Determination of phthalate esters in water samples using Nylon6 nanofibers mat-based solid-phase extraction coupled to liquid chromatography

Microchimica Acta

Volumn 168, Issue 3, 2010, Pages 267-275

  Xu, Qian ^a   Yin, Xueyan ^a   Wu, Shuyan ^a   Wang, Min ^a   Wen, Zuoyang ^a   Gu, Zhongze ^a  

^a SOUTHEAST UNIVERSITY   (China)

Author keywords

Electrospun nylon6 nanofibers mat; High performance liquid chromatography; Phthalate; Solid phase extraction; UV detection

Indexed keywords

EID: 77949657265     PISSN: 00263672     EISSN: 14365073     Source Type: Journal    
DOI: 10.1007/s00604-010-0290-8     Document Type: Article

References (37)

1. De Orsi D, Gagliardi L, Porra R, Berri S, Chimenti P, Granese A, Carpani I, Tonelli D (2006) A environmentally friendly reversed-phase liquid chromatography method for phthalates determination in nail cosmetics. Anal Chim Acta 555: 238.
2. Zhao RS, Wang X, Yuan JP, Lin JM (2008) Investigation of feasibility of bamboo charcoal as solid-phase extraction adsorbent for the enrichment and determination of four phthalate esters in environmental water samples. J Chromatogr A 1183: 15.
3. Harris CA, Henttu P, Parker MG, Sumpter JP (1997) The estrogenic activity of phthalate esters in vitro. Environ Health Perspect 105: 802.
4. Lin ZP, Ikonomou MG, Jing H, Mackintosh C, Gobas FAPC (2003) Determination of phthalate ester congeners and mixtures by LC/ESI-MS in sediments and biota of an urbanized marine inlet. Environ Sci Technol 37: 2100.
5. Calafat AM, Slakman AR, Silva MJ, Herbert AR, Needham LL (2004) Automated solid phase extraction and quantitative analysis of human milk for 13 phthalate metabolites. J Chromatogr B 805: 49.
6. Mori S (1976) Identification and determination of phthalate esters in river water by high-performance liquid chromatography. J Chromatogr B 129: 53.
7. CaiY Q, Cai Y, Shi YL, Liu JM, Mou SF, Lu YQ (2007) A liquid-liquid extraction technique for phthalate esters with water-soluble organic solvents by adding inorganic salts. Microchimica Acta 157: 73.
8. Li XJ, Zeng ZR, Chen Y, Xu Y (2005) Determination of phthalate acid esters plasticizers in plastic by ultrasonic solvent extraction combined with solid-phase microextraction using calix[4]arene fiber. Talanta 63: 1013.
9. Bartolome L, Cortazar E, Raposo JC, Usobiaga A, Zuloaga O, Etxebarria N, Fernandez LA (2005) Simultaneous microwave-assisted extraction of polycyclic aromatic hydrocarbons, polychlorinated biphenyls, phthalate esters and nonylphenols in sediments. J Chromatogr A 1068: 229.
10. Batlle R, Nerin C (2004) Application of single-drop microextraction to the determination of dialkyl phthalate esters in food simulants. J Chromatogr A 1045: 29.
11. de Souza MM, Bortoluzzi JH, Carasek E (2006) Thermal immobilization of poly(butylacrylate) on glass-ceramic rod for preparation of solid phase microextraction fibers. Microchimica Acta 155: 465.
12. Cortazar E, Zuloaga O, Sanz J, Raposo JC, Etxebarria N, Fernandez LA (2002) MultiSimplex optimisation of the solid-phase microextractions-gas chromatographic-mass spectrometric determination of polycyclic aromatic hydrocarbons, polychlorinated biphenyls and phthalates from water samples. J Chromatogr A 978: 165.
13. ZhaoRS WX, Yuan JP, Zhang LL (2009) Solid-phase extraction of bisphenol A, nonylphenol and 4-octylphenol from environmental water samples using microporous bamboo charcoal, and their determination by HPLC. Microchimica Acta 165: 3.
14. Zhao XL, Li JD, Shi YL, Cai YQ, Mou SF, Jiang GB (2007) Determination of perfluorinated compounds in wastewater and river water samples by mixed hemimicelle-based solid-phase extraction before liquid chromatography-electrospray tandem mass spectrometry detection. J Chromatogr A 1154: 52.
15. Guo GS, He CN, Wang ZH, Gu FB, Han DM (2007) Synthesis of titania and titanate nanomaterials and their application in environmental analytical chemistry. Talanta 72: 1687.
16. Moller K, Kobler J, Bein T (2007) Colloidal suspensions of mercapto-functionalized nanosized mesoporous silica. J Mater Chem 17: 605.
17. Klabunde KJ (2001) Nanoscale material in chemistry. Wiley-Interscience, New York.
