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Volumn 49, Issue 6, 2010, Pages 2983-2989

Reactions of organyl and silyl alane with 1.3.4.5.6-pentamethyl-2- aminoborazine

Author keywords

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Indexed keywords


EID: 77949346969     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic902490z     Document Type: Article
Times cited : (8)

References (64)
  • 43
    • 77949404035 scopus 로고    scopus 로고
    • Programs used for centering reflections, autoindexing, refinement of cell parameters and axial photographs are those described in: Sparks, R. A. Nicolet P3/R3 Operations Manual; Syntex Analytical Instruments: Cupertino, CA, 1978.
    • Programs used for centering reflections, autoindexing, refinement of cell parameters and axial photographs are those described in: Sparks, R. A. Nicolet P3/R3 Operations Manual; Syntex Analytical Instruments: Cupertino, CA, 1978.
  • 44
    • 77949415743 scopus 로고    scopus 로고
    • The SHELXTL, package of programs for calculations and plots is described in: Sheldrick, G. M. SHELXTL Users Manual, Revision 3; Nicolet XRD Corp.: Cupertino, CA, 1981.
    • The SHELXTL, package of programs for calculations and plots is described in: Sheldrick, G. M. SHELXTL Users Manual, Revision 3; Nicolet XRD Corp.: Cupertino, CA, 1981.
  • 45
    • 77949389642 scopus 로고    scopus 로고
    • SHELXTL uses scattering factors and anomalous dispersion terms taken from: International Tables of X-Ray Crystallography; Kynoch: Birmingham, England, 1968; IV.
    • SHELXTL uses scattering factors and anomalous dispersion terms taken from: International Tables of X-Ray Crystallography; Kynoch: Birmingham, England, 1968; Vol. IV.
  • 47
    • 77949393668 scopus 로고    scopus 로고
    • The NMR spectra for 1 can be compared with data for the acid and base fragment molecules (Me3Si)3Al-OEt21H NMR (C6D6, <5 0.24 (27 H, SiMe, 0.73 (6H, OCH 2CH3, 3.34(4H, OCH2CH3, 13C{1H) NMR(C6D6, δ2.84 (SiMe, 13.19 (OCH2CH3, 69.63 (OCH2CH 3, Me3N3B3Me2(NH 2) 1H NMR (C6D6, δ 0.47 (6 H, B-4, 6 Me, 1.93 (2 H, NH2, 2.56 (6 H, N-1,3 Me, 2.77 (3 H, N-5 Me, 13C{1H) NMR (C6D6, δ -0.10 (B-4,6 Me, 31.75 (N-1,3 Me, 34.53 (N-5 Me, 11B( 1H) NMR (C6D6, δ 26.2 (B-2, 36.3 B-4,6
    • 6): δ 26.2 (B-2), 36.3 (B-4,6).
  • 58
    • 77949351382 scopus 로고    scopus 로고
    • The descrepandes in CHN analytical data result from incomplete combustion of the samples as noted in analysis reports from commercial sources. This is likely due to formation of ceramic residues. Similar observations were made with analyses of, Me3Si2AlNH2]2. 11a
    • 11a
  • 63
    • 0003495856 scopus 로고
    • Powder Diffraction File
    • Card No. 25-1133, JCPDS, International Center for Powder Diffraction Data, Swarthmore, PA
    • Powder Diffraction File Card No. 25-1133, JCPDS, International Center for Powder Diffraction Data, Swarthmore, PA, 1975.
    • (1975)


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.