NH3-TPD measurements using a zeolite-based sensor

Measurement Science and Technology

Volumn 21, Issue 2, 2010, Pages

  Rodríguez Gonzlez, Luz ^a   Simon, Ulrich ^a  

^a RWTH AACHEN UNIVERSITY   (Germany)

Author keywords

H ZSM 5; Impedance spectroscopy; Sensor; Zeolite

Indexed keywords

GAS CHROMATOGRAPHY; SENSORS; SPECTROSCOPY; THICK FILMS;

DIGITAL ELECTRODES; H-ZSM-5; IMPEDANCE SPECTROSCOPY; TPD MEASUREMENTS; ZEOLITE-BASED SENSORS;

ZEOLITES;

EID: 76149136955     PISSN: 09570233     EISSN: 13616501     Source Type: Journal    
DOI: 10.1088/0957-0233/21/2/027003     Document Type: Article

References (39)

1. Raichle A, Ramin M, Singer D, Hunger M, Traa Y and Weitkamp J 2001 Influence of the aluminium content of zeolite H-ZSM-5 on the conversion of methylcyclohexane into a high-quality synthetic steamcracker feedstock Catal. Commun. 2 69-74
2. Franke M E and Simon U 2004 Solvate-supported proton transport in zeolites Chem. Phys. Chem. 5 465-72
3. Busca G 2006 The surface acidity and basicity of solid oxides and zeolites Chem. Ind. 108 247-318
4. Zhang W, Bao X, Guo X and Wang X 1999 A high-resolution solid-state NMR study on nanostructured H-ZSM-5 zeolite Catal. Lett. 60 89-94
5. Katada N and Niwa M 2004 Analysis of acid properties of zeolite and non-zeolitic solid acid catalysts using temperature-programmed desorption of ammonia Catal. Surv. Asia 3 161-70
6. Jozefowics L C, Karge H G and Coker E N 1994 Microcalorimetric investigation of H-ZSM-5 zeolites using an ultrahigh-vacuum system for gas adsorption J. Phys. Chem. 98 8053-60
7. 3 modified by basic metal oxides J. Phys. Chem. 98 8067-73
8. Hirschler A E 1963 The measurements of catalyst acidity using indicators forming stable surface carbonium ions J. Catal. 2 428-39
9. Tanabe K 1970 Solid Acids and Bases (Tokyo: Kodanska Academic Press)
10. 27Al-MAS-NMR spectroscopy Appl. Catal. A: Gen. 328 174-82
11. Niwa M, Nishikawa S and Katada N 2005 IRMS-PD of ammonia for characterization of acid site in β-zeolite Micropor. Mesopor. Mater. 82 105-12 (Pubitemid 40777916)
12. Niwa M, Suzuki K, Katada N, Kanougi T and Atoguchi T 2005 Ammonia IRMS-TPD study on the distribution of acid sites in mordenite J. Phys. Chem. B 109 18749-57
13. Corma A 1997 From microporous to mesoporous molecular sieve materials and their use in catalysis Chem. Rev. 97 2373-420
14. Katada N, Igi H, Kim J and Niwa M 1997 Determination of the acidic properties of zeolite by theoretical analysis of temperature-programmed desorption of ammonia based on adsorption equilibrium J. Phys. Chem. B 101 5969-97
15. Niwa M and Katada N 1997 Measurements of acidic property of zeolites by temperature programmed desorption of ammonia Catal. Surv. Japan 1 215-26
16. Lónyi F and Valyon J 2001 A TPD and IR study of the surface species formed from ammonia on zeolite H-ZSM-5, H-Mordenite and H-Beta Micropor. Mesopor. Mater. 47 293-301
17. Franke M E, Sierka M, Simon U and Sauer J 2002 Translational proton motion in ZSM-5: energy barriers and jump barriers from DFT calculations Phys. Chem. Chem. Phys. 4 5207-16
18. Xu X, Wang J and Long Y 2006 Zeolite-based materials for gas sensors Sensors 6 1751-64
