메뉴 건너뛰기




Volumn 203, Issue 1, 2010, Pages 73-80

Selective heteronuclear Hartmann-Hahn: A multiple-pulse sequence for selective magnetization transfer in the structural elucidation of "isotagged" oligosaccharides

Author keywords

2D NMR; Glycan; Heteronuclear Hartmann Hahn; Oligosaccharide; Peracetylation; Polarization transfer; Scandium triflate; Selective

Indexed keywords

GLYCAN; HARTMANN; HETERONUCLEAR; POLARIZATION TRANSFER; SCANDIUM TRIFLATE;

EID: 75749113994     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2009.12.003     Document Type: Article
Times cited : (3)

References (33)
  • 1
    • 36149026370 scopus 로고
    • Nuclear double resonance in the rotating frame
    • Hartmann S.R., and Hahn E.L. Nuclear double resonance in the rotating frame. Phys. Rev. 128 (1973) 2042-2053
    • (1973) Phys. Rev. , vol.128 , pp. 2042-2053
    • Hartmann, S.R.1    Hahn, E.L.2
  • 2
    • 36849106840 scopus 로고
    • Proton-enhanced NMR of dilute spins in solids
    • Pines A., Gibby M.G., and Waugh J.S. Proton-enhanced NMR of dilute spins in solids. J. Chem. Phys. 59 (1962) 569-590
    • (1962) J. Chem. Phys. , vol.59 , pp. 569-590
    • Pines, A.1    Gibby, M.G.2    Waugh, J.S.3
  • 4
    • 48749147783 scopus 로고
    • An improved sequence for broad-band decoupling - WALTZ-16
    • Shaka A.J., Keeler J., Frenkiel T., and Freeman R. An improved sequence for broad-band decoupling - WALTZ-16. J. Magn. Reson. 52 (1983) 335-338
    • (1983) J. Magn. Reson. , vol.52 , pp. 335-338
    • Shaka, A.J.1    Keeler, J.2    Frenkiel, T.3    Freeman, R.4
  • 5
    • 5144233105 scopus 로고
    • MLEV-17-based two-dimensional homonuclear magnetization transfer spectroscopy
    • Bax A., and Davis D.G. MLEV-17-based two-dimensional homonuclear magnetization transfer spectroscopy. J. Magn. Reson. 65 (1985) 355-360
    • (1985) J. Magn. Reson. , vol.65 , pp. 355-360
    • Bax, A.1    Davis, D.G.2
  • 6
    • 45949117739 scopus 로고
    • Improved techniques for homonuclear rotating-frame and isotropic mixing experiments
    • Rance M. Improved techniques for homonuclear rotating-frame and isotropic mixing experiments. J. Magn. Reson. 74 (1987) 557-564
    • (1987) J. Magn. Reson. , vol.74 , pp. 557-564
    • Rance, M.1
  • 7
    • 45449123980 scopus 로고
    • Iterative schemes for bilinear operators - application to spin decoupling
    • Shaka A.J., Lee C.J., and Pines A. Iterative schemes for bilinear operators - application to spin decoupling. J. Magn. Reson. 77 (1988) 274-293
    • (1988) J. Magn. Reson. , vol.77 , pp. 274-293
    • Shaka, A.J.1    Lee, C.J.2    Pines, A.3
  • 8
    • 0000492963 scopus 로고
    • Broadband homonuclear cross polarization in 2D NMR using DIPSI-2
    • Rucker S.P., and Shaka A.J. Broadband homonuclear cross polarization in 2D NMR using DIPSI-2. Mol. Phys. 68 (1989) 509-517
    • (1989) Mol. Phys. , vol.68 , pp. 509-517
    • Rucker, S.P.1    Shaka, A.J.2
  • 9
    • 0344448273 scopus 로고
    • Coherence transfer by isotropic mixing - application to proton correlation spectroscopy
    • Braunschweiler L., and Ernst R.R. Coherence transfer by isotropic mixing - application to proton correlation spectroscopy. J. Magn. Reson. 53 (1983) 521-528
    • (1983) J. Magn. Reson. , vol.53 , pp. 521-528
    • Braunschweiler, L.1    Ernst, R.R.2
  • 10
