Solid-phase microextraction using a diglycidyloxycalix[4]arene coated fiber combined with gas chromatography: Very simple, rapid and sensitive method for the determination of chlorobenzenes in water

Microchimica Acta

Volumn 168, Issue 1-2, 2010, Pages 161-167

  Li, Xiu Juan ^a   Ye, Chang Wen ^a   Huo, Xue Lian ^b   Zeng, Zhaorui ^b  

^a HUAZHONG AGRICULTURAL UNIVERSITY   (China)

^b WUHAN UNIVERSITY   (China)

Author keywords

Calixarene; Chlorobenzenes; Gas chromatography; Solid phase microextraction; Water

Indexed keywords

EID: 75749124330     PISSN: 00263672     EISSN: 14365073     Source Type: Journal    
DOI: 10.1007/s00604-009-0276-6     Document Type: Article

References (28)

1. Belardi RP, Pawliszyn J (1989) The application of chemically modified fused silica fibers in the extraction of organics from water matrix samples and their rapid transfer to capillary columns. Water Pollut Res J Can 24: 179-191.
2. Zhang Z, Yang MJ, Pawliszyn J (1994) Solid-phase microextraction. A solvent-free alternative for sample preparation. Anal Chem 66: 844A-853A. doi: 10. 1021/ac00089a001.
3. Lambropoulou DA, Konstantinou IK, Albanis TA (2007) Recent developments in headspace microextraction techniques for the analysis of environmental contaminants in different matrices. J Chromatogr A 1152: 70-96. doi: 10. 1016/j. chroma. 2007. 02. 094.
4. Vílchez JL, Prieto A, Araujo L, Navalón A (2006) Application of isotope dilution to the determination of anthracene in environmental samples by headspace solid-phase microextraction and gas chromatography-mass spectrometry. Microchim Acta 155: 435-439. doi: 10. 1007/s00604-006-0577-y.
5. Mullett WM, Pawliszyn J (2003) The development of selective and biocompatible coatings for solid phase microextraction. J Sep Sci 26: 251-260. doi: 10. 1002/jssc. 200390031.
6. Li X, Zeng Z, Gao S, Li H (2004) Preparation and characteristics of sol-gel-coated calix[4]arene fiber for solid-phase microextraction. J Chromatogr A 1023: 15-25. doi: 10. 1016/j. chroma. 2003. 09. 042.
7. Li X, Zeng Z, Zhou J, Gong S, Wang W, Chen Y (2004) Novel fiber coated with amide bridged-calix[4]arene used for solid-phase microextraction of aliphatic amines. J Chromatogr A 1041: 1-15. doi: 10. 1016/j. chroma. 2004. 04. 059.
8. Li X, Gong S, Zeng Z (2005) Development of sol-gel procedure for preparation of diglycidyloxycalix[4]arene solid-phase microextraction fiber with enhanced extraction efficiency. Chromatographia 62: 519-525. doi: 10. 1365/s10337-005-0665-x0009-5893/05/11.
9. Ye CW, Gao J, Yang C, Liu XJ, Li XJ, Pan SY (2009) Development and application of an SPME/GC method for the determination of trace phthalates in beer using a calix[6]arene fiber. Anal Chim Acta 641: 64-74. doi: 10. 1016/j. aca. 2009. 02. 052.
10. Li X, Zeng Z, Zhou J (2004) High thermal-stable sol-gel-coated calix[4]arene fiber for solid-phase microextraction of chlorophenols. Anal Chim Acta 509: 27-37. doi: 10. 1016/j. aca. 2003. 12. 008.
11. Zhou F, Li X, Zeng Z (2005) Determination of phenolic compounds in wastewater samples using a novel fiber by solid-phase microextraction coupled to gas chromatography. Anal Chim Acta 538: 63-70. doi: 10. 1016/j. aca. 2005. 02. 009.
12. Li X, Zeng Z, Xu Y (2006) A solid-phase microextraction fiber coated with diglycidyloxycalix[4] arene yields very high extraction selectivity and sensitivity during the analysis of chlorobenzenes in soil. Anal Bioanal Chem 384: 1428-1437. doi: 10. 1007/s00216-005-0281-5.
13. Li X, Zeng Z, Zeng Y (2007) Solid-phase microextraction coupled to gas chromatography for the determination of 2, 3-dimethyl-2, 3-dinitrobutane as a marking agent for explosives. Talanta 72: 1581-1585. doi: 10. 1016/j. talanta. 2007. 02. 018.