18. Smith JE, Medley CD, Tang Z, Shangguan D, Lofton C, Tan W (2007) Aptamer-conjugated nanoparticles for the collection and detection of multiple cancer cells. Anal Chem 79: 3075.
19. 4 for the determination of chlorophenols in environmental water samples coupled with liquid chromatography/spectrophotometry detection. J Chromatogr A 1180: 24.
20. Huang ZM, Zhang YZ, Kotaki M, Ramakrishna S (2003) A review on polymer nanofibers by electrospinning and their applications in nanocomposites. Compos Sci Technol 63: 2223.
21. Qi DJ, Kang XJ, Chen LQ, Zhang YY, Wei HM, Gu ZZ (2008) Electrospun polymer nanofibers as a solid-phase extraction sorbent for the determination of trace pollutants in environmental water. Anal Bioanal Chem 390: 929.
22. Kang XJ, Chen LQ, Zhang YY, Liu YW, Gu ZZ (2008) Performance of electrospun nanofibers for SPE of drugs from aqueous solutions. J Sep Sci 31: 3272.
23. Kang XJ, Pan C, Xu Q, Yao YF, Wang Y, Qi DJ, Gu ZZ (2007) The investigation of electrospun polymer nanofibers as a solid-phase extraction sorbent for the determination of trazodone in human plasma. Anal Chim Acta 587: 75-81.
24. Bortolato SA, Arancibia JA, Escandar GM (2008) A novel application of nylon membranes to the luminescent determination of benzo[a]pyrene at ultra trace levels in water samples. Anal Chim Acta 613: 218.
25. Dombrowski TR, Wilson GS, Thurman EM (1998) Investigation of anion-exchange and immunoaffinity particle-loaded membranes for the isolation of charged organic analytes from water. Anal Chem 70: 1969.
26. Zhang S, Shim WS, Kim J (2009) Design of ultra-fine nonwovens via electrospinning of Nylon 6: Spinning parameters and filtration efficiency. Mater Des 30: 3659.
27. Ojha SS, Afshari M, Kotek R, Gorga RE (2008) Morphology of electrospun nylon-6 nanofibers as a function of molecular weight and processing parameters. J Appl Polym Sci 108: 308.
28. Bazbouz MB, Stylios GK (2008) Alignment and optimization of nylon 6 nanofibers by electrospinning. J Appl Polym Sci 107: 3023.
29. Mit-uppatham C, Nithitanakul M, Supaphol P (2004) Effects of solution concentration, emitting electrode polarity, solvent type, and salt addition on electrospun polyamide-6 fibers: a preliminary report. Macromol Symp 216: 293.
30. Zhou QX, Ding YJ, Xiao JP (2006) Sensitive determination of thiamethoxam, imidacloprid and acetamiprid in environmental water samples with solid-phase extraction packed with multiwalled carbon nanotubes prior to high-performance liquid chromatography. Anal Bioanal Chem 385: 1520.
31. Polo M, Gomez-Noya G, Quintana JB, Llompart M, Garcia-Jares C, Cela R (2004) Development of a solid-phase microextraction gas chromatography/tandem mass spectrometry method for polybrominated diphenyl ethers and polybrominated biphenyls in water samples. Anal Chem 76: 1054.
32. Zhao RS, Wang X, Yuan JP, Lin JM (2008) Investigation of feasibility of bamboo charcoal as solid-phase extraction adsorbent for the enrichment and determination of four phthalate esters in environmental water samples. J Chromatogr A 1183: 15.
33. Li X, Zhong M, Xu SF, Sun C (2006) Determination of phthalates in water samples using polyaniline-based solid-phase microextraction coupled with gas chromatography. J Chromatogr A 1135: 101.
34. Li JD, Cai YQ, Shi YL, Mou SF, Jiang GB (2008) Analysis of phthalates via HPLC-UV in environmental water samples after concentration by solid-phase extraction using ionic liquid mixed hemimicelles. Talanta 74: 498.
35. Lopez-Jimenez FJ, Rubio S, Perez-Bendito D (2005) Determination of phthalate esters in sewage by hemimicelles-based solid-phase extraction and liquid chromatography-mass spectrometry. Anal Chim Acta 551: 142.
36. Regueir J, Llompart M, Garcia-Jares C, Garcia-Monteagudo JC, Cela R (2008) Ultrasound-assisted emulsification microextraction of emergent contaminants and pesticides in environmental waters. J Chromatogr A 1190: 27.
37. NiuHY CYQ, ShiYL WFS, Mou SF, Jiang GB (2007) Cetyltrimethylammonium bromide-coated titanate nanotubes for solid-phase extraction of phthalate esters from natural waters prior to high-performance liquid chromatography analysis. J Chromatogr A 1172: 113.