    • 0000354437 scopus 로고
    • Improvements in C-13 broad-band homonuclear cross-polarization for 2D and 3D NMR
    • Mohebbi A., and Shaka A.J. Improvements in C-13 broad-band homonuclear cross-polarization for 2D and 3D NMR. Chem. Phys. Lett. 178 (1991) 374-378
    • (1991) Chem. Phys. Lett. , vol.178 , pp. 374-378
    • Mohebbi, A.1    Shaka, A.J.2
  • 11
    • 0000284431 scopus 로고
    • Hetero-TOCSY experiments with WALTZ and DIPSI mixing sequences
    • Brown L.R., and Sanctuary B.C. Hetero-TOCSY experiments with WALTZ and DIPSI mixing sequences. J. Magn. Reson. 91 (1991) 413-421
    • (1991) J. Magn. Reson. , vol.91 , pp. 413-421
    • Brown, L.R.1    Sanctuary, B.C.2
  • 12
    • 0009195494 scopus 로고
    • The use of heteronuclear cross polarization to enhance the sensitivity of triple-resonance NMR experiments - improved 4D HCNNH pulse sequences
    • Richardson J.M., Clowes R.T., Boucher W., Domaille P.J., Hardman C.H., Keeler J., and Laue E.D. The use of heteronuclear cross polarization to enhance the sensitivity of triple-resonance NMR experiments - improved 4D HCNNH pulse sequences. J. Magn. Reson. Ser. B 101 (1993) 223-227
    • (1993) J. Magn. Reson. Ser. B , vol.101 , pp. 223-227
    • Richardson, J.M.1    Clowes, R.T.2    Boucher, W.3    Domaille, P.J.4    Hardman, C.H.5    Keeler, J.6    Laue, E.D.7
  • 13
    • 0010562609 scopus 로고    scopus 로고
    • "Kin" HEHAHA sequences, heteronuclear Hartmann-Hahn transfer with different bandwidths for spins I and S
    • Carlomagno T., Luy B., and Glaser S.J. "Kin" HEHAHA sequences, heteronuclear Hartmann-Hahn transfer with different bandwidths for spins I and S. J. Magn. Reson. 126 (1997) 110-119
    • (1997) J. Magn. Reson. , vol.126 , pp. 110-119
    • Carlomagno, T.1    Luy, B.2    Glaser, S.J.3
  • 14
    • 0001280375 scopus 로고    scopus 로고
    • Band-selective hetero- and homonuclear cross-polarization using trains of shaped pulses
    • Zuiderweg E.R.P., Zeng L., Brutscher B., and Morshauser R.C. Band-selective hetero- and homonuclear cross-polarization using trains of shaped pulses. J. Biomol. NMR 8 (1996) 147-160
    • (1996) J. Biomol. NMR , vol.8 , pp. 147-160
    • Zuiderweg, E.R.P.1    Zeng, L.2    Brutscher, B.3    Morshauser, R.C.4
  • 15
    • 0036435401 scopus 로고    scopus 로고
    • An effective strategy for structural elucidation of oligosaccharides through NMR spectroscopy combined with peracetylation using doubly C-13-labeled acetyl groups
    • Bendiak B., Fang T.T., and Jones D.N.M. An effective strategy for structural elucidation of oligosaccharides through NMR spectroscopy combined with peracetylation using doubly C-13-labeled acetyl groups. Can. J. Chem. 80 (2002) 1032-1050
    • (2002) Can. J. Chem. , vol.80 , pp. 1032-1050
    • Bendiak, B.1    Fang, T.T.2    Jones, D.N.M.3
  • 16
    • 0032718996 scopus 로고    scopus 로고
    • 13C-O-acetylated oligosaccharides: expanding the dimensions for carbohydrate structures
    • 13C-O-acetylated oligosaccharides: expanding the dimensions for carbohydrate structures. J. Biomol. NMR 15 (1999) 157-168
    • (1999) J. Biomol. NMR , vol.15 , pp. 157-168
    • Jones, D.N.M.1    Bendiak, B.2
  • 17
    • 13444256166 scopus 로고    scopus 로고
    • Rapid high-resolution four-dimensional NMR spectroscopy using the filter diagonalization method and its advantages for detailed structural elucidation of oligosaccharides
