Large scale melt synthesis in an open crucible of Na-fluorohectorite with superb charge homogeneity and particle size

Applied Clay Science

Volumn 48, Issue 1-2, 2010, Pages 39-45

  Kalo, Hussein ^a   Möller, Michael W ^a   Ziadeh, Mazen ^a   Dolejš, David ^b   Breu, Josef ^a  

^a UNIVERSITY OF BAYREUTH   (Germany)

^b UNIVERSITÄT BAYREUTH   (Germany)

Author keywords

Charge homogeneity; Fluorohectorite; Large scale synthesis; Melt synthesis

Indexed keywords

ALKALI-SILICATE GLASS; ALKYLAMMONIUM EXCHANGE; ARGON FLOW; CATION EXCHANGE CAPACITIES; COPPER COMPLEXES; FLUOROHECTORITE; FLUXING AGENTS; HIGH FREQUENCY INDUCTION; HUMIDITY CHAMBERS; HYDRATION BEHAVIORS; IN-SITU; LARGE SCALE SYNTHESIS; LASER LIGHT SCATTERING; LATERAL EXTENSION; LOW VAPOR PRESSURES; MEDIAN VALUE; PHASE PURITY; SEM; SHORT PERIODS; SILICON FLUORIDES; SYNTHESIS METHOD;

ARGON; COMPLEXATION; COPPER COMPOUNDS; FLUORINE; FLUORINE COMPOUNDS; GLASS; GLASSY CARBON; LIGHT; LIGHT SCATTERING; ORGANIC POLYMERS; SCANNING ELECTRON MICROSCOPY; SILICA; SILICATES; SILICON OXIDES; X RAY POWDER DIFFRACTION;

SYNTHESIS (CHEMICAL);

CLAY MINERAL; FLUORIDE; HOMOGENEITY; HYDRATION; MELT; MINERAL SYNTHESIS; PARTICLE SIZE; SILICA; SODIUM; SOLUBILITY; VAPOR PRESSURE;

EID: 76849090048     PISSN: 01691317     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.clay.2009.11.014     Document Type: Article

References (42)