19. Franke M E, Simon U, Moos R, Knezevic A, Müller R and Plog C 2003 Development and working principle of an ammonia gas sensor based on a refined model for solvate supported proton transport in zeolites Phys. Chem. Chem. Phys. 5 5195-8
20. Neumeier S, Echterhof T, Boelling R, Pfeifer H and Simon U 2008 Zeolite based trace humidity sensor for high temperature applications in hydrogen atmosphere Sensors Actuators B 134 171-4
21. Sahner K, Hagen G, Schönauer D, Rei S and Moos R 2008 Zeolites-versatile materials for gas sensor Solid State Ion. 179 2416-23
22. Moos R, Muller R, Plog C, Knezevic A, Leye H, Irion E, Braun T, Marquardt K J and Binder K 2002 Selective ammonia exhaust gas sensor for automotive applications Sensors Actuators B 83 181-9
23. Schönauer D, Moos R, Fleischer M and Wiesner K 2009 Selective mixed potential ammonia exhaust gas sensor Sensors Actuators B 140 585-90
24. Satsuma A, Shimizu K, Hattori T, Nishiyama H, Kakimoto S, Sugaya S and Yokoi H 2007 Polytungstate clusters on zirconia as a sensing material for a selective ammonia gas sensor Sensors Actuators B 123 757-62
25. Satsuma A, Shimizu K, Kashiwagi K, Endo T, Nishiyama H, Kakimoto S, Sugaya S and Yokoi H 2007 Ammonia sensing mechanism of tungstated-zirconia thick film sensor J. Phys. Chem C 111 12080-5
26. Kubinski D J and Visser J H 2008 Sensor and method for determining the ammonia loading of a zeolite SCR catalyst Sensors Actuators B 130 425-9
27. Sahner K and Moos R 2008 p-type semiconducting perovskite sensors for reducing gases-model description Sensor Lett. 6 808-11
28. Wang D Y, Yao S, Shost M, Yoo J, Cabush D, Racine D, Cloudt R and Willems F 2008 Ammonia sensor for closed-loop SCR control SAE Paper 2008-01-0919
29. 3 from zeolite H-ZSM-5 Solid State Ion. 179 1968-73
30. Simon U, Sanders D, Jockel J, Heppel C and Brinz T 2002 Design strategies for multielectrode arrays applicable for high-throughput impedance spectroscopy on novel gas sensor materials J. Comb. Chem. 4 511-5
31. Rodriguez-Gonzalez L 2007 Entwicklung einer neuen Methode zur impedanzspektroskopischen Erfassung der temperaturprogrammierten Desorption von Ammoniak in H-Form Zeolithen Doctoral Thesis RWTH Aachen University
32. Niwa M, Katada N, Sawa M and Murakami Y 1995 Temperature-programmed description of ammonia with readsorption based on the derived theoretical equation J. Phys. Chem. 99 8812-6
33. Cvetanovic R J and Amenomiya Y 1967 Application of a temperature- programmed desorption technique to catalyst studies Adv. Catal. 17 103-49
34. Forni L, Vatti F P and Ortoleva E 1995 Temperature-programmed desorption-diffusion of ammonia in molecular sieves V.ZSM-5 zeolite Micropor. Mater. 3 367-75
35. Parrillo E J and Gorte R J 1998 Design parameters for the construction and operation of heat flow calorimeters Thermochim. Acta 312 125-32
36. Lee C, Parrillo D J, Gorte R J and Farneth W E 1996 Relationship between differential heats of adsorption and Brønsted acid strengths of acidic zeolites: H-ZSM-5 and H-Mordenite J. Am. Chem. Soc. 118 3262-8
37. Farneth W E and Gorte R J 1995 Methods for characterizing zeolite acidity Chem. Rev. 95 615-35
38. Niwa M and Katada N 1997 Measurements of acidic property of zeolites by temperature programmed desorption of ammonia Catal. Surv. Japan 1 215-26
39. Gorte R J 1999 What do we know about the acidity of solid acids? Catal. Lett. 62 1-13