A fully automatic apparatus for thermal analysis of crystallization from solution and metastable zone width determinations

Journal of Thermal Analysis and Calorimetry

Volumn 100, Issue 2, 2010, Pages 493-500

  Bernardes, Carlos E S ^a   Da Piedade, Manuel E Minas ^a  

^a UNIVERSITY OF LISBON   (Portugal)

Author keywords

Ammonium chloride; Crystallization; Metastable zone width; Solubility; Thermal analysis; Turbidity

Indexed keywords

CHLORINE COMPOUNDS; CRYSTALLIZATION; MIXTURES; SOLUBILITY; TURBIDITY;

AMMONIUM CHLORIDE; COMPLETE DISSOLUTION; CRYSTALLIZATION PROCESS; CRYSTALLIZATION VESSELS; EQUILIBRIUM SOLUBILITIES; HEATING AND COOLING; METASTABLE ZONE WIDTH; POLYTHERMAL METHODS;

THERMOANALYSIS;

EID: 77951255099     PISSN: 13886150     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10973-009-0652-9     Document Type: Article

References (16)

1. Mullin JW. Crystallization. 4th ed. Oxford: Butterworth-Heinemann; 2001.
2. Brittain HG. Polymorphism in pharmaceutical solids. New York: Marcel Dekker; 1999.
3. Bernstein J. Polymorphism in molecular crystals. Oxford: Oxford University Press; 2002.
4. Nývlt J, Söhnel O, Matuchová M, Broul M. The kinetics of industrial crystallization. Amsterdam: Elsevier; 1985.
5. Hemminger W, Sarge SM. Definitions, nomenclature, terms, and literature. In: Brown ME, editor. Handbook of thermal analysis and calorimetry, vol. 1. Amsterdam: Elsevier; 1998. p. 1.
6. H Gürbüz B Özdemir 2003 Experimental determination of the metastable zone width of borax decahydrate by ultrasonic velocity measurement J Cryst Growth 252 343 349 10.1016/S0022-0248(02)02519-8
7. P Sessiecq F Gruy M Cournil 2000 Study of ammonium chloride crystallization in a mixed vessel J Cryst Growth 208 555 568 10.1016/S0022-0248(99)00411-X 1:CAS:528:DyaK1MXotVKltbs%3D (Pubitemid 30530540)
8. D Kashchiev GM van Rosmalen 2003 Review: nucleation in solutions revisited Cryst Res Technol 38 555 574 10.1002/crat.200310070 1:CAS:528:DC%2BD3sXmtF2rsrk%3D
9. JW Mullin J Nyvlt 1971 Programmed cooling of batch crystallizers Chem Eng Sci 26 369 377 10.1016/0009-2509(71)83012-9 1:CAS:528:DyaE3MXhsVers78%3D
10. B Mayrhofer J Nyvlt 1988 Programmed cooling of batch crystallizers Chem Eng Process 24 217 220 10.1016/0255-2701(88)85005-0 1:CAS:528:DyaL1MXlslOjt78%3D
11. Leidler KJ. Chemical kinetics. 2nd ed. New York: Harper and Row; 1987.
12. P Correia C Lopes ME Minas da Piedade JAA Lourenço ML Serrano 2006 Solubility and metastable zone width of 1-keto-1, 2, 3, 4-tetrahydro-6- methylcarbazole in acetone J Chem Eng Data 51 1306 1309 10.1021/je0600552 1:CAS:528:DC%2BD28Xlt1Gitr8%3D (Pubitemid 44197273)
13. O Sahim H Dolas H Demir 2007 Determination of nucleation kinetics of potassium tetraborate tetrahydrate Cryst Res Technol 42 766 772 10.1002/crat.200710904 (Pubitemid 47228969)
14. A Chianese N Santilli O Sohnel 1996 Influence of admixtures and operating conditions on the crystallization of ammonium chloride J Cryst Growth 166 1099 1104 10.1016/0022-0248(96)00063-2 1:CAS:528:DyaK28XlvVaqu7c%3D
15. HK Zimmerman 1952 The experimental determination of solubilities Chem Rev 51 25 65 10.1021/cr60158a002 1:CAS:528:DyaG38Xls1eqsA%3D%3D
16. Lide DR. Handbook of chemistry and physics. 87th ed. Boca Raton: Taylor and Francis; 2007.