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n (0.005mmol) was degassed through repeated freezepumpthaw cycles. The reaction solution was stirred by magnetic stirrer and irradiated at 300K using a 500W Xe lamp (USHIO Co.) equipped with an optical cut-off filter (>400 nm).
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n (0.005mmol) was degassed through repeated freezepumpthaw cycles. The reaction solution was stirred by magnetic stirrer and irradiated at 300K using a 500W Xe lamp (USHIO Co.) equipped with an optical cut-off filter (>400 nm).
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14
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34547317719
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77950855312
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2+ was stirred for 0, 15, 30, and 60min.
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2+ was stirred for 0, 15, 30, and 60min.
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16
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77950809700
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XPS were recorded on JPS-9010 (JOEL) with MgKα X-ray source (10 kV, 10 mA). FT-IR spectra were recorded on a JASCO 4100 FT-IR spectrometer in KBr disk at room temperature.
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XPS were recorded on JPS-9010 (JOEL) with MgKα X-ray source (10 kV, 10 mA). FT-IR spectra were recorded on a JASCO 4100 FT-IR spectrometer in KBr disk at room temperature.
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17
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84970582721
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77950800921
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Supporting Information is available electronically on the CSJ-journal web site
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Supporting Information is available electronically on the CSJ-journal web site, http://www.csj.jp/journals/chem-lett/index.html.
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