An improved headspace solid-phase microextraction method for the analysis of free-base nicotine in particulate phase of mainstream cigarette smoke

Analytica Chimica Acta

Volumn 663, Issue 1, 2010, Pages 49-54

  Bao, Mingliang ^a   Joza, Peter ^a   Rickert, William S ^a   Lauterbach, John H ^b  

^a Labstat International ULC   (Canada)

^b Lauterbach and Associates LLC   (United States)

Author keywords

Cigarette; Free base nicotine; Gas chromatography; Headspace; Mainstream tobacco smoke; Solid phase microextraction

Indexed keywords

CIGARETTE SMOKES; CORRECTION FACTORS; EXTRACTION TIME; FIBER TYPES; GC/MS ANALYSIS; GLASS FIBER FILTERS; HEADSPACE; HEADSPACE SOLID PHASE MICROEXTRACTION; HEADSPACES; HS-SPME; IMPROVED METHODS; KENTUCKY; MAINSTREAM CIGARETTE SMOKE; SIGNIFICANT IMPACTS; SOLID-PHASE MICROEXTRACTION; TOBACCO SMOKE;

FLOW PATTERNS; GAS CHROMATOGRAPHY; GLASS FIBERS; HYDRAULIC STRUCTURES; PYRIDINE; SMOKE; TOBACCO; WATER CONTENT;

EXTRACTION;

NICOTINE; SOLVENT; WATER;

ACCURACY; ANALYTIC METHOD; ARTICLE; CIGARETTE SMOKING; CONCENTRATION (PARAMETERS); FIBER; PRIORITY JOURNAL; SOLID PHASE MICROEXTRACTION; STATISTICAL MODEL; TEMPERATURE; TIME;

GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GASES; NICOTINE; PARTICLE SIZE; SMOKE; SOLID PHASE MICROEXTRACTION; TEMPERATURE; TIME FACTORS; TOBACCO; WATER;

NICOTIANA TABACUM;

EID: 77951619965     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2010.01.036     Document Type: Article

References (22)

1. Wayne G.F., Connolly G.N., Henningfield J.E. Tobacco Control 2006, 15:189-198.
2. Ashley D.L., Pankow J.F., Tavakoli A.D., Watson C.H. Nicotine Psychopharmacology, Handbook of Experimental Pharmacology 2009, vol. 192:437-456. Springer-Verlag, Berlin/Heidelberg.
3. Armitage A.K., Turner D.K. Nature 1970, 226:1231-1233.
4. Schievelbein H., Eberhardt R., Loschenkohl K., Rahlfs V., Bedall F.K. Agents Actions 1973, 3/4:254-258.
5. Henningfield J.E., Keenan R.M. J. Consult. Clin. Psychol. 1993, 61:743-750.
6. Morie G.P. Tobacco Sci. 1972, 16:167-168.
7. Brunnemann K.D., Hoffmann D. Food Cosmet. Toxicol. 1974, 12:115-124.
8. M.S. Frank, Standard Method Number SM-92: Procedure for the Determination of Extractable Nicotine in Cigarette Smoke. (accessed 25.07.79). http://www.tobaccodocuments.org/product_design/376373.html.
9. B.J. Ingebrethsen, C.S. Lyman, W.M. Coleman, P.R. Nelson, Smoke Nicotine " Volatility" Measurement Methods, (accessed 28.08.91). http://www.tobaccodocuments.org/rjr/508276435-6446.html.
10. Lewis D.A., Colbeck I., Mariner D.C. Anal. Chem. 1994, 66:3525-3527.
11. Ingebrethsen B.J., Lyman C.S., Risner C.H., Partom P., Gordon B.M. Aerosol. Sci. Technol. 1999, 35:874-886.
12. Pankow J.F., Tavakoli A.D., Luo W., Isabelle L.M. Chem. Res. Toxicol. 2003, 16:1014-1018.
13. Watson C.H., Trommel J.S., Ashley D.L. J. Agric. Food Chem. 2004, 52:7240-7245.
14. Clark T.J., Bunch J.E. J. Agri. Food Chem. 1997, 45:844-849.
15. Stanfill S.B., Ashley D.L. J. Chromatogr. A 1999, 858:79-89.
16. Watson C.H., Ashley D.L. J. Chromatogr. Sci. 2000, 38:137-144.
17. Yang S.S., Huang C.B., Smetena I. J. Chromatogr. A 2002, 942:33-39.
18. Merckel C., Pragst F., Ratzinger A., Aebi B., Bernhard W., Sporkert F. J. Chromatogr. A 2006, 1116:10-19.
19. Pieraccini G., Furlanetto S., Orlandini S., Bartolucci G., Giannini I., Pinzauti S., Moneti G. J. Chromatogr. A 2008, 1180:138-150.
20. Health Canada Health Canada tobacco reporting regulations. Part 3: Emissions from designated tobacco products. Canada Gazette Part II 2000, 134.
21. Lestremau F., Desauziers V., Roux J.C., Fanlo J.L. J. Chromatogr. A 2003, 999:71-81.
22. Bao M.L., Griffini O., Burrini D., Santianni D., Barbieri K., Mascini M. Analyst 1999, 124:459-466.