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X-Band EPR spectra were recorded on a Bruker Elexsys E500 spectrometerfitted with a Super High Q cavity (spectrometer settings for Figure 1: receivergain = 96 dB; modulation amplitude = 6 G: microwave power 6 mW; 74 and 37 scansaveraged for (a, c respectively)). Calibrations of the magnetic field andmicrowave frequency were achieved with a Bruker ER 035M Gaussmeter and an EIP548B microwave frequency counter, respectively. Low temperature spectra wererecorded using a liquid nitrogen flow-through cryostat in conjunction with aEurotherm B-VT2000 variable temperature controller.
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X-Band EPR spectra were recorded on a Bruker Elexsys E500 spectrometerfitted with a Super High Q cavity (spectrometer settings for Figure 1: receivergain = 96 dB; modulation amplitude = 6 G: microwave power 6 mW; 74 and 37 scansaveraged for (a, c respectively)). Calibrations of the magnetic field andmicrowave frequency were achieved with a Bruker ER 035M Gaussmeter and an EIP548B microwave frequency counter, respectively. Low temperature spectra wererecorded using a liquid nitrogen flow-through cryostat in conjunction with aEurotherm B-VT2000 variable temperature controller.
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2342658401
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Straindistributions of D and E were not included in the simulations
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Hanson, G. R.; Gates, K. E.; Noble, C. J.; Griffin, M.; Mitchell, A.;Benson, S. J. Inorg. Biochem. 2004, 98, 903-916. Straindistributions of D and E were not included in the simulations.
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26
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77951278410
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The E/D ratio 0.1 for the biradical represents an upper limit andis more likely to be closer to zero, but without resolution of the axialresonances, a precise value cannot be determined.
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The E/D ratio 0.1 for the biradical represents an upper limit andis more likely to be closer to zero, but without resolution of the axialresonances, a precise value cannot be determined.
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28
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