Sol-gel processing of a glycolated cyclic organosilane and itspyrolysis to silicon oxycarbide monoliths with multiscale porosity and large surface areas

Chemistry of Materials

Volumn 22, Issue 4, 2010, Pages 1509-1520

  Weinberger, Manuel ^a,b   Puchegger, Stephan ^a   Fröschl, Thomas ^b   Babonneau, Florence ^c   Peterlik, Herwig ^a   Hüsing, Nicola ^b  

^a UNIVERSITY OF VIENNA   (Austria)

^b UNIVERSITY OF ULM   (Germany)

^c UNIVERSITÉ PIERRE ET MARIE CURIE   (France)

Author keywords

[No Author keywords available]

Indexed keywords

ARGON ATMOSPHERES; CARBOSILANES; CHARACTERIZATION TECHNIQUES; CONCENTRATION OF; ELEMENTAL ANALYSIS; HIERARCHICAL NETWORK; HIERARCHICAL POROSITY; HYDROCHLORIC ACID SOLUTION; LARGE SURFACE AREA; MACROPORES; MACROPOROUS STRUCTURES; MESO-PORES; MODULUS VALUES; MULTISCALES; ORGANOSILANES; ORGANOSILICAS; PLURONICS; POLYMERIZATION-INDUCED PHASE SEPARATION; PORE DIAMETERS; POTASSIUM CHLORIDE; SILICON OXYCARBIDES; SOL-GEL PROCESSING; SOLID STATE NMR; STRUCTURAL FEATURE; SURFACE AREA; TEMPLATED; VOLUME SHRINKAGE;

ARGON; BLOCK COPOLYMERS; CHEMICAL ANALYSIS; CHLORINE COMPOUNDS; EFFLUENT TREATMENT; GELS; GLYCOLS; HYDROCHLORIC ACID; INERT GASES; MONOLITHIC INTEGRATED CIRCUITS; PHASE MODULATION; POLYMER BLENDS; POLYMERIZATION; POROSITY; PYROLYSIS; SILICON CARBIDE; SIZE SEPARATION; SOL-GEL PROCESS; SOLS; SUPERCRITICAL FLUID EXTRACTION; SUPERCRITICAL FLUIDS;

PHASE SEPARATION;

EID: 77049115251     PISSN: 08974756     EISSN: 15205002     Source Type: Journal    
DOI: 10.1021/cm903031d     Document Type: Article

References (51)

