Optimization of synthesis parameters in interfacial polycondensation using design of experiments

Polymer Bulletin

Volumn 64, Issue 3, 2010, Pages 303-314

  Iliescu, Smaranda ^a   Grozav, Ion ^c   Funar Timofei, Simona ^a   Plesu, Nicoleta ^a   Popa, Adriana ^a   Ilia, Gheorghe ^a,b  

^a ACADEMY OF ROMANIAN SCIENTISTS   (Romania)

^b WEST UNIVERSITY OF TIMISOARA   (Romania)

^c POLITEHNICA UNIVERSITY OF TIMISOARA   (Romania)

Author keywords

Design of experiments; Gas liquid; Interfacial polycondensation

Indexed keywords

ALKALINE MEDIUM; DESIGN OF EXPERIMENTS METHODS; GAS LIQUIDS; INHERENT VISCOSITY; INTERFACIAL POLYCONDENSATION; MOLAR RATIO; REACTION CONDITIONS; REACTION TEMPERATURE; REACTION TIME; SYNTHESIS PARAMETERS;

DESIGN OF EXPERIMENTS; LIQUIDS; POLYCONDENSATION;

SYNTHESIS (CHEMICAL);

EID: 77951482525     PISSN: 01700839     EISSN: None     Source Type: Journal    
DOI: 10.1007/s00289-009-0212-2     Document Type: Article

References (23)

1. Cortés MT, Sierra EV (2006) Effect of synthesis parameters in polyaniline: influence on yield and thermal behavior. Polym Bull 56:37-45
2. Ramos VD, da Costa HM, Pereira AO, Rocha MCG, Gomes AS (2005) Effect of peroxide concentration on the modification of the LLDPE: statistical experimental design and thermal properties. Polym Bull 54:117-122
3. da Costa HM, Ramos VD, Visconte LLY, Furtado CRG (2007) Design and analysis of single-factor experiments: analysis of variance of the effect of rice husk ash and commercial fillers in NR compounds. Polym Bull 58:597-610
4. Makoska M (2000) A general green methodology in organic synthesis. Pure Appl Chem 72:1399-1403
5. Millich F, Lambing LL (1980) Interfacial synthesis of polyphosphonate and polyphosphate esters. VII. Temperature effects and reaction loci in polycondensations of hydroquinone with phenylphosphonic dichloride and 4-methylthiophenil phosphorodichloridate. J Polym Sci Polym Chem Ed 18:2155-2162
6. Imai Y, Kamata H, Kakimoto M-A (1984) Preparation and properties of high transition temperature aromatic polyphosphonates by phase-transfer-catalyzed polycondensation of phenylphosphonic dichloride with bisphenols. J Polym Sci Polym Chem Ed 22:1259-1265
7. Richards M, Dahiyat BI, Arm DM, Lin S, Leong KW (1991) Interfacial polycondensation and characterization of polyphosphates and polyphosphonates. J Polym Sci A Polym Chem 29:1157-1165
8. Roy S, Maiti S (2001) Synthesis and characterization of unsaturated polyphosphonates. J Polym Mater 17:267-282
9. Senthil S, Kannan P (2002) Synthesis and characterization of liquid-liquid-crystalline polyphosphonates containing disubstituted ferrocene esters as mesogens. J Polym Sci A Poly Chem 40:2256-2263
10. Narendran N, Kishore K (2003) Studies on polyphosophate esters synthesis. J Appl Polym Sci 87:626-631
11. Huang X, Li B, Shi B, Li L (2008) Investigation on interfacial interaction of flame retarded and glass fiber reinforced PA66 composites by IGC/DSC/SEM. Polymer 49:1049-1055
12. Lyon RE, Takemori MT, Safronava N, Stoliarov SI, Walters RN (2009) A molecular basis for polymer flammability. Polymer 50:2608-2617
13. Iliescu S, Ilia G, Dehelean G, Popa A (2002) New polyphosphonates obtained by vapor-liquid interfacial polycondensation. Polym Bull 48:451-456
14. Iliescu S, Ilia G, Popa A, Dehelean G, Pascariu A, Macarie L, Plesu N (2004) Mixed quaternary ammonium and phosphonium salts bound to macromolecular supports for removal bacteria from water. Mol Cryst Liq Cryst 418:195-203
15. Iliescu S, Ilia G, Plesu N, Popa A, Pascariu A (2006) Solvent and catalyst-free synthesis of polyphosphates. Green Chem 8:727-730
16. Iliescu S, Ilia G, Pascariu A, Popa A, Plesu N (2007) Organic solvent-free synthesis of phosphorus containing polymers. Pure Appl Chem 79:1879-1884
17. Suh NP (2001) Axiomatic design advances and applications. Oxford University Press, New York
18. Miron M, Grozav I, Todea C (2004) Notiuni fundamentale de metodologia cercetarii stiintifice medicale (Fundamental notions on research methodology in medical science). Marineasa, Timisoara
19. Montgomery DC (1991) Design and analyses of experiments, 3rd edn. Wiley, New York
20. Jiju A (2003) Design of experiments for engineers and scientists. Elsevier, Burlington
21. Grozav I, Turc C, Banciu F (2007) The optimization of the soldering process through experiment design. In: Weiss Z (ed) Virtual design and automation. Publishing House of University of Technology, Poznan, pp 407-414
22. Hinkelmann K, Kemthorne O (2005) Design and analyses of experiments. Wiley, New York
23. MINITAB v. 15, Minitab Inc., USA.http://www.minitab.com/products/minitab/