    • Armstrong G.S., Mandelshtam V.A., Shaka A.J., and Bendiak B. Rapid high-resolution four-dimensional NMR spectroscopy using the filter diagonalization method and its advantages for detailed structural elucidation of oligosaccharides. J. Magn. Reson. 173 (2005) 160-168
    • (2005) J. Magn. Reson. , vol.173 , pp. 160-168
    • Armstrong, G.S.1    Mandelshtam, V.A.2    Shaka, A.J.3    Bendiak, B.4
  • 18
    • 33845560617 scopus 로고
    • Enhancement of nuclear magnetic resonance signals by polarization transfer
    • Morris G.A., and Freeman R. Enhancement of nuclear magnetic resonance signals by polarization transfer. J. Am. Chem. Soc. 101 (1979) 760-762
    • (1979) J. Am. Chem. Soc. , vol.101 , pp. 760-762
    • Morris, G.A.1    Freeman, R.2
  • 19
    • 0345311216 scopus 로고
    • H-1 and C-13 assignments from sensitivity-enhanced detection of heteronuclear multiple-bond connectivity by 2D multiple quantum NMR
    • Bax A., and Summers M.F. H-1 and C-13 assignments from sensitivity-enhanced detection of heteronuclear multiple-bond connectivity by 2D multiple quantum NMR. J. Am. Chem. Soc. 108 (1986) 2093-2094
    • (1986) J. Am. Chem. Soc. , vol.108 , pp. 2093-2094
    • Bax, A.1    Summers, M.F.2
  • 20
    • 0001736119 scopus 로고
    • An improved method for two-dimensional heteronuclear relayed-coherence-transfer NMR spectroscopy
    • Bax A., Davis D.G., and Sarkar S.K. An improved method for two-dimensional heteronuclear relayed-coherence-transfer NMR spectroscopy. J. Magn. Reson. 63 (1985) 230-234
    • (1985) J. Magn. Reson. , vol.63 , pp. 230-234
    • Bax, A.1    Davis, D.G.2    Sarkar, S.K.3
  • 21
    • 84888390140 scopus 로고
    • Coherence transfer in the rotating frame, application to heteronuclear cross-correlation spectroscopy
    • Müller L., and Ernst R.R. Coherence transfer in the rotating frame, application to heteronuclear cross-correlation spectroscopy. Mol. Phys. 38 (1979) 963-992
    • (1979) Mol. Phys. , vol.38 , pp. 963-992
    • Müller, L.1    Ernst, R.R.2
  • 23
    • 0000375910 scopus 로고
    • Optimized heteronuclear cross polarization in liquids
    • Ernst M., Griesinger C., Ernst R.R., and Bermel W. Optimized heteronuclear cross polarization in liquids. Mol. Phys. 74 (1991) 219-252
    • (1991) Mol. Phys. , vol.74 , pp. 219-252
    • Ernst, M.1    Griesinger, C.2    Ernst, R.R.3    Bermel, W.4
  • 24
    • 36049055838 scopus 로고
    • Coherent averaging effects in magnetic resonance
    • Haeberlen U., and Waugh J.S. Coherent averaging effects in magnetic resonance. Phys. Rev. 175 (1968) 453-467
    • (1968) Phys. Rev. , vol.175 , pp. 453-467
    • Haeberlen, U.1    Waugh, J.S.2
  • 25
    • 75749083400 scopus 로고
    • A theoretical-study of coherence transfer by isotropic mixing - calculation of pulse sequence performance for systems of biological interest
    • Remeroski M.L., Glaser S.J., and Drobny G.P. A theoretical-study of coherence transfer by isotropic mixing - calculation of pulse sequence performance for systems of biological interest. J. Magn. Reson. 68 (1989) 110-131
    • (1989) J. Magn. Reson. , vol.68 , pp. 110-131
    • Remeroski, M.L.1    Glaser, S.J.2    Drobny, G.P.3
  • 26
    • 0343457477 scopus 로고
