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Volumn , Issue 6, 2010, Pages 973-975

Water-mediated multicomponent reaction: A facile and efficient synthesis of multisubstituted thiazolidine-2-thiones

Author keywords

Green method; Heterocyclic compounds; MCR; Synthesis; Thiazolidine 2 thione

Indexed keywords

3 BENZYL 4 HYDROXY 4 PHENYLTHIAZOLIDINE 2 THIONE; ALPHA BROMOKETONE; AMINE; KETONE; THIAZOLE DERIVATIVE; THIAZOLIDINE 2 THIONE DERIVATIVE; UNCLASSIFIED DRUG;

EID: 77949911025     PISSN: 09365214     EISSN: 14372096     Source Type: Journal    
DOI: 10.1055/s-0029-1219558     Document Type: Article
Times cited : (35)

References (28)
  • 9
    • 70349659498 scopus 로고    scopus 로고
    • Roux M V., Temprado M, Jiménez P, Foces-Foces C, Notario R, Parameswar A R., Demchenko A V., Chickos J S., Deakyne C A., Ludden A K., Liebman J F., J. Phys. Chem. A 2009 113 10772
    • (2009) J. Phys. Chem. A , vol.113 , pp. 10772
    • Roux, M.V.1
  • 27
    • 77949879824 scopus 로고    scopus 로고
    • Note
    • Crystallographic data (excluding structure factors) for the structures in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication number CCDC 747685.
  • 28
    • 77949892879 scopus 로고    scopus 로고
    • Note
    • General Procedure To a solution of amines 1 (0.75 mmol) in H2O (3 mL), CS2 (1.5 mmol) and a-bromoketone 2 (0.5 mmol) were added. Subsequently, K2CO3 (0.25 mmol) was located to the mixture. After stirring the mixture at r.t. for 1 h, the mixture was extracted with EtOAc (3 10 mL), and the combined organic layers were dried overnight with anhyd Na2SO4. After the organic solvent was removed, the residue was subjected to silical gel chromatography PEEtOAc (5:1) as eluent to give pure products.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.