a, 11.9767(15) Å, b, 12.5712(15) Å, c, 17.38
-
- 3, R1(wR2) = 0.0677 (0.1824) and S = 1.019 for 8291 independent reflections with I > 2σ(I). CCDC reference numbers: 741327 for 1 and 751985 for 2.
-
-
-
-
48
-
-
77952105791
-
-
Elemental analyses (H and C) were performed on a Perkin-Elmer 2400CHN elemental analyzer. W, Sb, Sn, K and Na were analyzed on a PLASMA-SPEC-II, LEEMAN(USA) ICP atomic emission spectrometer. IR spectra were recorded in the range of 4000-220 cm-1 on a JASCO FT-IR-480 spectrophotometer using KBr pellets. TG analyses were performed on a Pyris Diamond TG/DTA instrument in flowing N2 with a heating rate of 10 °C min-1. Electrochemical measurements were carried out on a CHI 604B electrochemical workstation at room temperature. The working electrode was the glassy carbon electrode. A platinum wire was used as the counter electrode and an Ag/AgCl (3 M KCl) was the reference electrode. In anti-tumor experiments, the cells were cultured in 1640 supplemented with 10% FCS, and maintained in 5% CO2 at 37 °C.In MTT assays, a sample was dissolved in 10% FCS and filtered through a 0.22 μm pore filtration membrane. The concent
-
2 at 37 °C.In MTT assays, a sample was dissolved in 10% FCS and filtered through a 0.22 μm pore filtration membrane. The concentration of stock 1 was adjusted to 10, 50, 100, 500 or 1000 μg/mL for 48 h and followed by a four-hour-incubation with MTT. The MTT transformed crystals were dissolved in dimethyl sulfoxide, and absorbance at 490 nm was measured using a microplate reader.
-
-
-
|