    • The time dependence of coherence transfer in homonuclear isotropic mixing experiments
    • Cavanagh J., Chazin W.J., and Rance M. The time dependence of coherence transfer in homonuclear isotropic mixing experiments. J. Magn. Reson. 87 (1990) 110-131
    • (1990) J. Magn. Reson. , vol.87 , pp. 110-131
    • Cavanagh, J.1    Chazin, W.J.2    Rance, M.3
  • 27
    • 85006911915 scopus 로고
    • A theorem relating cross-relaxation and Hartmann-Hahn transfer in multiple-pulse sequences - optimal suppression of TOCSY transfer in ROESY
    • Schleucher J., Quant J., Glaser S.J., and Griesinger C. A theorem relating cross-relaxation and Hartmann-Hahn transfer in multiple-pulse sequences - optimal suppression of TOCSY transfer in ROESY. J. Magn. Reson. A 112 (1995) 144-151
    • (1995) J. Magn. Reson. A , vol.112 , pp. 144-151
    • Schleucher, J.1    Quant, J.2    Glaser, S.J.3    Griesinger, C.4
  • 28
    • 0000151181 scopus 로고
    • False transverse NOE enhancements in CAMELSPIN spectra
    • Keeler J., and Neuhaus D. False transverse NOE enhancements in CAMELSPIN spectra. J. Magn. Reson. 68 (1986) 568-574
    • (1986) J. Magn. Reson. , vol.68 , pp. 568-574
    • Keeler, J.1    Neuhaus, D.2
  • 29
    • 0012615648 scopus 로고    scopus 로고
    • Scandium trifluoromethanesulfonate as an extremely active Lewis acid catalyst in acylation of alcohols with acid anhydrides and mixed anhydrides
    • Ishihara K., Kubota M., Kurihara H., and Yamamoto H. Scandium trifluoromethanesulfonate as an extremely active Lewis acid catalyst in acylation of alcohols with acid anhydrides and mixed anhydrides. J. Org. Chem. 61 (1996) 4560-4567
    • (1996) J. Org. Chem. , vol.61 , pp. 4560-4567
    • Ishihara, K.1    Kubota, M.2    Kurihara, H.3    Yamamoto, H.4
  • 30
    • 45949124641 scopus 로고
    • Broadband spin decoupling in isotropic liquids
    • Shaka A.J., and Keeler J. Broadband spin decoupling in isotropic liquids. Prog. NMR Spect. 19 (1987) 47-129
    • (1987) Prog. NMR Spect. , vol.19 , pp. 47-129
    • Shaka, A.J.1    Keeler, J.2
  • 31
    • 0042819665 scopus 로고    scopus 로고
    • Elimination of zero-quantum interference in two-dimensional NMR spectra
    • Thrippleton M.J., and Keeler J. Elimination of zero-quantum interference in two-dimensional NMR spectra. Angew. Chem. Int. Ed. 42 (2003) 3938-3941
    • (2003) Angew. Chem. Int. Ed. , vol.42 , pp. 3938-3941
    • Thrippleton, M.J.1    Keeler, J.2
  • 32
    • 45249127991 scopus 로고
    • Rapid recording of 2D NMR spectra without phase cycling - application to the study of hydrogen-exchange in proteins
    • Marion D., Ikura M., Tschudin R., and Bax A. Rapid recording of 2D NMR spectra without phase cycling - application to the study of hydrogen-exchange in proteins. J. Magn. Reson. 85 (1989) 393-399
    • (1989) J. Magn. Reson. , vol.85 , pp. 393-399
    • Marion, D.1    Ikura, M.2    Tschudin, R.3    Bax, A.4
  • 33
    • 0001634007 scopus 로고
    • z-filters for purging phase-distorted or multiplet-distorted spectra
    • Sørensen O.W., Rance M., and Ernst R.R. z-filters for purging phase-distorted or multiplet-distorted spectra. J. Magn. Reson. 56 (1984) 527-534
    • (1984) J. Magn. Reson. , vol.56 , pp. 527-534
    • Sørensen, O.W.1    Rance, M.2    Ernst, R.R.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.