1. Ammann L., Bergaya F., and Lagaly G. Determination of the cation exchange capacity of clays with copper complexes revisited. Clay Minerals 40 (2005) 441-453
2. Anfilogov V.N., Bragina G.I., Bobylev I.B., and Zyuzeva N.A. Fluorine and chlorine structural position in silicate melt. Geokhimiya 1 (1979) 30-36
3. Bale C., Chartrand P., Degterov S.A., Eriksson G., Hack K., Ben Mahfoud R., Melancon J., Pelton A.D., and Petersen S. FactSage thermochemical software and databases. Calphad-Computer Coupling of Phase Diagrams and Thermochemistry 26 2 (2002) 189-228
4. Baumgartner A., Sattler K., Thun J., and Breu J. A route to microporous materials through oxidative pillaring of micas. Angewandte Chemie-International Edition 47 9 (2008) 1640-1644
5. Baumgartner A., Wagner F.E., Herling M., and Breu J. Towards a tunable pore size utilizing oxidative pillaring of the mica ferrous tainiolite. Microporous and Mesoporous Materials 123 1-3 (2009) 253-259
6. Breu J., Seidl W., Stoll A.J., Lange K.G., and Probst T.U. Charge homogeneity in synthetic fluorohectorite. Chemistry of Materials 13 (2001) 4213-4220
7. Breu J., Seidl W., and Stoll A. Fehlordnung bei Smectiten in Abhängigkeit vom Zwischenschichtkation. Zeitschrift für Anorganische und Allgemeine Chemie 629 (2002) 503-515
8. Decarreau A., Grauby O., and Petit S. The actual distribution of octahedral cations in 2:1 clay minerals: results from clay synthesis. Applied Clay Science 7 1-3 (1992) 147-167
9. 2 and Pd-circle nanoparticles growing in the interlamellar space of montmorillonite in binary liquids. Applied Clay Science 15 1-2 (1999) 221-239
10. Ferrage E., Lanson B., Malikova N., Plancon A., Sakharov B.A., and Drits V.A. New insights on the distribution of interlayer water in bi-hydrated smectite from X-ray diffraction profile modeling of 00l reflections. Chemistry of Materials 17 13 (2005) 3499-3512
11. Ferrage E., Lanson B., Sakharov B.A., Geoffroy N., Jacquot E., and Drits V.A. Investigation of dioctahedral smectite hydration properties by modeling of X-ray diffraction profiles: influence of layer charge and charge location. American Mineralogist 92 (2007) 1731-1743
12. Kaviratna P.D., Pinnavaia T.J., and Schroeder P.A. Dielectric properties of smectite clays. Journal of Physics and Chemistry of Solids 57 12 (1996) 1897-1906
13. Klapyta Z., Fujita T., and Iyi N. Adsorption of dodecyl- and octadecyltrimethylammonium ions on a smectite and synthetic micas. Applied Clay Science 19 1-6 (2001) 5-10
14. Lagaly G. Characterization of clays by organic compounds. Clay Minerals 16 (1981) 1-21
15. Lagaly G. Layer charge determination by alkylammonium ions. In: Mermut A.R. (Ed). Layer Charge Characteristics of 2:1 Silicate Clay Minerals (1994), Clay Mineral Society 1-46
16. Lagaly G. Surface and interlayer reactions: bentonites as adsorbents. In: Churchman G.J., Fitzpatrick R.W., and Eggleton R.A. (Eds). Clays Controlling the Environment (1995), CSIRO publishing, Melbourne 137-144
17. Lagaly G., and Gardolinsky J.E.F.C. Grafted organic derivatives of kaolinite: II. Intercalation of primary n-alkylamines and delamination. Clay Minerals 40 4 (2005) 547-556
18. Lagaly G., and Weiss A. Anordnung und Orientierung kationischer Tenside auf Silicatoberflächen. Kolloid-Zeitschrift und Zeitschrift für Polymere 243 (1971) 48-55
19. Malikova N., Cadene A., Dubois E., Marry V., Durand-Vidal S., Turq P., Breu J., Longeville S., and Zanotti J.M. Water diffusion in a synthetic hectorite clay studied by quasi-elastic neutron scattering. Journal of Physical Chemistry C 111 47 (2007) 17603-17611
20. 2 glasses. Journal of the American Ceramic Society 64 (1981) C20
21. McGahay V., and Tomozawa M. The origin of phase separation in silicate melts and glasses. Journal of Non-Crystalline Solids 109 (1989) 27-34
22. Mermut A.R., and Lagaly G. Baseline studies of the Clay Minerals Society Source Clays: layer-charge determination and characteristics of those minerals containing 2:1 layers. Clays and Clay Minerals 49 5 (2001) 393-397
23. Meunier A. Why are clay minerals small?. Clay Minerals 41 2 (2006) 551-566
24. Muller F., Besson G., Manceau A., and Drits V.A. Distribution of isomorphous cations within octahedral sheets in montmorillonite from Camp-Bertaux. Physics and Chemistry of Minerals 24 3 (1997) 159-166
25. 2. Journal of Non-Crystalline Solids 188 1-2 (1995) 136-146
26. Oueslati W., Karmous M.S., Rhaiem H., Lanson B., and Amara A.B.H. Effect of interlayer cation and relative humidity on the hydration properties of a dioctahedral smectite. Zeitschrift für Kristallographie 26 (2007) 417-422
27. Palin E.J., Dove M.T., Hernandez-Laguna A., and Sainz-Diaz C.I. A computational investigation of the Al/Fe/Mg order-disorder behavior in the dioctahedral sheet of phyllosilicates. American Mineralogist 89 1 (2004) 164-175
28. Pelton A.D., and Blander M. Thermodynamic analysis of ordered liquid solutions by a modified quasi-chemical approach - application to silicate slags. Metallurgical Transactions B-Process Metallurgy 17 4 (1986) 805-815
29. Pelton A.D., Thompson W.T., Bale C.W., and Eriksson G. FactSage thermochemical database for calculations in materials chemistry at high-temperatures. High Temperature Science 26 (1989) 231-250
30. Perez-Rodriguez J.L., Carrera F., Poyato J., and Perez-Maqueda L.A. Sonication as a tool for preparing nanometric vermiculite particles. Nanotechnology 13 3 (2002) 382-387
31. Pinnavaia T.J., Park I., LeBaron P.C., and Triantafyllidis K.S. Epoxy clay fabric film composites with unprecedented oxygen barrier properties. Chemistry of Materials 18 (2006) 4393-4398
32. Ruhlicke G., and Niederbudde E.A. Determination of layer-charge density of expandable 2:1 clay minerals in soils and loess sediments using the alkylammonium method. Clay Minerals 20 3 (1985) 291-300
33. 2) system. Contributions to Mineralogy and Petrology 148 2 (2004) 180-200
34. Soma M., Tanaka A., Seyama H., Hayashi S., and Hayamizu K. Bonding states of sodium in tetrasilicic sodium fluor mica. Clay Science 8 (1990) 1-8
35. Taruta S., Obara R., Takusagawa N., and Kitajima K. Effect of layer charge on chemical and physical properties of synthetic K-fluorine micas. Journal of Materials Science 40 21 (2005) 5597-5602
36. Tateyama H., Nishimura S., Tsunematsu K., Jinnai K., Adachi Y., and Kimura M. Synthesis of expandable fluorine mica from talc. Clays and Clay Minerals 40 2 (1992) 180-185
37. Tenorio R.P., Alme L.R., Engelsberg M., Fossum J.O., and Hallwass F. Geometry and dynamics of intercalated water in Na-fluorhectorite clay hydrates. Journal of Physical Chemistry C 112 2 (2008) 575-580
38. Tetsuka H., Ebina T., Nanjo H., and Mizukami F. Highly transparent flexible clay films modified with organic polymer: structural characterization and intercalation properties. Journal of Materials Chemistry 17 33 (2007) 3545-3550
39. Utracki L.A., Sepehr M., and Boccaleri E. Synthetic, layered nanoparticles for polymeric nanocomposites WNCO. Polymers for Advanced Technologies 18 1 (2007) 1-37
40. 2O-NaF. Glastechnische Berichte 42 (1969) 506-509
41. 2 systems. Journal of the American Ceramic Society 76 8 (1993) 2059-2064
42. 2 system. ISIJ International 33 1 (1993) 26-35