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15
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77949573831
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Note
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-1, Flack parameter = -0.037(17), Measured reflections = 49308, Unique reflections = 3645, Reflections with I > 2σ(I) = 3607 [R(int) = 0.0477]. Refinement of 238 variables with anisotropic thermal parameters for all non-hydrogen atoms gave R1 (all) = 0.0476, R(obs) = 0.0473, wR2 (all) = 0.1304 and wR2 (obs) = 0.1299, with S = 1.061.
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-
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16
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77949592260
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Note
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II crystals would not be a conglomerate because the two compounds are diastereoisomers and not enantiomers
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18
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34250728460
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H. O. Stumpf C. L. M. Pereira A. C. Doriguetto C. Konzen L. C. B. Meira N. G. Fernandes Y. P. Mascarenhas J. Ellena M. Knobel Eur. J. Inorg. Chem. 2005 24 5018
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Stumpf, H.O.1
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Knobel, M.9
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