14. Li X, Zeng Z, Hu M, Mao M (2005) High operationally stable sol-gel diglycidyloxycalix[4] arene fiber for solid-phase microextraction of propranolol in human urine. J Sep Sci 28: 2489-2500. doi: 10. 1002/jssc. 200500029.
15. Wang Y, Lee HK (1998) Determination of chlorobenzenes in water by solid-phase extraction and gas chromatography-mass spectrometry. J Chromatogr A 803: 219-225. doi: 10. 1016/S0021-9673(97)01252-1.
16. Oliver BG, Bothen KD (1980) Determination of chlorobenzenes in water by capillary gas chromatography. Anal Chem 52: 2066-2069. doi: 10. 1021/ac50063a017.
17. Melcher RG, Morabito PL (1990) Membrane/gas chromatographic system for automated extraction and determination of trace organics in aqueous samples. Anal Chem 62: 2183-2188. doi: 10. 1021/ac00219a006.
18. Vidal L, Canals A, Kalogerakis N, Psillakis E (2005) Headspace single-drop microextraction for the analysis of chlorobenzenes in water samples. J Chromatogr A 1089: 25-30. doi: 10. 1016/j. chroma. 2005. 06. 058.
19. Tor A (2006) Determination of chlorobenzenes in water by drop-based liquid-phase microextraction and gas chromatography-electron capture detection. J Chromatogr A 1125: 129-132. doi: 10. 1016/j. chroma. 2006. 06. 081.
20. Vidal L, Psillakis E, Domini CE, Grané N, Marken F, Canals A (2007) An ionic liquid as a solvent for headspace single drop microextraction of chlorobenzenes from water samples. Anal Chim Acta 584: 189-195. doi: 10. 1016/j. aca. 2006. 10. 053.
21. Vidal L, Domini CE, Grané N, Psillakis E, Canals A (2007) Microwave-assisted headspace single-drop microextraction of chlorobenzenes from water samples. Anal Chim Acta 592: 9-15. doi: 10. 1016/j. aca. 2007. 03. 066.
22. Zhao F, Lu S, Du W, Zeng B (2009) Ionic liquid-based headspace single-drop microextraction coupled to gas chromatography for the determination of chlorobenzene derivatives. Microchim Acta 165: 29-33. doi: 10. 1007/s00604-008-0092-4.
23. Chisvert A, Románb IP, Vidal L, Canals A (2009) Simple and commercial readily-available approach for the direct use of ionic liquid-based single-drop microextraction prior to gas chromatography Determination of chlorobenzenes in real water samples as model analytical application. J Chromatogr A 1216: 1290-1295. doi: 10. 1016/j. chroma. 2008. 12. 078.
24. Kozani RR, Assadi Y, Shemirani F, Hosseini MM, Jamali MR (2007) Part-per-trillion determination of chlorobenzenes in water using dispersive liquid-liquid microextraction combined gas chromatography-electron capture detection. Talanta 72: 387-393. doi: 10. 1016/j. talanta. 2006. 10. 039.
25. He Y, Wang Y, Lee HK (2000) Trace analysis of ten chlorinated benzenes in water by headspace solid-phase microextraction. J Chromatogr A 874: 149-154. doi: 10. 1016/s0021-9673(00)00067-4.
26. Li X, Chen J, Du L (2007) Analysis of chloro- and nitrobenzenes in water by a simple polyaniline-based solid-phase microextraction coupled with gas chromatography. J Chromatogr A 1140: 21-28. doi: 10. 1016/j. chroma. 2006. 11. 044.
27. United States Environmental Protection Agency (EPA), Method 8121, Rev. 0 (1994) Chlorinated hydrocarbons by gas chromatography: capillary column technique. U. S. EPA, September, 1994. http://www. epa. gov/waste/hazard/testmethods/sw846/online/index. htm.
28. American Society for Testing and Materials (ASTM), D6520-00 (2000) Standard practice for the solid phase micro extraction (SPME) of water and its headspace for the analysis of volatile and semi-volatile organic compounds. ASTM International, ASTM Committee D-19, January 10, 2000. http://www. astm. org/Standards/D6520. htm.