1. Rouxel, T.; Massouras, G.; Sorarù, G.-D. J. Sol-Gel Sci. Technol.1999, 14, 87.
2. Sorarù, G.-D.; Dallapiccola, E.; D'Andrea, G. J. Am. Ceram. Soc. 1996, 79, 2074.
3. Sorarù, G.-D.; Modena, S.; Guadagnino, E.; Colombo, P.; Egan, J.; Pantano, C. J. Am. Ceram. Soc. 2002, 85, 1529.
4. Moysan, C.; Riedel, R.; Harshe, R.; Rouxel, T.; Augereau, F.J. Eur. Ceram. Soc. 2002, 22, 2389.
5. Babonneau, F.; Thorne, K.; Mackenzie, J. D. Chem. Mater. 1989,1, 554.
6. Babonneau, F.; Bois, L.; Yang, C.-Y.; Interrante, L. V. Chem.Mater. 1994, 6, 51.
7. Liu, Q.; Shi, W.; Babonneau, F.; Interrante, L. V. Chem. Mater.1997, 9, 2434.
8. Sorarù, G. D.; Liu, Q.; Interrante, L. V.; Apple, T. Chem. Mater.1998, 10, 4047.
9. Corriu, R. J. P.; Leclercq, D.; Mutin, P. H.; Vioux, A. J. Sol-Gel Sci. Technol. 1997, 8, 327.
10. Corriu, R. J. P.; Leclerq, D.; Mutin, P. H.; Vioux, A. J. Mater. Sci. 1995, 30, 2313.
11. Kockrick, E.; Frind, R.; Rose, M.; Petasch, U.; Böhlmann, W.; Geiger, D.; Herrmann, M.; Kaskel, S. J. Mater. Chem. 2009, 19, 1543.
12. Trassl, S.; Motz, G.; Rössler, E.; Ziegler, G. J. Am. Ceram. Soc. 2002, 85, 239.
13. Trassl, S.; Kleebe, H.-J.; Störmer, H.; Motz, G.; Rössler, E.; Ziegler, G. J. Am. Ceram. Soc. 2002, 85, 1268.
14. Babonneau, F.; Sorarù, G. D.; D'Andrea, G.; Dirè, S.; Bois, L. Mater. Res. Soc. Symp. Proc. 1992, 271, 789.
15. Sorarù, G. D.; D'Andrea, G.; Campostrini, R.; Babonneau, F.; Mariotto, G. J. Am. Ceram. Soc. 1995, 78, 379.
16. Singh, A. K.; Pantano, C. G. Mater. Res. Soc. Symp. Proc. 1992, 271, 795.
17. Pauletti, A.; Handjani, S.; Fernandez-Martin, C.; Gervais, C.; Babonneau, F. J. Ceram. Soc. Jpn. 2008, 116, 449.
18. Toury, B.; Blum, R.; Goletto, V.; Babonneau, F. J. Sol-Gel Sci. Technol. 2005, 33, 99.
19. Toury, B.; Babonneau, F. J. Eur. Ceram. Soc. 2005, 25, 265.
20. Masse, S.; Laurent, G.; Babonneau, F. J. Non-Cryst. Sol. 2007, 353, 1109.
21. Nakanishi, K.; Soga, N. J. Am. Ceram. Soc. 1991, 74, 2518.
22. Nakanishi, K.; Komura, H.; Takahashi, R.; Soga, N Bull. Chem. Soc. Jpn. 1994, 67, 1327.
23. Nakanishi, K. J. Porous Mater. 1997, 4, 67.
24. Nakanishi, K.; Kanamori, K. J. Mater. Chem. 2005, 15, 3776.
25. Nakanishi, K. Bull. Chem. Soc. Jpn. 2006, 79, 673.
26. Ivanova, R.; Lindman, B.; Alexandridis, P. Langmuir 2000, 16, 3660.
27. Hüsing, N.; Raab, C.; Torma, V.; Roig, A.; Peterlik, H. Chem. Mater. 2003, 15, 2690.
28. Smått, J.-H.; Schunk, S.; Lindén, M. Chem. Mater. 2003, 15, 2354.
29. Nakanishi, K.; Kobayashi, Y.; Amatani, T.; Hirao, K.; Kodaira, T. Chem. Mater. 2004, 16, 3652.
30. Brandhuber, D.; Torma, V.; Raab, C.; Peterlik, H.; Kulak, A.; Hüsing, N. Chem. Mater. 2005, 17, 4262.
31. Brandhuber, D.; Peterlik, H.; Hüsing, N. Small 2006, 2, 503.
32. Hartmann, S.; Brandhuber, D.; Hüsing, N. Acc. Chem. Res. 2007, 40, 885.
33. Nakanishi, K.; Amatani, T.; Yano, S.; Kodaira, T. Chem. Mater. 2008, 20, 1108.
34. Weinberger, M.; Fröschl, T.; Puchegger, S.; Peterlik, H.; Hüsing, N. Silicon 2009, 1, 19.
35. Konishi, J.; Fujita, K.; Nakanishi, K.; Hirao, K. Chem. Mater. 2006, 18, 864.
36. Konishi, J.; Fujita, K.; Oiwa, S.; Nakanishi, K.; Hirao, K. Chem. Mater. 2008, 20, 2165.
37. Sonnenburg, K.; Adelhelm, P.; Antonietti, M.; Smarsly, B.;Nöske, R.; Strauch, P. Phys. Chem. Chem. Phys. 2006, 8, 3561.
38. Zampieri, A.; Kullmann, S.; Selvam, T.; Bauer, J.; Schwieger, W.; Sieber, H.; Fey, T.; Greil, P. Microporous Mesoporous Mater. 2006, 90, 162.
39. Landskron, K.; Hatton, B. D.; Perovic, D. D.; Ozin, G. A. Science 2003, 302, 266.
40. Brondani, D. J.; Corriu, R. J. P.; El Ayoubi, S.; Moreau, J. J. E.; Wong Chi Man, M. Tetrahedron Lett. 1993, 34, 2111.
41. Massiot, D.; Fayon, F.; Capron, M.; King, I.; Le Calvé, S.; Alonso, B.; Durand, J.-O.; Bujoll, B.; Gan, Z.; Hoatson, G. Magn. Reson. Chem. 2002, 40, 70.
42. Migliori, A.; Sarrao, J. L. Resonant Ultrasound Spectroscopy; John Wiley & Sons, Inc.: New York, 1997.
43. Weinberger, M.; Puchegger, S.; Rentenberger, C.; Puchberger, M.; Hüsing, N.; Peterlik, H. J. Mater. Chem. 2008, 18, 4783.
44. Teixeira, J. J. Appl. Crystallogr. 1988, 21, 781.
45. Zhong, H.; Liu, J.; Wang, P.; Yang, J.; Yang, Q. Microporous Mesoporous Mater. 2009, 123, 63.
46. Yu, C.; Fan, J.; Tian, B.; Zhao, D. Chem. Mater. 2004, 16, 889.
47. Guo, W.; Park, J.-Y.; Oh, M.-O.; Jeong, H.-W.; Cho, W.-J.; Kim, I.; Ha, C.-S. Chem. Mater. 2003, 15, 2295.
48. Bagshaw, S. A.; Prouzet, E.; Pinnavaia, T. J. Science 1995, 269, 1242.
49. Prouzet, E.; Cot, F.; Nabias, G.; Larbot, A.; Kooyman, P.; Pinnavaia, T. J. Chem. Mater. 1999, 11, 1498.
50. Fukushima, M.; Yasuda, E.; Teranishi, Y.; Nakamura, K.; Tanabe, Y. J. Ceram. Soc. Jpn. 2004, 112, 612.
51. Puchegger, S.; Brandhuber, D.; Hüsing, N.; Peterlik, H. J. Non-Cryst. Solids 2006, 352, 5251.